ArC Instruments ArC ONE Control User manual

® ArC Instruments Ltd., 2017
Memristor Characterisation Platform
User Manual
rev. 1.3

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®ArC Instruments Ltd.
Contents
1. Introduction
2
2. Getting Started
3
2.1. Out of the Box
3
2.2. Software Installation and Update
5
3. Using the ArC GUI
6
3.1. At a Glance
6
3.2. Starting a New Session
8
3.3. Connecting to ArC ONE®
10
3.4. Basic Operations
11
Device Selection
11
Custom Arrays
12
Read Operation
13
Manual Write Pulsing
14
Data Display
14
Device History
15
Saving Data
15
3.5. Advanced Pulsing Modules
20
FormFinder
21
CurveTracer
22
SwitchSeeker
23
Endurance
25
Retention
25
VolatilityRead
26
STDP
27
3.6. SuperMode
28
4. Example Use Cases
29
5. Troubleshooting
30
5.1. Connection Issues
30

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®ArC Instruments Ltd.
1. Introduction
ArC Instruments®delivers high performance testing platforms for characterizing ‘en masse’ novel
technologies in a fast and automated fashion.
ArC ONE®is specifically designed for working with emerging 2-terminal nanoelectronic memory
devices. The instrument is controlled through a simple yet powerful user interface that allows
for ArC ONE®capabilities to be broadly accessible, from research students to competent test
engineers.
ArC ONE®can effortlessly be integrated into any R&D setting to accelerate discovery. It can be used
with any prober for accessing from single up to 1024 devices directly on wafer or even be used as a
stand-alone portable testing capability to enable advanced in-situ physicochemical characterisation
techniques.
And while this instrument provides unrivalled versatility in testing, it does so without compromising
on performance; delivering ns pulsing and other bespoke state-of-art capabilities that are essential for
characterising advanced memory devices.
This guide covers the installation of this apparatus and details its capabilities.

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®ArC Instruments Ltd.
2. Getting Started
2.1. Out of the box
The ArC ONE®system consists of a hardware instrumentation board (ArC ONE®) and a dedicated
software graphical user interface –GUI (ArC ONE Control®)
The hardware and adjacent components straight out of the box are illustrated below
Figure 1: Out of the box: ArC ONE® hardware instrumentation board. Mini USB cable. AC adaptor.
To power up the board, either plug in the provided AC power adaptor in the DC plug, or connect a
desktop power supply to the banana sockets. Toggle the power supply switch towards the required
power supply input. The red and green LEDs should turn on, indicating the board is powered. For best
results, utilise a battery supply.
The PLCC socket holds packaged samples. Its pin map is illustrated below in Figure 2.
In the case where devices need to be accessed away from the board, (eg via a probe card to solid-
state devices on wafer), the surrounding headers provide access to individual word- and bitline
addresses.

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®ArC Instruments Ltd.
Figure 2: PLCC68 and surrounding headers pin map

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2.2. Software Installation and Update
To install the ArC ONE®Control GUI, follow the steps below: (for Windows 7 and 8)
1. Download the source files from:
http://arc-instruments.com/files/full/ArC_ONE_Control_full.zip
2. Unzip the files to a folder of your choice. The directory should look like below.
3. Install mBED drivers:
Go to: developer.mbed.org/handbook/Windows-serial-configuration
Follow steps 1 and 2 to install the drivers.
4. You’re good to go. Double click on ArC ONE Control.exe in the ArC ONE Control folder to
start the interface. Connect your PC to the board via the USB cable and plug in the
provided DC adaptor. If you notice any anomalies, reset the mBED.
To update the ArC ONE®Control GUI suite, first start the interface, make sure the ArC ONE®board is
connected via USB and look for the Platform Manager launch button on the top left corner of the GUI.
An internet connection is required for this feature.
If the button is active, then an update is available. Click the button to start the automatic updater.
You can manually check for updates at Settings/Check for updates.
If you encounter any problems, please contact us at [email protected]

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®ArC Instruments Ltd.
3. Using the ArC ONE®Control GUI
The ArC ONE®Control GUI is distributed under the General Public License (GNU) Version 3. It is therefore
an open-source copy, allowing any user to modify and re-utilise its contents, as long as the original creator
is mentioned. Keep a copy of the initial source file to ensure the operation of the ArC®platform.
We are not responsible for any damage to the platform, or computer system utilised by this code. For
more information, please consult:
https://www.gnu.org/licenses/gpl-3.0.en.html
3.1. At a Glance
The ArC GUI allows easy control of the ArC ONE®platform. It is divided into a number of functional panels:
Toolbar: contains buttons for saving data, creating, opening and clearing a session, ArC ONE®connection
management as well as a GUI session mode indicator (refer to Section 3.3) and an ArC ONE®connection
indicator, on the right hand side. File menu contains Save, Open, Clear and Exit options. Settings menu
allows the user to modify hardware settings and choose a new working directory on the fly. Help menu
shows the documentation (this file), and ArC Instruments Ltd. contact information.
Manual Operations panel: Contains buttons for reading a single selected cell or the full array. The Custom
Array checkbox restricts the crossbar active devices to any combination of devices in a 32x32 array, based
on a text file. The read type can be changed via the drop down menu. The reading voltage can also be set
via the input text field. Clicking 'Update' updates the reading method on the ArC ONE®board. Manual
pulsing of 0 to ±12V and down to 90ns can be applied on the selected device by pressing +Pulse (positive
pulse) or -Pulse (negative pulse). Separate input fields allow for independent setting of positive and
negative pulsing polarities.
Crossbar Panel: Direct selection of individual devices is performed by left clicking the required position.
The selected crosspoint is highlighted by a thick black outline and represents the current device under
Figure 3: At a glance –functional panels of the ArC ONE® GUI

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test (DUT) for any further operation. The resistive state of each device is represented by the colour of the
cell, and the colour coding is illustrated at the right of the crossbar. Hovering over a cross-point reveals the
absolute resistance value of the last read operation. Additionally, left clicking and dragging allows
selection of a square region of devices in a crossbar if local testing is required.
Data Plot panel: Top plot shows the resistive state evolution of a device. Bottom plot shows the pulse
amplitude and pulse duration per pulse number in chronological order. During the application of an
automated pulsing script, the plot is updated live with incoming measurement data.
Device History panel: Contains the pulsing history for each device in the crossbar, if any is available. History
entries can be accessed to display additional measurement results.
Pulsing Modules panel: The drop-down menu contains a number of custom pulsing scripts, and selecting
one displays its corresponding options which the user can then set. Panels include custom device
operation scripts such as FormFinder, SwitchSeeker, standard IV measurement protocols such as
CurveTracer, and memristor specific characterisation pulsing scripts such as Endurance and Retention.
The pulsing scripts are described in detail in Section 3.5.
3.2. Starting a New Session

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On starting the GUI, the window on the right below will appear which allows setting up a new
measurement session. There are 2 main setting categories:
General Settings:
The Session Mode dropdown selects the operating
mode of the system and four options:
1. Live: Local -normal operation mode, all
outputs are applied to the on-board package
holder, and to the surrounding headers (Figure
5)
2. Live: External BNC –in this mode of operation
your device under test should be connected to
the instrument through the BNC terminals.
The board applies stimuli and reads out data
exclusively through the BNC terminals (Figure
6). In the Crossbar Panel the target device
appears as address [W=1, B=1]. WARNING:
Please ensure no package is connected in the
PLCC68 holder or through the header bank.
3. Live: BNC to Local –in this operating regime
the instrument’s biasing circuitry is disabled
and all voltage/current biasing to target
devices is provided through the BNC terminals
(Figure 7). The ArC platform only performs
routing, i.e. directs bias voltages/currents from
the BNCs to the selected device (in PLCC68
package or via header banks).
4. Offline –mode used to visualize previously
acquired measurements through the ArC
system. ArC ONE®biasing hardware disabled.
Working Directory entry allows the user to choose
the directory in which measurement sessions will
be saved. Press the browse button on the right of
the entry to navigate. This can be setup later as well.
Session Name entry sets the name of the session.
Hardware Settings:
Reading Cycles: Every test device resistive state READ measurement is by default an average of n
recorded data points. This entry sets the value of n. A higher number translates into a slower, but more
accurate measurement. n=50 is a reasonable, general purpose choice.
Sneak Path Limiting sets up the sneak path mitigation technique employed in selectorless crossbar
arrays. The user can chose between V/2, V/3.
Sneak Path Limiting Option
Biasing Nodes
V/2
V/3
Active wordline
Vwrite
Vwrite
Active bitline
GND
GND
Inactive wordline
Vwrite/2
2*Vwrite/3
Inactive bitline
Vwrite/2
Vwrite/3
Array Shape counters set up the size of the array. Any size is selectable between 1 and 32 word- and
bitlines.
Press Start to start a new session with the selected settings. Cancel to abort.
Figure 4: New session panel.

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Figure 5: Live: Local session mode board
connectivity.
Figure 6: Live: External BNC session
mode board connectivity.
Figure 7: Live: BNC to Local session
mode board connectivity.

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3.3. Connecting to ArC ONE®
After the new session has been set up, the right hand side of the toolbar should indicate the session
mode, and the connection status showing Disconnected as below.
Make sure ArC ONE®is connected to the PC via an USB cable, and the board is powered up. A blue
LED on the on-board mBED indicates the board is connected to the PC, and red and green LEDs
indicate the board is powered up.
From the toolbar (above), select the corresponding COM port of the ArC ONE®board. If you don’t
know it, you can find it in Windows by going to:
-Right click My Computer;
-Select Manage;
-On the left hand side, select Device Manager;
-Search for Ports (COM and LTP) and expand;
-Look for a device named: mbed Serial Port (COMX), and make a note of the COM port
number.
Return to the GUI and select the respective COM port from the dropdown list, and click Connect.
If the port is not there, click Refresh and wait for up to 10 seconds. The port should now appear.
Once the connection is successful, the connection status will turn green like below:
If any connection problems occur, please refer to Section 5 of this manual.

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3.4. Basic Operations
Many basic operations such as reading and writing, as well as data display and device history
visualisation are available at a click of a button. As a general rule of thumb, the buttons coloured in
orange perform invasive operations on the selected device, or range of devices. Buttons coloured in
dark blue perform non-invasive operations, such as updating ArC ONE®settings or managing data
display options.
Device Selection
Left click the required device on the Crossbar
Panel to select it. The device will be highlighted
by a black outline. Any following invasive operation
will be performed on that device.
Hovering the mouse over a crossbar device shows
address and resistance information in the small
floating information panel.
The address of the currently selected device
appears on top of the Manual Operations panel,
along with its corresponding last measured value
of resistance.
Left click and drag in order to select a range of
devices. A box with a thick red outline will indicate
the selected sub-array. Right click anywhere on
the Crossbar Panel to toggle the visibility of the
box.
Figure 8: Manual Operations Panel.
Figure 9: Crossbar Panel showing device range selection.

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Custom Arrays
If only a particular set of crosspoints is required for a measurement session, these can be selected on
the interface via checking the Custom Array checkbox. A file open dialogue will appear which allows
the user to select a text file containing the required addresses, formatted in the following way:
Wordline, Bitline
The same open file dialogue will appear if the browse array file button is pressed.
The set of device addresses are then highlighted in the Crossbar Panel, while the others are hidden.
Any device select, or device operation will be constrained to this set.
The devices within the range selected by left clicking and dragging will constitute the target area for
any operations carried out via the Apply to Range directive.
1, 1
2, 31
3, 3
4, 29
5, 5
6, 27
7, 7
8, 25
9, 9
10, 23
11, 11
12, 21
13, 13
14, 19
15, 15
16, 17
17, 16
18, 18
Figure 10: Custom
array file format
example.
Figure 11: Manual Operations panel –
custom array controls.
Figure 12: Example of a custom array.

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Read Operation
In the Read Operations sub-panel, click Read Single to perform one READ operation on the selected
device (highlighted in the Crossbar Panel, and listed on top of the Manual Operations panel). The new
value of resistance is updated there.
The Data Plot panel will be updated with the new measurement.
Click Read All to read all devices in the crossbar.
Update Read updates the reading method on the ArC board. Select the reading method between:
1. Classic: reads at 0.5V, suitable for linear resistors, fast;
2. TIA: reads at a programmable voltage;
3. TIA4P: RECOMMENDED - Kelvin sensing at a programmable voltage;
Select the reading voltage by left-clicking the up and down arrows in the reading voltage counter, or
introducing a float number by hand.
Remember to click Update Read every time the reading method, or reading voltage is changed.
Figure 13: Manual Operations panel.
Figure 14: ReadClassic schematic illustration.

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Manual Write Pulsing
In the Manual Pulsing sub-panel, single WRITE pulses can be applied on a selected device.
Click the +Pulse to immediately apply a positive voltage pulse, and –Pulse to apply a negative pulse.
The parameters of the pulse, such as amplitude and duration, can be changed via the entry fields
above the corresponding buttons.
A READ operation is automatically performed after each manual pulse. The new measurement is
added in the Data Plot panel, along with the applied manual pulse.
Checking the Lock checkbox disables the negative pulse parameter entry fields. Clicking –Pulse will
then apply a negative pulse with the parameters of the positive pulse entry fields.
For example: positive pulse parameters are 1V 100ms, negative pulse parameters are 2V 1ms. Clicking
+Pulse will apply 1V 100ms, -Pulse will apply 2V 1ms. After checking the Lock checkbox, clicking +Pulse
will apply 1V 100ms, and –Pulse will apply -1V 100ms.
Data Display
In the Display Options sub-panel, the user can modify the plot options in the Data Plot panel.
Press Full to display all recorded data points for the selected device.
Press Range to display the last X number of points, where X is set in the adjacent counter.
Tick the log Y checkbox to set logarithmic Y axis in the top subplot of the Data Plot panel.
Understanding the Data Plot panel.
Top subplot shows read value of resistance at each pulse number.
Bottom subplot shows:
-Blue horizontal line marker shows the voltage at which the respective resistance data point
was measured at.
-Blue square marker shows a WRITE voltage pulse amplitude
-Green ‘+’ marker shows the pulse width of a WRITE voltage pulse, shown on the right hand
side Y axis.
A WRITE pulse followed by a READ pulse are displayed in the same pulse number on the x-axis: a blue
square marker showing the WRITE pulse amplitude, and a blue horizontal line showing the read
voltage of the consecutive READ pulse. The resulting value of resistance measured during the
respective READ pulse is shown in the corresponding pulse number data point in the top subplot.
Figure 14: TIA-based read schematic illustration.
Figure 16: Example of a data plot showing evolution of resistance during an arbitrary manual pulsing session.
Figure 15: Example Data Plot

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For example, in Figure 16 at pulse #1, the resistance is read at 0.5V as ~9kΩ. Next, a 2V, 100µs voltage
pulse is applied shown at pulse#2. The resistance is then automatically read as 15kΩ, also at 0.5V,
indicated by the blue horizontal line marker at the same pulse #2. Therefore, a 2V, 100µs voltage pulse
has changed the resistance of the device as read at 0.5V, from 9kΩ to 15kΩ.
Right click on the Data Plot panel for extra display options such as setting custom x and y-axis range,
or exporting the figure image files.
Device History
All invasive device operations are logged in the
Device History panel.
Device addresses are added from top to bottom in
a chronological order following any operation.
The last device address where an operation was
performed is underlined.
Selecting a device address from the Device History
panel will also select and display its pulsing history
in the Data Plot panel.
Single device operations are listed below its
corresponding address from top to bottom in a
chronological order.
These become visible by clicking the dropdown
marker.
READ operations are tagged with Read x N, where
N is the number of read pulses applied in
sequence.
WRITE operations are tagged with Pulse x N,
where N is the number of manual WRITE pulses
applied in sequence.
Advanced pulsing algorithms are tagged with their
corresponding name.
Double clicking some advanced pulsing algorithm
entries displays further measurement results.
For example, following a CurveTracer
measurement, double clicking the ‘CurveTracer’
history entry will display the resulting IV curve. See
Section 3.5 for more information.
Saving Data
All raw data is saved in standard .csv files by clicking the save button in the toolbar. Every READ or
WRITE operation is represented as a line entry in this file, following the format below:
Wordline, Bitline: target device address.
Resistance: Last read resistance of the target device.
Amplitude: WRITE pulse amplitude for WRITE operation, READ pulse amplitude for READ operation.
CAUTION: In the case of a WRITE operation, the READ pulse amplitude is not stored!
PulseWidth: Pulse duration. CAUTION: Marked as ‘0’ for READ operations!
Tag: Descriptive tag providing extra information regarding the respective data point.
ReadTag: RX: X represents the read type employed for the READ operation during the respective
point measurement.
ReadVoltage: represents the reading voltage employed for the READ operation during the respective
measurement point.
Wordline, Bitline, Resistance, Amplitude, PulseWidth, Tag, ReadTag, ReadVoltage
Figure 17: Device history panel
example.

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Tag
Description
Observation
F R X V= Vread
A read operation recorded
following Read All.
X represents the read type
employed:
0. Classic
1. TIA
2. TIA4P
Vread represents the reading
voltage (in V).
Data point is not recorded in
the Device History panel.
Vread is also recorded in the
Amplitude column.
PulseWidth is recorded as 0.
S R X V= Vread
A read operation recorded
following Read Single. All
other indicators identical to
above.
Data point is displayed in
Device History panel.
PulseWidth is recorded as 0.
P
Pulse applied through the
+Pulse or –Pulse directives in
the Manual Operations panel
of the interface.
The ‘Resistance’ field contains
the resistance of the target
device as read immediately
after the application of the
pulse. Compare to the value
read before the pulse to
quantify the change in
resistance elicited by this pulse.
CT_s
Start point of a CurveTracer
measurement.
Resistance represents the
resistance of the device read at
Vread=Amplitude.
PulseWidth is recorded as 0.
CT_i_ x
Intermediate data points
during a CurveTracer
measurement.
x represents the cycle number.
Same as above.
CT_e
End point of a CurveTracer
measurement.
Same as above
FF_s
Start of a FormFinder
measurement.
The ‘Resistance’ field contains
the resistance of the target
device as read immediately
after the application of the
pulse. Compare to the value
read before the pulse to
quantify the change in
resistance elicited by this pulse.
FF_i
Intermediate point of a
FormFinder measurement
Same as above
FF_e
End point of a FormFinder
measurement.
Same as above
SS_s
Start of a SwitchSeeker
measurement
The ‘Resistance’ field contains
the resistance of the target
device as read immediately
after the application of the
pulse. Compare to the value
read before the pulse to
quantify the change in
resistance elicited by this pulse.
SS_i
Intermediate point of a
SwitchSeeker measurement
Same as above
SS_e
End point of a SwitchSeeker
measurement
Same as above
RET_s
Start of a Retention
measurement.
READ voltage shown in
‘Amplitude’ field.

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RET_ x
Intermediate point of a
Retention measurement.
x indicates the time point in
seconds of each
measurement.
Same as above
RET_e
End of a Retention
measurement
Same as above
EN_s
Start of Endurance
measurement
WRITE voltage pulse
parameters saved in
‘Amplitude’ and ‘PulseWidth’
fields. ‘Resistance’ field contains
the resistance of the target
device as read immediately
after the application of the
pulse.
EN_i
Intermadiate point of
Endurance measurement
Same as above
EN_e
End point of Endurance
measurement
Same as above
Example Measurement
The example plot coincides with the raw data listed below, from one device at address W=15, B=15.
Pulse #
Wordline
Bitline
Resistance
Amplitude
(V)
(s)
Tag
ReadTag
Vread
0
15
15
3710.626
0.5
0
S R2 V=0.5
R2
0.5
1
15
15
3709.371
0.5
0
S R2 V=0.5
R2
0.5
2
15
15
3711.8
0.5
0
S R2 V=0.5
R2
0.5
3
15
15
3711.342
0.5
0
S R2 V=0.5
R2
0.5
4
15
15
3712.748
0.5
0
S R2 V=0.5
R2
0.5
5
15
15
5387.196
0.095865
0
CT_s
R2
0.095865
6
15
15
5132.203
0.197452
0
CT_i_1
R2
0.197452
7
15
15
4678.331
0.298781
0
CT_i_1
R2
0.298781
8
15
15
4168.121
0.399095
0
CT_i_1
R2
0.399095
9
15
15
3710.786
0.498812
0
CT_i_1
R2
0.498812
10
15
15
3329.797
0.601575
0
CT_i_1
R2
0.601575
11
15
15
3015.44
0.706225
0
CT_i_1
R2
0.706225
12
15
15
2788.292
0.810664
0
CT_i_1
R2
0.810664
13
15
15
2623.501
0.912557
0
CT_i_1
R2
0.912557
14
15
15
2490.076
1.014837
0
CT_i_1
R2
1.014837
Figure 178: Example measurement raw data display in the Data Plot.

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15
15
15
2621.308
0.912573
0
CT_i_1
R2
0.912573
16
15
15
2789.779
0.810455
0
CT_i_1
R2
0.810455
17
15
15
3020.242
0.706225
0
CT_i_1
R2
0.706225
18
15
15
3331.286
0.601511
0
CT_i_1
R2
0.601511
19
15
15
3720.155
0.498795
0
CT_i_1
R2
0.498795
20
15
15
4177.835
0.398998
0
CT_i_1
R2
0.398998
21
15
15
4687.421
0.298636
0
CT_i_1
R2
0.298636
22
15
15
5160.943
0.197452
0
CT_i_1
R2
0.197452
23
15
15
5411.013
0.095865
0
CT_i_1
R2
0.095865
24
15
15
5234.892
-0.09978
0
CT_i_1
R2
-0.09978
25
15
15
4851.898
-0.20206
0
CT_i_1
R2
-0.20206
26
15
15
4356.187
-0.30347
0
CT_i_1
R2
-0.30347
27
15
15
3871.069
-0.40329
0
CT_i_1
R2
-0.40329
28
15
15
3491.388
-0.5044
0
CT_i_1
R2
-0.5044
29
15
15
3146.329
-0.60612
0
CT_i_1
R2
-0.60612
30
15
15
2899.183
-0.70682
0
CT_i_1
R2
-0.70682
31
15
15
2710.133
-0.8068
0
CT_i_1
R2
-0.8068
32
15
15
2563.161
-0.90872
0
CT_i_1
R2
-0.90872
33
15
15
2415.091
-1.01092
0
CT_i_1
R2
-1.01092
34
15
15
2515.301
-0.9085
0
CT_i_1
R2
-0.9085
35
15
15
2652.484
-0.80683
0
CT_i_1
R2
-0.80683
36
15
15
2830.457
-0.70664
0
CT_i_1
R2
-0.70664
37
15
15
3060.042
-0.60627
0
CT_i_1
R2
-0.60627
38
15
15
3369.232
-0.50439
0
CT_i_1
R2
-0.50439
39
15
15
3738.675
-0.40321
0
CT_i_1
R2
-0.40321
40
15
15
4194.151
-0.3035
0
CT_i_1
R2
-0.3035
41
15
15
4640.74
-0.20174
0
CT_i_1
R2
-0.20174
42
15
15
4973.099
-0.09959
0
CT_e
R2
-0.09959
43
15
15
3578.096
0.5
0
S R2 V=0.5
R2
0.5
44
15
15
3580.594
0.5
0
S R2 V=0.5
R2
0.5
45
15
15
2714.075
0.8
0
S R2 V=0.8
R2
0.8
46
15
15
2715.643
0.8
0
S R2 V=0.8
R2
0.8
47
15
15
2715.713
0.8
0
S R2 V=0.8
R2
0.8
48
15
15
4449.561
0.3
0
S R2 V=0.3
R2
0.3
49
15
15
4454.619
0.3
0
S R2 V=0.3
R2
0.3
50
15
15
4454.496
0.3
0
S R2 V=0.3
R2
0.3
51
15
15
4453.649
0
0
FF_s
R2
0.3
52
15
15
4455.347
-0.25
0.0001
FF_i
R2
0.3
53
15
15
4450.094
-0.5
0.0001
FF_i
R2
0.3
54
15
15
4448.665
-0.75
0.0001
FF_i
R2
0.3
55
15
15
4437.407
-1
0.0001
FF_i
R2
0.3
56
15
15
4420.111
-1.25
0.0001
FF_i
R2
0.3
57
15
15
4171.116
-1.5
0.0001
FF_i
R2
0.3
58
15
15
3355.073
-1.75
0.0001
FF_i
R2
0.3
59
15
15
2714.42
-2
0.0001
FF_e
R2
0.3
60
15
15
2717.5
0.3
0
S R2 V=0.3
R2
0.3
61
15
15
2717.707
0.3
0
S R2 V=0.3
R2
0.3
62
15
15
2717.669
0.3
0
S R2 V=0.3
R2
0.3
63
15
15
2717.591
0
0
FF_s
R2
0.3
64
15
15
2719.074
0.25
0.0001
FF_i
R2
0.3
65
15
15
2718.968
0.5
0.0001
FF_i
R2
0.3
66
15
15
2716.181
0.75
0.0001
FF_i
R2
0.3
67
15
15
2715.721
1
0.0001
FF_i
R2
0.3
68
15
15
2713.022
1.25
0.0001
FF_i
R2
0.3
69
15
15
2713.36
1.5
0.0001
FF_i
R2
0.3
70
15
15
2776.728
1.75
0.0001
FF_i
R2
0.3
71
15
15
4390.111
2
0.0001
FF_e
R2
0.3
72
15
15
4414.533
0.3
0
S R2 V=0.3
R2
0.3
73
15
15
4420.807
0.3
0
S R2 V=0.3
R2
0.3
74
15
15
4421.931
0.3
0
S R2 V=0.3
R2
0.3

19
®ArC Instruments Ltd.
75
15
15
4438.629
0.3
0
S R2 V=0.3
R2
0.3
76
15
15
4437.45
0.3
0
S R2 V=0.3
R2
0.3
77
15
15
5745
2
1.00E-04
P
R2
0.3
78
15
15
5791.744
0.3
0
S R2 V=0.3
R2
0.3
79
15
15
5794.007
0.3
0
S R2 V=0.3
R2
0.3
80
15
15
2802
-2
1.00E-04
P
R2
0.3
81
15
15
2759
-2
1.00E-04
P
R2
0.3
82
15
15
2763.08
0.3
0
S R2 V=0.3
R2
0.3
83
15
15
2761.165
0.3
0
S R2 V=0.3
R2
0.3
84
15
15
2762.447
0.3
0
S R2 V=0.3
R2
0.3
85
15
15
3999.051
2
0.0001
EN_s
R2
0.3
86
15
15
2861.266
-2
0.0001
EN_i
R2
0.3
87
15
15
3936.899
2
0.0001
EN_i
R2
0.3
88
15
15
2888.566
-2
0.0001
EN_i
R2
0.3
89
15
15
3927.748
2
0.0001
EN_i
R2
0.3
90
15
15
2935.807
-2
0.0001
EN_i
R2
0.3
91
15
15
3960.851
2
0.0001
EN_i
R2
0.3
92
15
15
3010.295
-2
0.0001
EN_i
R2
0.3
93
15
15
3975.576
2
0.0001
EN_i
R2
0.3
94
15
15
3030.883
-2
0.0001
EN_i
R2
0.3
95
15
15
4004.491
2
0.0001
EN_i
R2
0.3
96
15
15
3069.084
-2
0.0001
EN_i
R2
0.3
97
15
15
3993.906
2
0.0001
EN_i
R2
0.3
98
15
15
3098.52
-2
0.0001
EN_i
R2
0.3
99
15
15
3931.544
2
0.0001
EN_i
R2
0.3
100
15
15
3140.177
-2
0.0001
EN_i
R2
0.3
101
15
15
4010.678
2
0.0001
EN_i
R2
0.3
102
15
15
3161.425
-2
0.0001
EN_i
R2
0.3
103
15
15
4076.823
2
0.0001
EN_i
R2
0.3
104
15
15
3209.966
-2
0.0001
EN_e
R2
0.3
105
15
15
3215.763
0.3
0
S R2 V=0.3
R2
0.3
106
15
15
3215.978
0.3
0
S R2 V=0.3
R2
0.3
107
15
15
3216.013
0.3
0
S R2 V=0.3
R2
0.3
108
15
15
3215.842
0.3
0
S R2 V=0.3
R2
0.3