Plasmatic Systems PLASMA-PREEN I User manual

Plasmatic Systems, Inc.
1327 Aaron Road
North Brunswick, NJ 08902
TEL: [phone]
FAX: [phone]
Web site: www.plasmapreen.com
E Mail: [e-mail]
USER MANUAL FOR PLASMA-PREEN SYSTEM
GE-JEM25BF-

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TABLE OF CONTENTS
I.
INTRODUCTION
3
II.
PLASMA-PREEN FEATURES
3
III.
SYSTEM SETUP: WATER COOLED REACTOR
4
IV.
PLASMA-PREEN CONTROLLER FRONT PANEL CONTROLES
6
V.
SYSTEM SETUP BARREL REACTOR
7
VI.
SAFETY INFORMATION
7
VII.
AVOIDING EXPOSURE TO EXCESSIVE MICROWAVE ENERGY
9
VIII.
GROUNDING INSTRUCTIONS
9
IX.
CARING FOR YOUR PLASMA-PREEN SYSTEM
10
X.
TROUBLE SHOOTING
11
XI.
PLASMA-PREEN APPLICATION GUIDE
12
XII.
PLASMA-PREEN SPECIFICATIONS
13
XIII.
SUGGESTED MAINTENANCE
13
XIV.
PLASMA-PREEN CONTROLS
14
XV.
PLASMA-PREEN CONTROL PANEL
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XVI.
FUNCTION AND USE OF THE ION TRAP
17
XVII.
DIRECTIONS AND USE OF THE WATER RECIRCULATING SYSTEM
17
XVIII.
WATER TEMPERATURE MEASUREMENT
18
XIX.
THE OPERATING PROCEDURE FOR PLASMA-PREEN SYSTEMS WITH THE
CONTROL PANEL:
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I. INTRODUCTION
1. You are now the proud owner of a PLASMA-PREEN system. The PLASMA-PREEN is a
plasma etching system capable of performing many functions in the plant or laboratory.
See applications guide in Section X.
2. The PLASMA-PREEN system is manufactured from a microprocessor controlled
microwave oven and uses the relevant digital control functions incorporated in the
microwave oven. The PLASMA-PREEN system also has an additional analog power
control feature added to provide a wider control range of plasma power.
3. The PLASMA-PREEN system operates by flowing a process gas (usually oxygen or argon)
at reduced pressure (from 1 to 5 torr) through the process chamber and exciting the plasma
discharge with the microwave energy from the microwave oven. This process produces
ionized gas species and free radicals within the gas. These active species sputter and/or
react with the work within the chamber. Since this process occurs in the gas phase at
reduced pressure, little material is consumed or discharged. Reactions occur at the work
surface (gas solid interface) and are subject to the geometrical constraints this arrangement
introduces. For example, if two flat parts are bonded together the area attacked is the
narrow bond line exposed to the plasma.
4. Much of the plasma power eventually is dissipated as heat. For processing heat sensitive
components it becomes necessary to limit the average plasma power or to heatsink the
work. Plasmatic Systems has therefore developed a water cooled unit for this purpose.
5. We feel confident that you will discover many applications for the PLASMA-PREEN
system in your work that you may not have considered before.
II. PLASMA-PREEN FEATURES
Reasonably Priced
Reduces Effluents
High Power to 700 Watts
Safety Designed
Electronic Digital Controls
Ease of Use
Duty Cycle Control
Simplicity of
Analog Power Control
Maintenance
Process Memory
Reliability of
Water-Cooled Base Plate
Performance
2.45 GHz Operation
Optional 50Hz 220V Power
Available

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III. SYSTEM SETUP: WATER COOLED REACTOR
1. Remove the bell jar and its contents from the inside of the PLASMA-PREEN unit. The
PLASMA-PREEN is shipped with the vacuum tube (3/8" O.D. tube) and water tubes (1/4"
O.D. copper tubes with brass fittings) disconnected. Reconnect the vacuum tube and water
tubes to the appropriate fittings in the rear of the unit. If the unit was ordered without the
PLASMA-PREEN gas control panel, reconnect the flowmeter assembly to the gas inlet
(The silver colored fitting on the lower right side when facing the rear of the water cooled
unit). Screw in the flowmeter brackets into the holes provided in the upper right side of the
unit. Use one wrench inside the unit (5/8" for the brass water lines and 3/4" for the silver-
colored vacuum line) and one outside the unit (9/16" for the brass water lines and 11/16"
for the vacuum line) to tighten the fittings. Mount the bell jar, open side down, on the
gasket and on top of the base plate.
2. Place the unit in any location, but be sure to leave at least one inch of clearance at the top
and three inches on each side to assure proper ventilation and access to the controls.
3. Connect the PLASMA-PREEN System to a vacuum pump with a capacity of at least 3.0
CFM (85 l/m), capable of pumping down to 50 microns.
4. ALCATEL MODEL VACUUM PUMP SET UP
1. Remove the pump from the box.
2. Remove the plastic cap from the exhaust port (The port to the upper right of the
sight glass near the front of the pump).
5. Locate the blue exhaust mist eliminator and screw it into the exhaust port until snug. DO
NOT OVER TIGHTEN!!
1. Locate the long vacuum hose inlet fitting assembly. Insert the "O"-ring and retainer
between the inlet fitting on the end of the hose and the vacuum pump inlet port
(Located to rear left top of the pump near the motor) using the clamp provided.
Make certain the "O"- Ring is still wet with non-combustible pump oil to insure a
proper vacuum seal. NOTE: The other end of the long vacuum hose is connected to
the PLASMA-PREEN control unit.
2. Fill the pump with 2.0 to 4lbs (0.9 to 1.8Kilo-grams) of KRYTOX 1525 supplied.
Check the oil level in the pump. It should be somewhere between the "Min." and
"Max." levels that are indicated at the side of the oil sight glass.
3. The pump is ready for use.
4. NOTE: Use only KRYTOX 1525 non-combustible vacuum pump oil.
6. For PLASMA-PREEN units purchased without a PLASMA-PREEN controller. Connect
the process gas line to the bottom fitting on the flowmeter. If a gas manifold was

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purchased from Plasmatic Systems then connect a process gas to each of the manifold inlet
fittings being used. Set the regulators at 10 PSI.
7. If a PLASMA-PREEN controller was purchased from Plasmatic Systems, Inc. See Figure
2.
1. Connect one end of the short piece of vacuum tubing to the controller fitting
marked "TO PLASMA-PREEN" on rear of the control unit and the other end of the
tubing to the large left fitting (facing the front of the unit near the brass water lines)
of the PLASMA-PREEN water cooled units or the bottom filling of the barrel unit.
2. The longer piece of vacuum hose connects the vacuum pump to the PLASMA-
PREEN controller at the fitting marked "TO VACUUM PUMP".
3. The gas inlet tube is connected to the top center rear gas fitting marked "MIX GAS
OUT" and the large right fitting of the PLASMA-PREEN water cooled units or the
top fitting of the barrel unit.
4. DO NOT Plug the vacuum pump into any of the outlets in the rear of the
PLASMA-PREEN controller.
5. The process gases are connected to the rear gas fitting marked "GAS A" and "GAS
B", one on the right side and one on the left side. NOTE: the flowmeter on the right
controls the gas on the right side and the flowmeter on the left controls the gas flow
on the left. The "GAS A" flowmeter controls gas "A" and the "GAS B" flowmeter
controls gas "B".
6. The regulators on the front panel of the PLASMA-PREEN controllers should be set
for 5 PSI.
7. If one of the process gas flowmeters in not being used it should be shut off at the
needle valve.
8. Plug the domestic model into a standard 110 to 120 Volt 15 amp properly-grounded outlet.
For the export model, plug the unit into a 220 Volt 50 Hz grounded outlet.
9. NOTE: If the unit has been stored in an extremely cold area, wait a few hours before
plugging it in.
10. If the vacuum pump contains non-combustible oil DO NOT ADD ANY HYDROCARBON
OIL TO THE PUMP. USE ONLY KRYTOX 1525.
11. Connect the water lines to a water source and drain. The water inlet and outlet tubes are
interchangeable. The unit requires minimal water flow, about 0.3 Gal/min. or more.
IV. PLASMA-PREEN CONTROLLER FRONT PANEL CONTROLS

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1. The left most electrical switch turns on any accessories plugged into the rear of the
system in the UP position. DO NOT PLUG THE VACUUM PUMP INTO THIS
UNIT AS THE VACUUM PUMP REQUIRES TOO MUCH CURRENT.
2. The center switch in the UP position turns on the gas flow into the PLASMA-
PREEN unit.
3. The right switch in the UP position opens the solenoid, that is contained in the
control box, between the PLASMA-PREEN unit and the vacuum pump. The down
position opens up a solenoid that bleeds gas into the vacuum chamber and closes off
the vacuum solenoid.
4. Between the two vacuum lines in the rear of the PLASMA- PREEN controller is a
needle valve that controls the rate gas is bleed into the system. This is useful if
small parts are being cleaned preventing them from blowing around during the vent
cycle.

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V. SYSTEM SETUP BARREL REACTOR
1. Open the door to the PLASMA-PREEN unit and remove the literature inside. Locate the
inner chamber and place it inside the outer chamber within the unit. Connect the vacuum
line to the bottom connector on left side of the unit in the rear. If the vacuum pump was
purchased from Plasmatic Systems set it up as described in Section III-4 and III-8.
2. Connect the process gas line to the bottom fitting on the flowmeter. The top of the
flowmeter connection or the "MIXED GAS OUT" of the Plasma-Preen controller should
be connected to the top gas inlet connection on the left hand side (If facing front).
3. Plug the domestic unit into a standard 110 to 120 Volt 15 amp/60 Hz properly-grounded
outlet. For the export unit, plug it into a 220 Volt 50 Hz grounded outlet.
4. NOTE: If the unit has been stored in an extremely cold area, wait a few hours before
plugging it in.
5. To insure proper air flow, DO NOT remove the feet from the bottom of the unit.
VI. SAFETY INFORMATION
1. A microwave oven is one of today's safest appliances. Each microwave oven meets the
safety performance standards for emissions set by the United States Department of Health
and Human Services.
2. To reduce the risk of burns, electric shock, fire, injury to persons or exposure to excessive
microwave energy:
3. Read all instructions before using this equipment.
4. Read and follow the specific , AVOIDING POSSIBLE EXPOSURE TO EXCESSIVE
MICROWAVE ENERGY, SECTION THAT FOLLOWS THIS SECTION.
5. Install the unit to allow sufficient air circulation around the rear of the unit. Install the unit
on a stable base where it will not fall or get wet. If the unit is water cooled make certain the
water lines are tight and secure.
6. THIS UNIT MUST BE ELECTRICALLY GROUNDED. Connect it only to a properly
grounded outlet. See GROUNDING INSTRUCTIONS, Section VII.
7. DO NOT run the unit with the bell jar at atmospheric pressure or without gas flowing
through the reaction chamber (no load condition) unless using the timer feature. While
short periods of no load operation will not damage the unit, this procedure is not
recommended.
8. DO NOT operate the unit if it has a damaged cord or plug, if it is not working properly, or
if it has been damaged or dropped. Electrical shock, fire or other hazard may result.

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9. The unit should be serviced by qualified service personnel.
10. DO NOT cover or block any openings on the oven, or fire may result.
11. DO NOT use the unit outdoors, for damage to the unit or electrical shock may result.
12. DO NOT immerse the chord or plug in water, for electrical shock may result.
13. Keep the cord away from heated surfaces, or electrical shock may result.
14. See door surface cleaning instructions in "Cleaning your PLASMA-PREEN unit" Section
VIII.
15. Should materials inside the unit catch fire, keep the door closed, turn the unit off and
disconnect the power from the unit by pulling out the plug or shutting off the main power
to the unit at the fuse box or circuit- breaker.
16. DO NOT use the unit for storage. Do not leave paper products, books or other combustibles
inside the unit when it is not in use for. A fire may start if the unit is accidentally turned on.
17. DO NOT run the unit with metal parts external to the vacuum chamber.
18. CAUTION: BE CERTAIN THE VACUUM CHAMBER IS AT ATMOSPHERIC
PRESSURE BEFORE ATTEMPTING TO OPENING THE DOOR TO THE PLASMA-
PREEN UNIT.
19. The PLASMA-PREEN unit has a built in light filter which filters 90% of the light. DO
NOT look at the glowing plasma, at close range, for extended periods of time as eye strain
may result.
20. Treat the vacuum chamber as you would any large piece of glass.
21. DO NOT use incompatible gases (such as hydrogen and oxygen mixtures) in the reaction
chamber.
22. DO NOT run the water-cooled unit at full power in the CW mode for more than 15 minutes
at a time without a water flow. This will prevent over heating of the baseplate and gasket.
23. CAUTION: The glass vacuum chamber can become HOT when operating at pull power at
100% duty cycle. TAKE PROPER PRECAUTIONS WHEN HANDLING THE HOT
GLASS.
24. When using the analog power control TRY NOT TO RUN AT SETTINGS BETWEEN 80
and 99 (100 or full power is OK). This will prolong the life of the analog power control
unit.
VII. AVOIDING POSSIBLE EXPOSURE TO EXCESSIVE MICROWAVE
ENERGY.

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1. DO NOT attempt to operate the PLASMA-PREEN unit with the door open since open-door
operation can result in harmful exposure to microwave energy. It is very important not to
defeat or tamper with the safety interlocks.
2. DO NOT place any object between the unit front face and the door or allow soil, cleaner or
residue to accumulate on sealing surfaces.
3. DO NOT operate the unit if it is damaged. It is particularly important that the oven door
close properly and that there is no damage to the: (1)door (bent), (2)hinges and latches
(broken or loosened), (3)door seals and sealing surfaces (4) the fittings in the rear of the
unit (removed or loose).
4. The unit should not be adjusted or repaired by anyone except properly qualified service
personnel.
VIII. GROUNDING INSTRUCTIONS
1. The PLASMA-PREEN system must be grounded and connected to the same ground as the
vacuum pump. In the event of an electrical short circuit, grounding reduces the risk of
electrical shock by providing an escape wire for the electric current. This unit is equipped
with a chord having a grounding wire with a grounding plug. The plug must be plugged
into an outlet that is properly installed and grounded.
2. WARNING: Improper use of the grounding plug can result in a risk of electrical shock.
3. Consult a qualified electrician or serviceman if the grounding instructions are not
completely understood, or if doubts exist as to whether the unit is properly grounded.
4. If it is necessary to use an extension cord, use only a 3-wire extension cord that has a 3-
blade grounding plug, and a 3-slot receptacle that will accept the plug on the unit. The
marked rating of the extension cord should be equal to or greater than the electrical rating
of the unit.
5. CAUTION: The glass vacuum chamber can become HOT when operating at pull power at
100% duty cycle. TAKE PROPER PRECAUTIONS WHEN HANDLING THE HOT
GLASS, ESPECIALLY UNDER VACUUM. DO NOT OPEN THE DOOR WHEN
THE BELL JAR IS UNDER VACUUM. THE POSSIBILITY OF IMPLOSION
ALWAYS EXISTS WITH GLASS UNDER VACUUM ESPECIALLY IF THE
GLASS IS HOT.
6. When the run is finished, shut off the vacuum pump and vent the bell jar immediately by
turning the vent valve towards the back of the unit. If the bell jar is not vented immediately
oil may suck up from the vacuum pump and contaminate the system. PLASMA-PREEN
units shipped without the Control Panel are equipped with a vent valve. The vent valve has
a 0.013" diameter flow-constricting orifice to prevent small parts from flying around inside
the bell jar during the venting operation. The gas flow is automatically shut off when the
vent valve is in the vent position.

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7. After the system reaches atmospheric pressure (about 20 seconds) open the door and the
bell jar may be lifted.
8. Load the system with the work to be cleaned and repeat the above steps. Adjust the time,
duty cycle, analog power and thermal resistance to the heat sink based on the effects of the
plasma on the work.
IX. CARING YOUR PLASMA-PREEN SYSTEM
1. DO NOT USE abrasive cleaners, cleaning pads or steel wool, as they can scratch or dull
the unit door.
2. Clean the interior and exterior of the unit with a damp cloth. DO NOT USE SOLVENTS as
they may damage or discolor the plastic components.
3. Make certain that nothing is blocking the door and the sealing surfaces.
4. The bell jar may be removed and cleaned as you would any glass object. Soap and water
works well. Be sure to rinse thoroughly as traces of soap on the inside may cause the glass
to weaken in an oxygen plasma. Avoid solutions containing hydrofluoric acid as it may
weaken the glass.
5. The rubber gasket can also be cleaned with a damp cloth. Do not use sharp objects as they
might cut the rubber and prevent the formation of the vacuum seal. Should the unit become
contaminated, it can be cleaned by operating it empty, at full power, for 15 minutes
preferably using oxygen as the process gas.

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X. TROUBLE SHOOTING GUIDE
1. Unit stops by itself- Line voltage too low or the unit is improperly grounded.
2. Nothing happens when the numbers are pushed- Remember to press the pads firmly and to
press CLOCK before entering time setting. Press CLEAR PAD and start over.
3. Plasma appears concentrated in one corner of the bell jar- Check the vacuum connections
and the vacuum tubing for leaks. Check vacuum pump oil for contamination.
4. Vacuum pump starts noisily- Normal operation pump oil is cold and has a high viscosity.
5. Vacuum pump does not settle down or gas can be felt exiting from the pump- The vent
valve is in the vent position (for PLASMA-PREEN systems without the control panel), the
bell jar is not fitting snugly against the rubber gasket. Vent the system, readjust and try
again.
6. Work is getting too hot- Heat sink the work better in the (water cooled unit only) and/or
reduce the power or duty cycle.
7. No reaction is occurring or the reaction is very slow- Increase the work temperature by
placing a piece of glass between the work and the heatsink (water-cooled unit only) and/or
increase the analog power or duty cycle.
8. Solder on the work is sputtering or smearing- Reduce the process temperature, use the ion
trap (Section XV) and/or reduce the power.
9. The vacuum baseplate is getting hot- Check the water flow and water temperature.

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XI. PLASMA-PREEN APPLICATION GUIDE
INDUSTRY
FEATURE
BENEFIT
Electronic
Argon Plasma Cleaning
Wire Bond Pads
Without Iontrap
Pd-Ag Die Attach Pads
(Between 5 and 10 min)
Gold Plated Parts
Solder Preforms
Epoxy Bleed
Preparation for Soldering
Photoresist Removal
Oxidizable Metal Surfaces
Gold or Aluminum Wire
Removal of Some Metal Oxides
Argon Plasma Cleaning
Devices with Sensitive Chips
With Iontrap
Laser Diode Facets
(~15 to 30 min)
Ceramics with Soft Solder
PC Boards with Soft Solder
Oxygen Plasma Cleaning
Photoresist Removal
(5 min @ full power)
Bare Ceramic Substrates
Removal of Plastic Encapsulants
for Failure Mode Analysis
Glass Parts
Metal Oxide Parts
Gold Plated Parts
Silicon
Gallium Arsenide
Indium Phosphide
Preparation of Plastics for Gluing
Optical
Oxygen Plasma Cleaning
Glass, Si or GaAs Optics
(5 to 15 min)
Finger Prints
Epoxy Residues
Oil Residues
Lapping Compound Binders
Parts will Pass the "Water
Break Test" After Cleaning

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XII. PLASMA-PREEN SYSTEM SPECIFICATIONS
The PLASMA-PREEN system comes in three versions. The first is a barrel type reactor. The second is a
water cooled unit with a reaction chamber size of 8" x 6" x 2". The third is a larger water cooled unit with
a reaction chamber size of 9" x 7" x 3". System specifications of these units are described below
Barrel Reactor System
PLASMA-PREEN I
Chamber
Barrel
Diameter
4.1"
Length
6.0"
Material
Pyrex (Quartz on Special
Order)
Water Cooled Systems
PLASMA-PREEN II
Model No.
862
973
Chamber
Rectangular
Rectangular
Dimensions
8" x 6" x 2"
9" x 7" x 3"
Cooling Along
8" x 6" side
9" x 7" side
Material
Pyrex & Aluminum
Pyrex & Aluminum
External w x h x d
28" x 12" x 13"
28" x 12" x 13"
Shipping Weight
65 pounds
80 pounds
Power
Electrical
115V ac 15 Amp service
grounded or 220V ac 50Hz
Plasma
Variable 100 to 750 Watts
Frequency
2.45 Ghz
Duty Cycle
adjustment
From 10% to continuous
Flow meter Standard
(5 cu-ft./Hr. at STP)
Utilities required
Vacuum pump
Water and Drain
Gas Supply
Oxygen
Argon
XIII. SUGGESTED MAINTENANCE
1. Change the vacuum pump oil on a regular basis to remove accumulated contamination.
2. Keep the unit clean especially around the front door seal area.
3. If the bell jar becomes dirty, clean in any manner appropriate for glassware. If soap is used
thoroughly rinse to remove all traces as interaction with the plasma will weaken the glass.
4. Additional bell jars and gaskets are available from Plasmatic Systems, Telephone (732)-
297-9107 or FAX: [phone].

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XIV. PLASMA-PREEN CONTROLS
The ANALOG POWER CONTROL KNOB is located on the right hand side of the unit. It is equipped
with an indicator dial where 100 corresponds to 100% power and 0 corresponds to about 100 watts of
power. TRY TO AVOID RUNNING THE ANALOG CONTROL UNIT AT SETTING BETWEEN
80 AND 99 (100 or full power is OK). This will prolong the life of the analog control unit. See the next
page for a layout of the PLASMA-PREEN touch pad control panel.
Some of the microwave oven functions are not used in the PLASMA-PREEN system. These functions
are indicated by an asterisk (*) symbol.
1. DISPLAY. -Displays time of day, time during processing functions, power level being used,
process mode and instructions.
2. *popcorn
3. *chicken.
4. TIME COOK Energizes the Plasma-Preen system for a selected amount of time using 100% duty
cycle
5. REMINDER Can be used like an alarm clock
6. NUMBER PADS. Touch these pads to enter process time, time of day and power level.
7. EXPRESS COOK. Touch the number 1 through 6 pad for 1 to 6 minutes of processing time at
100% duty cycle. For example, touch 2 then START for 2 minutes of processing time.
8. POWER LEVEL. Touch this pad before changing to another duty cycle.
9. SOUND Touch the SOUND pad to change the intensity of the beeper.
10. TIMER Uses no microwave energy functions as a timer.
11. *beverage
12. *potato
13. *vegetable
14. *defrost auto/time
15. DELAY START. Allows you to program the Plasma-Preen system to begin operation at a preset
time of day-up to a 12-hour delay.
16. START PAUSE. After all selections are made, touch this pad to start the microwave power.
17. HELP Touch this pad and the pad that you want help about. The display will describe how to use
the selected function.CLEAR/OFF. When touched, it shuts off the microwave energy and erases
all settings except time of day. When held for 3 seconds the Lock-Out feature will be activated. To
deactivate, press and hold the CLEAR/OFF pad for 3 seconds.

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18. ADD 30 SECONDS. Press this pad to add 30 seconds of process time, to add 30 seconds to the
process time as it’s counting down or for an “instant on” for 30 seconds.
19. AM PM Sets AM or PM time of day. Also sets display scrolling speed.CLOCK. Touch this
pad to enter time of day or check time of day during processing. To set the clock, first touch
CLOCK pad and then enter time of day, then press AM or PM. For example, if the time is
1:30PM, touch number pads 1, 3 and 0 and “1:30” will appear in the display, touch “PM”.
Then touch START or CLOCK pad. To reset or change time, simply repeat above
process.PLASMA-PREEN CONTROL PANEL

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20. MICROWAVE CONTROL PANEL
Denotes functions not used in the PLASMA-PREEN system.
(also indicated by lower case letters)

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POWER LEVEL or DUTY CYCLE To reduce the duty cycle depress the POWER
LEVEL pad and one numeric pad . The duty cycle is based on a 30 second
time interval. i.e. a 50% duty cycle is 15 seconds on and 15 seconds off.
The following chart gives the percent duty cycle each Number Pad stands for:
automatic = 100%
9 =90%
4 =40%
8 = 80%
3 =30%
7 =70%
2 =20%
6 =60%
1 =10%
5 =50%
XV. FUNCTION AND USE OF THE ION TRAP
The ion trap is made from perforated aluminum sheet. Work to be processed is surrounded by the iontrap
within the vacuum chamber. This has two effects: First is the neutralization of the ionic portion of the plasma.
Second is to shield the work from residual microwave radiation by acting as a Faraday cage. The use of the ion
trap causes less damage to the work, makes for milder reaction conditions and reduces process reaction rates
by 50%. The use of the ion trap is indicated when process power and temperature reduction still cause damage
to the work.
XVI. DIRECTIONS FOR SETUP AND USE OF THE WATER RECIRCULATING
SYSTEM
1. Locate the water tank in a convenient location near the PLASMA-PREEN II system. The
location can be on the floor under the bench on which the PLASMA-PREEN is located.
2. Fill up the tank to within 1 inch of the top (2.5cm). An algaecide like that used in
swimming pools may be added to suppress the growth of algae (Use about 1 teaspoon).
3. Attach one of the water lines of the recirculating system to one of the copper tubes of the
PLASMA-PREEN system and the other water line to other copper tube of the PLASMA-
PREEN system. Fit the top to the water tank.
4. Plug in the water pump into a 115V/60Hz outlet (220V/50Hz if so equipped) and the water
recirculating system is ready for operation.

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XVII. WATER TEMPERATURE MEASUREMENT
1. Read the water temperature using the supplied thermometer. Note the setting either degrees
Farenheight of Centagrade..
2. Under no circumstances should the water temperature exceed 120 deg F. or 48 deg C. as
damage to the water pump and/or the PLASMA-PREEN gasket may result.
3. This will give about 2 hours of continuous operation with the water in the tank initially at
room temperature (70 deg F.).
4. NOTE: The water in the tank serves as the system heatsink and must be given an
opportunity to cool between runs.
5. CAUTION: Check the water level periodically and refill when the level drops 2 inches (5
cm.) below the top of the water tank.
XIX. THE OPERATING PROCEDURE FOR PLASMA-PREEN SYSTEMS WITH
THE CONTROL PANEL:
1.
Open up the vent valve and close the vacuum valve by placing the right switch in
the down position
2.
Turn on the vacuum pump.
3.
Open the process gas input line by placing the center switch in the up position.
4.
Turn on the water recirculating system by placing the left switch in the up position.
5.
Open the system and place your work on the base plate, close the bell jar so it rests
firmly on the red "O"-Ring.
6.
Shut off the vent valve and open up the vacuum valve by placing the right switch
in the up position. Allow the unit to fully pump down, make sure the pressure
gauge reads over 25 (This number may vary depending on the calibration of the
gauge, it should be the same from run to run).
7.
Adjust the flowrate of process gas to read about 2 to 3 on the flowmeter. This
adjustment should be done while the system is under vacuum. Make sure the gas
channel that is not being used is shut off completely.
8.
Turn on the microwave energy (See manual). Run for the indicated time.
9.
A good place to start is 1 minute, observe the results of the process and adjust the
time and/or power accordingly.
10.
When the run is finished and the bell jar cooled down, open the vent valve and shut
off the vacuum valve by placing the right switch in the down position. NOTE: The
rate of venting can be controlled by adjusting the manual valve located in the rear
of the control panel between the two vacuum lines.
11.
When the system is fully vented as indicated by the pressure gauge reading zero
and is no longer moving, open up the system, remove your work and the system is
now ready for the next run.

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Process gas line Solenoid
Vent Valve Solenoid
Wiring Diagramfor 115 Volt PLASMA-PREEN Controller
115 Volts In
Accessory switch
Vacuum Valve solenoid
115Volts Out

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Fig 2
VacuumfromCpanel
PLASMA-PREENControl Panel Connections
Rear View
Adjustable
Vent
Valve
Gas to PP
Pump
OFF
Control Panel Front View
PLASMA-PREENCONTROLLER
Input Gas
ON
Vacuum
Gauge
Inches
FromGas
Tank "B" "B"
Flowmeter "A"
Inlet
Pressure
"A"
"A" Gas
Regulator
Control
OFF
Accessories
ON
To Vacuum Fitting
of the Plasma-Preen Unit
Gas Control Panel
FromGas
Tank "A"
(out) (in)
IN OUT
Water
Gas In
Plasma-Preen
"A"
Plasma-PreenUnit
Inlet
Pressure
"B" Gas
Vacuum
Off
Vent
"B" Gas
Regulator
Control
Flowmeter "B"