FTS Dura-Dry II User manual

Document # MNL-032-A, Rev. 004, 12/07
Dura-Dry II
Condenser Module
Operator’s Manual
FTS
3538 Main Street
Stone Ridge, NY 12484 USA
www.SPIndustries.com
[phone] or 001 [phone]
SP Service:
[phone] or 001 [phone]
FAX: [phone]
E-Mail: [email protected]
™

© SP Industries, Inc. Rev.004, 12/07
ii
Notice
This Operation Manual contains confidential and proprietary information of SP Industries, Inc. and
may be used only by a recipient designated by and for purposes specified by SP Industries, Inc.
Reproduction of, dissemination of, modifications to, or the creation of derivative works from this
manual, by any means and in any form or manner, is expressly prohibited, except with the prior
written permission of SP Industries, Inc. Permitted copies of this document must retain all proprietary
notices contained in the original.
The information in this document is subject to change without prior notice. Always confirm with SP
Industries, Inc. that you are using the most current version of this document. SP Industries, Inc. is
free to modify any of its products and services, in any manner and at any time, notwithstanding the
information contained in this document.
THE CONTENTS OF THIS DOCUMENT SHALL NOT CONSTITUTE ANY WARRANTY OF ANY
KIND, EITHER EXPRESSED OR IMPLIED, INCLUDING BUT NOT LIMITED TO THE IMPLIED
WARRANTIES OF MERCHANTABILITY AND/OR FITNESS FOR A PARTICULAR PURPOSE OR
GIVE RISE TO ANY LIABILITY OF SP INDUSTRIES, INC., ITS AFFILIATES OR ITS SUPPLIERS.
The terms and conditions governing the use of this Operation Manual shall consist of those set forth
in written agreements with SP Industries, Inc.
All brand or product names mentioned may be trademarks or registered trademarks of their respective companies.
© 2007 SP Industries, Inc. All marks herein are used under license.

© SP Industries, Inc. Rev.004, 12/07
iii
Contents
Important Symbols......................................................................................................................4
Foreward......................................................................................................................................5
Safety Precautions ...........................................................................................................................5
Inspection .........................................................................................................................................6
Overview......................................................................................................................................7
Installation...................................................................................................................................9
Unpacking.........................................................................................................................................9
Physical Location............................................................................................................................10
Ambient Air Requirements .............................................................................................................10
Electrical Requirements .................................................................................................................10
Vacuum Pump Installation and Maintenance.................................................................................11
Liquid Nitrogen Trap.................................................................................................................12
Installation.......................................................................................................................................13
Operation........................................................................................................................................14
Cleaning..........................................................................................................................................14
Pre-Operational Baseline Performance Test.........................................................................15
System Start-Up........................................................................................................................16
Microprocessor Control Panel ........................................................................................................16
Normal Operation ...........................................................................................................................17
Installation for Manifold Systems............................................................................................18
Installation.......................................................................................................................................19
Installation and Use of Quick-Vac Valves ......................................................................................19
Diagram of Quick-Vac Valves ........................................................................................................20
System Defrost and Shut Off...................................................................................................21
Troubleshooting........................................................................................................................22
General...........................................................................................................................................22
Removing the Condenser...............................................................................................................24
Vacuum Leak Troubleshooting Procedure.....................................................................................25
Maintenance ..............................................................................................................................26
Service & Warranties................................................................................................................28
FTS Warranties and Service Agreements......................................................................................28
Standard Warranty .........................................................................................................................29
Service Options ..............................................................................................................................30
Return of FTS Equipment...............................................................................................................31
Material Safety Data Sheets.....................................................................................................32

© SP Industries, Inc. Rev.004, 12/07
4
Important Symbols
Warning! Refer to manual text. Injury or even death
may result if a recommendation marked with this symbol
is not heeded.
Electric Shock Danger! Use appropriate caution to avoid injury or death.
Burn Danger! Potentially hot surface. Use appropriate caution.
Do not store flammable materials in chamber.
Wear Safety Glasses.
Crush Hazard. Keep hands clear when operating door.
Corrosive Chemical. Wear suitable gloves, safety glasses, and protective clothing.
Property Caution! To prevent damage to chamber equipment and/or load, adhere to
procedures marked by this symbol.
Practical Operating Tip. These recommendations streamline unit operation and prevent
common operator errors.

© SP Industries, Inc. Rev.004, 12/07
5
Foreward
Thank you for buying an SP Industries / Hotpack product. Our goal is 100 percent customer
satisfaction. If you are in any way dissatisfied with your order, please contact us immediately.
Safety Precautions
Your satisfaction and safety will be assured by a complete understanding of this equipment.
To assure your satisfaction and safety, as end user of this equipment, it is the operator’s
responsibility to understand its function and operational characteristics. Before operating this
equipment please read this instruction manual thoroughly. Ensure that all operators receive
appropriate training.
Awareness of the stated cautions and warnings, compliance with recommended operating
parameters, and performance of periodic maintenance requirements are important for safe and
satisfactory operation.
Your instruction and maintenance manual is valuable as it contains information to help you better
understand and operate the equipment you have purchased. It includes a wiring diagram and
contact numbers, which you may require at some future date. Keep it close at hand and refer to it
often. Additional manuals may be purchased from our Parts Department.
If any part of these instructions is not clearly understood, please feel free to contact Customer
Service for clarification.
If you require replacement parts, we must have the model and serial numbers plus all electrical
information from the nameplate.
The unit should be used for its intended application; alterations or modifications will void the
warranty. This product is not intended, nor can it be used, as a sterile or patient-connected
device, nor is it designed for use in Class I, II, or III locations as defined by the National Electrical
Code.
Never use with toxic, corrosive, flammable or organic materials unless special precautions are in
place to prevent injury to personnel or damage to equipment.
Never operate unit without all covers in place.
Never clean with solvents. Use mild detergent and water only.
Never allow hands or body to be exposed to open vacuum ports.
WARNING! FOLLOW THESE INSTRUCTIONS TO AVOID INJURY AND/OR DAMAGE TO
EQUIPMENT.
CAUTION
As a routine safety precaution, always wear safety glasses when working with
this equipment.

Operator’s Manual: Dura Dry II Foreward
© SP Industries, Inc. Rev.004, 12/07
6
Always verify that the electric service and other utilities match the unit’s requirements before
connecting to power.
Always wear safety glasses when using glass flasks.
Always practice team lifting when moving heavy equipment.
Always ensure that refrigeration air intake is clear and clean.
Always ensure that only an authorized technician services the refrigeration, heat transfer,
vacuum and electrical systems.
Always assume that internal parts may be very cold or very hot. Utilize personal protective
equipment to avoid burns.
Inspection
This merchandise was carefully packed and thoroughly inspected before leaving our factory.
Save all packing material if apparatus is received damaged.
Responsibility for its safe delivery is assumed by the carrier upon acceptance of the shipment,
therefore, claims for loss or damage sustained in transit must be made upon the carrier by
recipient as follows:
Visible loss or damage
Note any external evidence of loss or damage on the freight bill, or express receipt, and have it
signed by the carrier's agent. Failure to adequately describe any such external evidence of loss
or damage may result in carrier's refusing to honor your damage claim. The form required to file
such a claim will be supplied by the carrier.
Concealed loss or damage
Concealed loss or damage means loss or damage which does not become apparent until the
merchandise has been unpacked and inspected. Should either be discovered, make a written
request for inspection by the carrier's agent with 15 days of the delivery date; then file a claim
with the carrier since the damage is the carrier's responsibility. By following these instructions
carefully, we guarantee our full support of your claim to be compensated for loss from concealed
damage.
Do not -- for any reason -- return this unit without first obtaining authorization. Please
supply nameplate data, including model number and serial number, in any
correspondence to the manufacturer.
WARNING
DO NOT STORE OR PROCESS FLAMMABLE MATERIALS This unit is
not designed (nor is it intended to be used) for the purpose of processing
or storage of materials that may contain volatile flammable solvents or that
may emit flammable vapors during processing or storage.

© SP Industries, Inc. Rev.004, 12/07
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Overview
The Dura-Dry II MP Condenser Modules are the most durable condenser modules available. The
stainless steel condenser and stainless steel condenser housing are virtually indestructible
regardless of the acid or solvent your product may contain. This system features a
microprocessor control complete with digital temperature and vacuum indication, as well as
system status and diagnostic indicators to provide you with the most advanced laboratory freeze-
dryer available. The Dura-Dry II MP Condenser Module is available in -85°C condenser
configuration. The Dura-Dry also features a hinged cabinet front for complete accessibility of the
vacuum pump and other internal components, as well as completely visible condenser and
standard hot gas defrost. The result is the most durable condenser module available anywhere.
Additional standard features for the Dura-Dry II MP Condenser Module include a convenient
drain line, stainless steel top work surface, as well as an easily removable condenser. All of these
features are provided to you to insure the most dependable and repeatable freeze-drying
available today.
Front View
1. Chamber Door
2. Microprocessor Control
3. Vacuum Pump Access Door
Model Specifications FD2085
Performance 20 liters per 24 hours with maximum low condenser
temperature at -85°C, MP control
Dimensions W x D x
H
32 x 29.5 x 33.5” (81.3 x 75 x 85 cm)
Weight lbs/kg 435/198
Electrical130A without vacuum pump
1Available for 208V/60Hz, 220V/50Hz or 200V/50Hz. Vacuum pump electrical requirements are not included.
Add 6A for vacuum pump. All high voltage components are located in an enclosed electrical housing to meet
international standards.
1
3
2
Options: Can be used as a
manifold system with the
Dura-Port manifold, or at any
time in the future as a tray
dryer with the stoppering or
bulk tray dryer chambers.

Operator’s Manual: Dura Dry II Overview
© SP Industries, Inc. Rev.004, 12/07
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Rear Panel Hookups
1. Communication Port
2. Sterile Air Inlet
3. Circuit Breaker
Right Side Condenser Ventilation
12
3

© SP Industries, Inc. Rev.004, 12/07
9
Installation
Unpacking
The Dura-Dry II MP is packed and shipped complete with vacuum pump in its own carton.
Certain items, such as a Liquid Nitrogen Trap, will be shipped in a separate container.
Remove from the packing material and make a visual inspection for shipping damage.
Concealed damage can occur even if the crate or carton is undamaged. This damage is the
responsibility of the transportation company. If the equipment has suffered shipping damage,
contact the transportation company immediately. All packing material must be kept for their
inspection.
FTS carefully tests all products thoroughly for quality and operational specifications prior to
shipment. The products are adequately packed to ensure their quality and operational status.
Before placing the unit in its permanent location, record the following information.
9Serial Number__________________________
9
9Model Number_________________________
9
9Electrical Requirement___________________
NOTE:The above information is located on a tag in the rear of the machine where the line cord
enters the machine.
If you need to contact FTS regarding the performance or operation of the unit, the above
information will allow us to respond in a more timely fashion.

Operator’s Manual: Dura Dry II Installation
© SP Industries, Inc. Rev.004, 12/07
10
Physical Location
The Dura-Dry II MP Condenser Module is mounted on heavy-duty casters and may be rolled
into place at this time. Since this is an air-cooled system it requires adequate airflow and an
ambient of approximately 75°F (25°C). The rear of the system, and any condensing fins
exposed in the sides of the unit, should have at least six inches of clearance from any
obstructions. If the airflow is obstructed, or the ambient is not +/- 5°F (+/-3°C) the system will
not meet specifications. The system should be relocated to a more suitable location or
additional room ventilation should be provided.
Ambient Air Requirements
Electrical Requirements
There will be one power line cord running from the rear of the Dura-Dry II MP. The serial tag at
the rear of each system has the voltage requirements for that system. The voltage tolerance for
this system is +/-5%. These tolerances are necessary because of the lower temperature
specifications of these units. Check the voltage requirements as stated on your serial tag
against your power supply.
All Dura-Dry II MP units are shipped with NEMA 6-30P plugs (except units sold overseas; no
plug). We recommend a 30A supply with a NEMA 6-30R outlet. The plug with ground needs to
be connected to a grounded outlet at the supply. The maximum current draw (utilizing the
largest standard pump) is 16A/60Hz or 21A/50Hz. Avoid the use of extension cords
whenever possible. If an extension cord is required, it should be of sufficient size to supply 30
amps without heating
55°F to 69°F (12°C to
21°C) Acceptable
70°F to 75°F (21°C to
24°C) Ideal
75°F to 80°F (24°C to
27°C).
Acceptable, but a reduction in the cooling capacity of the
unit is to be expected (about a 1% cooling capacity
reduction per degree above 72°F).
80°F to 85°F (27°C to
29.5°C) Expect reduced reliability. Warranty may be voided.
Over 85°F (Over
29.5°C) Not Acceptable. Warranty will be voided.
NOTE: These systems will not work properly on voltage other
than that ordered and specified. If incorrect voltage has been
ordered, contact the FTS Service Department and they will
recommend the a
pp
ro
p
riate transformer