Phenom ProX User manual

Phenom User Manual
ProX / Pro / Pure
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3
Things you must know
1. Introduction
2. System overview
3. Installing the
Phenom
4. Using the Phenom
CONTENTS
Things you must know 6
Introduction 8
1.1 Unpacking the Phenom components 8
1.2 Packaging contents 9
System overview 10
Controls 10
Connections 12
Screens 13
Installing the Phenom 18
Preparation 18
3.1 Requirements for positioning the Phenom components 18
3.2 Assembling the flat panel touch screen monitor 18
Connections 19
3.3 Connecting the Phenom 19
3.4 Activating the system 21
3.4.1 Switching on the Phenom 21
3.4.2 Switching ‘on’ the flat panel touch screen monitor 21
3.4.3 Calibrating the flat panel touch screen monitor 21
Using the Phenom 22
Preparation 22
4.1 Waking-up the Phenom 22
4.2 Preparing samples 22
4.2.1 Samples that cannot be prepared in colloidal graphite or silver paint 23
4.2.2 Particle samples 23
4.2.3 Polymers 24
4.2.4 Metals 24
4.2.5 Biological samples 24
4.2.6 Heavy metal coating 25
4.3 Loading samples 25
4.3.1 Activating the sample holder 26
Operation 26
4.4 Using the touch screen 27
4.5 Optical imaging 27
4.5.1 Adjusting focus 27
4.5.2 Adjusting brightness and contrast 27
4.5.3 Adjusting magnification (ProX / Pro) 28
4.5.4 Moving the sample 28
4.5.5 Sample overview 28
4.5.6 Storing images 28
4.6 lectron imaging 30
4.6.1 Adjusting focus 30
4.6.2 Adjusting brightness and contrast 31
4.6.3 Magnifying the image 31
4.6.4 Rotating the image 31
4.6.5 Moving the sample 32
4.6.6 Storing images 32
4.7 Viewing stored images 33
4.7.1 Comparing images (ProX / Pro) 34
4.7.2 Deleting stored images 34
4.8 Measuring on stored images (ProX / Pro) 35
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4
4.9 Unloading the sample 35
4.10 Switching off the Phenom electron source 36
4.10.1 Switching off the Phenom 36
4.10.2 Switching off the flat panel touch screen monitor 37
4.10.3 Switching off the system completely 37
Phenom settings 37
75.1 Live viewing settings 37
5.1.1 Mode 37
5.1.2 Resolution 37
5.1.3 Quality 38
5.1.4 Intensity 38
5.2 Acquired image settings 38
5.2.1 Detector mode 38
5.2.2 Quality 39
5.2.3 Resolution 39
5.2.4 Presets 39
5.2.5 Storing user settings 40
5.3 Date and time 40
5.3.1 Adjusting the date 40
5.3.2 Adjusting the time 40
5.4 Databar / image type / UI mode 40
5.4.1 Databar 40
5.4.2 Image type 40
5.4.3 UI mode 41
5.5 Label 41
5.6 USB stick / Mode 41
5.6.1 USB stick 41
5.6.2 Mode 41
5.7 Advanced settings 42
5.7.1 SW (software) version 42
5.7.2 Shutdown 42
5.7.3 StoreSys(tem)Info 43
5.7.4 Routine pages 43
5.7.4.1 Source Tilt 43
5.7.4.2 Stigmate 44
5.7.4.3 Network 45
5.7.4.4 Connectivity 46
Maintenance 48
Troubleshooting 49
7.1 rror recovery and reporting 53
7.1.1 Rotary knob state indicator 53
7.1.2 rror messages and warnings 53
7.2 Power down 55
7.3 Rebooting the Phenom software 55
Preparing the Phenom for transport 56
8.1 Return procedure 56
8.2 Prepare for packing 56
8.3 Disconnecting and packing 57
Technical specifications 58
5. Phenom settings
6. Maintenance
7. Troubleshooting
8.
Preparing the
Phenom for
transport
9. Technical
specifications
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5
Phenom-World and the Phenom-World logo are registered trademarks of
Phenom-World Bv. PhenomTM is a trademark of Phenom-World BV.
Other product and company names mentioned herein may be the trademarks of their
respective owners.
This user guide was produced using XPress®document publishing software, a registered
trademark of Quark Technology and the ArialTM family of typefaces. Arial is a trademark of
The Monotype Corporation registered in the U.S. Patent & Trademark Office and may be
registered in other jurisdictions.
Ralph Schiedon
Joris Dobbelsteen
Sander Stoks
Jeroen Smulders
Karl Kersten
Koen Driessen
Karel van der Mast
Addo Hammen
Willem Theuws
Rob Rood (ROOD Text productions)
Copyright ©2013 by Phenom-World BV
The information and materials contained herein are confidential and proprietary to
Phenom-World BV. They are provided for your organization’s internal use on a need to
know basis. They cannot be duplicated or disseminated for any third party without the
express consent of Phenom-World BV.
The information contained in this document has been composed with great care for quality,
reliabilty and accuracy and may be changed without notice.
Phenom-World BV will not accept liability for any consequence of use of this document.
Trademark
Acknowledgments
Production
Acknowledgments
Principal Contributors
Technical Publication
Disclaimer
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6
CAUTION!
General Safety
Important information
To avoid Fire or
Personal Injury
Things you must know
PleasereadalloftheseinstructionsbeforeyouoperatethePhenom.
Savetheseinstructionsforfuturereference.
Review the following safety precautions to avoid injury and prevent damage to the
Phenom microscope.
All safety and operating instructions must be read before the
microscope is operated, this is to avoid personal injury and prevent damage to the
Phenom.
To avoid potential hazards, use this product only as specified.
The user must not attempt to service the appliance beyond those means described in
the user's operating instructions.
All other servicing is to be performed by qualified service personnel.
Replace Fuse with identical type.
If a fuse is replaced, use the type as mentioned on the type plate.
Ground the Microscope.
The microscope is grounded through the grounding conductor of the power cord.
To avoid electrical shock the grounding conductor must be connected to earth ground.
Before using the microscope verify that the microscope is properly grounded.
Use correct power cord.
Only use the power cord specified for this product and approved for the country of
use.
Power Disconnect.
The power switch on the mains supply disconnects the microscope from the mains.
Do not block the power switch; it must be accessible to the user at all times.
Do not operate without covers.
The microscope must never be operated with the cover removed.
Do not operate the microscope with suspected failures or damaged covers.
If you suspect damage or failure of the product, do not disassemble this product.
Have it serviced by qualified and authorized service personnel. Servicing is required
when the microscope is damaged in any way, such as when the power supply cord or
the plug is damaged, liquid has been spilled in the microscope, it does not operate
normally or has been dropped.
Provide proper ventilation.
Adequate airflow must be allowed around the power supply and Phenom microscope .
Do not block the ventilation openings. Respect at least 20 cm of free space to the
sides, the front, the back and the top of the Phenom microscope. Do not put materials
in the air gap between the Phenom microscope and the table.
Do not operate in wet and damp conditions.
The required room temperature and maximum humidity as specified in the system's
technical specifications (see chapter 9, ‘Technical specifications’) must be respected
at all times.
Do not operate in an explosive atmosphere.
Make sure that there is proper room ventilation such that the environmental air cannot
contain combustible gasses.
Do not use compressed-gas canisters in the vicinity of the system.
Propellants of canisters are very often combustible.
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7
Environmental
aspects
Notes!
Equipment recycling
To reduce the use of natural resources and to avoid the release of substances that
could be harmful to the environment or human health we advise you to recycle this
product.
For information about recycling options please contact Phenom-World’s Customer
Support.
Disposal of your old product
Your product is designed and manufactured with high quality materials and
components, which can be recycled and reused.
When this crossed-out wheeled bin symbol is attached to a product it means the
product is covered by the uropean Directive 2002/96/ C.
Please act according to your local rules and do not dispose of your old products with
your normal household waste. The correct disposal of your old product will help
prevent potential negative consequences for the environment and human health.
Equipment classification
The Phenom should be used indoor in a controlled electromagnetic environment.
The Phenom electron microscope is C compliant with the following directives:
– 73/023/ C Low Voltage Directive
– 89/336/ C lectromagnetic Compatibility Directive
– 96/29/ URATOM Ionizing Radiation Directive following article 3.2 e.
Using the following standards:
N61010-1 Safety measurements for electrical equipment for measurement, control and
laboratory use.
N61326-1 lectrical equipment for measurement, control and laboratory use – MC
requirements (industrial level) and that the X-ray emission is below 1 µSv/h at 10 cm
distance from the surface
Phenom microscopes are classified as:
• Safety class 1 ( N 61010-1)
• Pollution class 2 ( N 61010-1)
• Installation (Overvoltage) category 2 ( N 61010-1)
• Plug connected
– MC lectroMagnetic Compatibility
– Licensing or registration for X-ray might be required according to local regulations.
For most of urope no licensing or registration is necessary (see 96 / 29 / uratom
directive, para. 3.2.e).
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8
Preparation
Unpacking
Caution!
1. Introduction
Congratulations on your purchase of the PhenomTM microscope. The PhenomTM is a high
resolution desktop imaging tool that combines an optical camera for never-lost navigation
and a high quality scanning electron microscope (S M) for detailed imaging to bring a
completely new approach to microscopy.
The Phenom’s innovative user interface utilizes intuitive touch screen controls which allows
users to observe superb quality images with minimal operator training.
The Phenom can handle a wide range of samples with minimal preparation.
We are sure that if used properly, the Phenom will bring you years of enjoyment.
You will want to keep this user manual handy, as it is a convenient source of information
about the Phenom.
1.1 Unpacking the Phenom components
Make sure the room where the Phenom components are to be placed is clean and dry
and that room temperature is between 15 °C and 30°C (59 °F and 86°F).
Room humidity should not exceed 80% RH.
Avoid direct sunlight, vibrations and strong magnetic fields.
Also refer to chapter 3.1 ‘Requirements for positioning the Phenom components’.
1First inspect the packaging before opening it. If the packaging is damaged or if the
locks are open, we recommend that you report this to Phenom-World’s Customer
Support:
- address: Dillenburgstraat 9
5652 AM indhoven
The Netherlands
- e-mail: [email protected]
- phone: [phone]
- fax: [phone]
- opening hours: Monday - Friday, 09:00 - 17:00 (C T, GMT +1)
It is however very likely that, despite slight damage to the packaging, the Phenom
components are still in good condition.
2Open all 4 locks and open the top cover completely.
3Remove the front panel by lifting it upwards.
4Remove all loose foam parts.
5Lower the plastic bag and remove the Phenom microscope.
Due to the weight, it is recommended that two people, one on each side, lift the
Phenom out of the box. Donot lift from the front as the door could easily be
damaged. Donot lift by the plexiglass frontcap or by the door handle.
6Confirm that all Phenom components are present. For a complete list of components,
refer to chapter 1.2 ‘Packaging contents’.
7Take the boxes out of the other compartment.
8Unpack all accessories prior to installation.
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1.2 Packaging contents
Please verify that the Phenom box contains the following items. They are provided to help
you set up and use the Phenom. If any of these items are missing or damaged, contact your
dealer immediately.
Save the packaging materials in case you need to transport the Phenom.
Phenom microscope ProX / Pro / Pure - 17"flat panel touch screen monitor (Pure)
- 19"flat panel touch screen monitor (ProX / Pro)
Flat panel touch screen Pre-vacuum pump Power supply
monitor VGA cable
Rotary knob Rotary knob Sample holder
extension cable
USB Flash drive Pre-vacuum pumphose - Power cable Europe 2 x
- Power cable US 2 x
Mouse (ProX / Pro) Phenom Starter it User manual
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Controls
Phenom microscope
Mouse
(Pro)
Rotary knob
USB Flash drive
2. System overview
1ySystem control button
- Switches the Phenom from standby or hibernate mode to operation mode.
- Switches the Phenom from operation mode to standby.
POWER
- Blinks green when the Phenom power supply is switched on and the Phenom goes
to operation mode.
- Blinks green when the Phenom switches from standby or hibernate mode to
operation mode.
- Lights up orange in standby mode.
- Blinks orange (1 second on, 3 seconds off) in hibernate mode.
- Lights up green in operation mode.
2 SAMPLE (sample indicator)
Lights up green when a sample is loaded.
3- Lights up orange when the door is locked.
- Lights up green when the door is unlocked.
4 Door
5 Sample loading bay
To insert the sample holder into the Phenom.
6 Sample holder
7 USB ports
- To insert the supplied USB Flash drive.
- To insert the mouse USB connector or the rotary knob USB connector.
8Operates the Phenom together with the touch screen and the rotary knob.
9Operates the Phenom together with the touch screen and the mouse (ProX / Pro).
10 To store images on.
10
Fig. 1
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11
Flat panel touch
screen monitor
Power supply
Pre-vacuum pump
11 USB cable
Connects the monitor to the Phenom (rear) USB port.
12 Monitor controls
y- switches the monitor on and off.
L D - lights up green when the monitor is switched on.
Displays monitor menu and selects menu items.
– and +
Navigate through and adjust monitor settings.
13 Touch screen
Operates the Phenom together with the rotary knob and the mouse (ProX / Pro).
14 0 / Iswitch
15 Connection for power cable
16 Fuse holder
Contains the fuses.
17 Connection for pre-vacuum pumphose
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12
Connections
Phenom microscope
Flat panel touch
screen monitor
1 EDX / USB port
Connects the Phenom DS ( nergy Dispersive Spectroscopy) detector to the
ProSuite eeBox PC (ProX).
2 Reset button
Reboots the Phenom software.
3 Connection for pre-vacuum pumphose
Connects the Phenom to the pre-vacuum pump.
4 Ethernet connector
Connects the Phenom to the Local Area Network.
PUSH button
Opens the ethernet connector.
5 USB port
Connects the Phenom to the monitor USB port.
6 VGA connector
Connects the Phenom to the monitor VGA connector.
7 USB ports
Connect the Phenom to the rotary knob and the mouse (ProX / Pro) and the ProSuite
for ProX.
8 Power connector (out)
Connects the Phenom to the pre-vacuum pump.
The Phenom supplies power to the pre-vacuum pump.
PUSH button
Opens the power connector.
9 Power connector (in)
Connects the Phenom to the power supply.
10 Power connector (in)
Connects the monitor to the mains outlet.
11 VGA connector
Connects the monitor to the Phenom VGA connector.
Fig. 2 Rear view: microscope (left) and monitor (right)
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Screens
Screens
selection bar
Image screen
IMAGE – selects Image screen.
ARCHIVE – selects Archive screen.
SETTINGS – selects Settings screen.
ADVANCED – selects Advanced settings screen. Refer to 5. ‘Phenom settings’.
?– when ’?’ is pressed, the Help function is enabled and a balloon with
information appears when any other button is touched. The balloon
gives information about the function of the button.
The Image screen is used to view samples, take pictures, and operate the Phenom.
1 Main viewing window
Displays magnified part of the sample.
2 Data bar
10 µm – current ruler size.
– dynamic representation of ruler size
(depending on magnification factor)
. . . . x – magnification factor.
. . . . µm – Field Of View (total picture size).
FEB 092006 12 : 15 PM – Date and time.
IMG S121206_0012 – Sample / file name.
Items to be shown can be selected on the Settings screen.
Fig. 3
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3 Electron overview window
Displays the part of the sample that is magnified in the main viewing window, with the
largest field of view (lowest magnification factor).
4 Button bar
The buttons define the functionality of the rotary knob:
- Magnifies part of the image.
- Adjusts overall contrast of the image.
- Adjusts brightness of the image.
- Adjusts focus of the image.
- Rotates the image (electron imaging mode only).
5- Takes a picture of the image in the electron overview window.
6- Refreshes the electron overview window.
7 Status window
- Gives information on the current status of the Phenom.
- Displays messages during operation, when problems occur or when action by the
user is required.
Progress bar
- Indicates the remaining time when the Phenom is performing durative actions.
- Indicates the remaining wake-up time when the Phenom is waking up from standby
and hibernate mode.
8- Takes a picture of the image in the optical overview window. Refer to ‘11. Optical
overview window’.
9- Makes a composite image overview of the entire sample area.
10 Button bar
- Transfers sample from loading position to optical imaging position and vice-
versa.
- Selects electron imaging or optical imaging .
The appropriate circle lights up green to indicate the active mode.
- Replaces when the Phenom is waking up from standby or hibernate mode
and indicates the progress of the wake-up process.
- Takes a digital picture of the image in the main viewing window.
11 Optical overview window
- Displays the part of the sample that is magnified in the main viewing window.
-
Displays composite image overview of the entire sample area.
12
Move the sample in up, down, left and right direction.
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15
Archive screen
The Archive screen is used to view, compare and delete sample images stored on the
USB Flash drive or on a Windows network share.
1 Main viewing window
Displays currently selected image
2 Data bar
3 Thumbnail gallery
Shows your pictures in thumbnail format.
4 Scroll bar
Move the slider to scroll through your images.
5 Button bar
- jects sample and allows door to be opened.
- Deletes selected image.
- Holds the selected image so it can be compared with other images.
- Activates the measuring function.
- Stores a copy of a measured image on USB Flash drive or network share,
including measurement data.
- Shows archive images stored on the USB Flash drive ( ) or network share
( ). This button is only operational when both storage locations are available
and valid network settings have been set in the Settings screen. For this refer to
4.5.5 ‘Sample overview’ and 4.6.6. ‘Storing images’.
- Digital zoom: digitally magnifies the stored image.
- Scrolls through your stored images.
Fig.4
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Settings screen
Notes!
The Settings screen allows you to adjust the various Phenom settings to suit your own
personal preferences. For this refer to 5. ‘Phenom settings’.
1 Live viewing
Adjusts and stores viewing conditions such as imaging mode, pixel resolution and
averaging speed.
2 Date and time adjustment
Adjusts date and time.
3 USB / network
Selects USB Flash drive (USB) or network share (network) to store images.
4 Data bar
Selects the items to be displayed in the data bar in the main viewing window and / or
on the saved images.
Image type
Selects file format for stored image.
5 U(ser) I(nterface) mode
Selects the desired User Interface mode. Select whether the button bar on the Image
screen will be placed on the left or on the right side of the screen.
6 Source
Displays the total time the Phenom electron source has been operational.
Only visible when Advanced is activated. Refer to 11 ‘Advanced’).
– When the Phenom electron source is replaced, the timer will start counting again from
zero. Operating hours of the previous source will not be taken into account.
– When new software is installed on the Phenom, the timer will copy the operating
hours from the previous software versions.
7 Label
nter image / file name. Refer to 5.5 ‘Label’.
Fig.5
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8 SW version
Shows current Phenom software version.
Previous
Shows previous Phenom software version.
Rollback
Returns to previous software version.
Shutdown
Prepares the Phenom for complete switch-off.
StoreSysInfo
Stores a file with the current system information on the USB Flash drive (fig. 1,10).
SW version, Previous, Rollback, Shutdown and StoreSysInfo are advanced
settings that can be accessed by touching the Advanced button (11) and entering the
log-in password. Only visible when Advanced is activated. Refer to 11 ‘Advanced’.
9 Mode
Switches the Phenom to standby or hibernate (power saving) mode.
10 USB stick
Formats USB Flash drive or delete content on USB Flash drive.
11 Sample holder
Displays the sample holder name when an activated sample holder is inserted.
No sample holder inserted lights up when:
- you start imaging without a sample holder inserted.
- the inserted sample holder needs to be activated. Refer to 4.3.1 ‘Activating the
sample holder’.
12 Advanced
Protected login modes for experienced users.
13 Acquired image
Adjusts and stores settings such as pixel resolution, picture quality and detector mode
for images to be saved.
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Preparation
Note!
CAUTION!
3. Installing the Phenom
The indications between brackets behind button and connector names refer to the items in
the overview illustrations on pages 10 - 17. E.g. (fig. 2,3) refers to item 3 in figure 2.
3.1 Requirements for positioning the Phenom
components
Place the Phenom, touch screen, pre-vacuum pump and power supply on a flat,
steady surface, out of direct sunlight and away from sources of excessive dust, dirt,
heat, water, moisture, vibration, and strong magnetic fields.
Place both the power supply and pre vacuum pump either on the floor or on the table
near to where the Phenom microscope is placed.
Make sure that the adapter 0 / Iswitch (fig. 1,14) switch is accessible at all times.
Make sure the Phenom power supply is switched off before making any connections.
Recommended table size is 120 x 75 cm (47" x 29.5") with a load rating of 100 kg
(220.5 lbs).
Allow sufficient cooling of the Phenom, power supply and pre-vacuum pump by
keeping all cooling vents clear of obstructions.
Make sure room temperature is between 15 °C and 30 °C
(59 °F and 86 °F) and that room humidity does not exceed 80% RH.
Position the touch screen in such a way that you avoid glare or reflections from
overhead lighting or outside sources of light.
Keep the screen clean and set brightness and contrast to a level that enables you to
see the screen clearly. For cleaning the screen, refer to 6. ‘Maintenance’ and for
setting brightness and contrast, use the and – / +buttons (fig. 1, 12) on the
monitor.
When positioning the Phenom always work with two persons, one at each end.
3.2 Assembling the flat panel touch screen
monitor
Place the monitor foot onto the desktop stand.
Position the monitor above the foot and align the connectors. Gently press until the
foot clicks into position.
18
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Connections
Note!
14
14
3.3 Connecting the Phenom
The figures between parentheses refer to the corresponding figures in the illustration.
1Connect the pre-vacuum pumphose (1) between the pump inlet and the Phenom
pre-vacuum pump connector.
Place the nut at one end of the hose onto the pump inlet screw thread and the nut
at the other end of the hose onto the pump connector screw thread.
Turn both nuts clockwise until they are finger tight.
Use a 13 mm (0.51") spanner (wrench) to tighten the nut at the pump side.
It takes 1 to 1.5 full turn to properly tighten the nut.
Tighten the nut at the other end of the hose, using a 14 mm (0.51") spanner
(wrench).
2Connect the pump power cable (2) to the Phenom pump output connector.
> The Phenom will now provide power to the pre-vacuum pump.
To remove the pump power cable, first press the PUSH button to open the power
connector.
3Connect the monitor VGA cable (3) between the monitor
VGA connector and the Phenom VGA connector.
15
14
19
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20
Note!
4Connect the monitor USB cable (4) to the USB port at the rear of the Phenom.
5Connect the power cable (5) of the power supply to the Phenom power connector.
6Connect the power cable (6) of the power supply to a wall outlet.
7Connect the monitor power cable (7) to a wall outlet.
8Connect the USB connector of the rotary knob (8) to one of the twin USB ports at the
rear of the Phenom. If necessary, use the rotary knob extension cable.
9Connect the USB connector of the mouse (9 - ProX / Pro) to the other twin USB port.
10 Connect the USB Flash drive (10) to one of the USB ports at the Phenom front.
11 Optionally you can connect an ethernet cable (not supplied) between the Phenom
thernet connector and your router / gateway or cable modem.
If the Phenom is connected to the Internet, the technical performance of the Phenom
will be monitored by Phenom-World’s Customer Support.
This increases the predictability of maintenance requirements and ensures greater
uptime (the time the Phenom is ‘up’ and running) for your Phenom.
Connect an ethernet cable (11) between the Phenom thernet connector and
your router / gateway or cable modem.
> The Phenom will now try to acquire an IP (Internet Protocol) address via DHCP
(Dynamic Host Configuration Protocol).
To remove the ethernet cable, first press the PUSH button (12) to open the
thernet connector.
To activate this function, refer to chapter 5.7.4 ‘Routine Pages - Remote
Assistant’.
Sometimes assignment of IP addresses is MAC address based. A Media Access Control
(MAC) address is a unique identifier, attached to most network adapters. It is a number that
acts like a name for a particular network adapter.
Some companies assign IP addresses to known MAC addresses only, in order to avoid any
non-company computer accessing the network or infecting the network with viruses.
When a MAC address is required, please contact Phenom-World’s Customer Support:
- address: Dillenburgstraat 9
5652 AM indhoven
The Netherlands
- e-mail: [email protected]
- phone: [phone]
- fax: [phone]
- opening hours: Monday - Friday, 09:00 - 17:00 (C T)
PW_Phenom_Pro_X_Pro_Pure_Print:PW_Phenom_G2_Pro_G2_Pure 19-11-13 20:54 Pagina 20