Extended Systems ExStik DO600 User manual

Dissolved Oxygen
DO600
II
RECALL
USERGUIDE
ExStik®DO600
DissolvedOxygenMeter
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Extech DO600-K Waterproof ExStik II Dissolved Oxygen Meter Kit

DO600-en-EU_V7.2 09/14
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Dissolved Oxygen
DO600
II
RECALL
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Membrane
Cathode
Electrode Bottom View
Introduction
CongratulationsonyourpurchaseoftheExStik®DO600dissolvedoxygen/temperaturemeter
whichsimultaneouslydisplaysdissolvedoxygenandtemperature.Unitsofmeasureare%
saturation,mg/lorppmfordissolvedoxygen,and°Cor°Ffortemperature.Advancedfeatures
includeDataHold,25pointsmemory,autopoweroff,automatictemperaturecompensation,
salinityandaltitudecompensation.Thismeterisshippedfullytestedandcalibratedand,with
properuse,willprovideyearsofreliableservice.Pleasevisitourwebsitetocheckforthe
latestversionofthisUserGuide,ProductUpdates,andCustomerSupport.
MeterDescription
FrontPanelDescription
1. Batterycompartmentcover
2. LCDDisplay
3. MODE/HOLDbutton
4. CAL/RECALLbutton
5. ON/OFFbutton
6. ElectrodeRetainingCollar
7. DissolvedOxygenSensor
8. BondedMembraneCapassembly
9. Membrane&Cathode
(Note:TheElectrodestoragecapisnotshown)
LCDDisplay
1. Bargraphdisplay
2. Measurementunits
3. Maindisplay
4. LowBatteryindicator
5. Temperaturedisplay
6. Readingholdindicator
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DO600-en-EU_V7.2 09/14
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Operation
PreparetheElectrode
Theelectrodeisshipped“dry”andrequiresfillingwiththesuppliedelectrolytesolutionbefore
use.Themembraneshouldbeinplaceanddoesnotneedreplacement.Followtheprocedureat
theendofthisguideforfillingthebondedcap.
NOTE:Makesurethattherearenoairbubblesintheelectrodebeforeuse.
PoweringtheExStik®
TheExStik®usesfour(4)CR2032LithiumIonBatteries.PresstheON/OFFbuttontoturnthe
meteronoroff.Ifthebatteriesareweak,the‘BAT’indicatorappearsontheLCD.Theauto
powerofffeatureshutstheExStik®offautomaticallyafterapproximately10minutesof
inactivity.Theautopowerofffeaturemaybetemporarilydisabledforconvenienceorfor
extendedpolarizationtime.
StartupPolarizationPeriod
WhentheExStik®ispoweredupforthefirsttime,theelectroderequirespolarization.Inorder
forthistooccurathreeminute(approx.)polarizationperiodmustelapsebeforemeasurements
canbemade.Aspecialcircuitisincludedinthismeterwhich,uponturn‐on,maintainsavery
smallbiasingcurrenttotheelectrodeforaperiodofsevendays.Thiskeepstheelectrode
polarizedandenablestheusertomakeimmediatemeasurements(withina7dayperiod)
withoutwaitingfortheelectrodetore‐polarize.EachtimetheExStik®isturnedon,the
polarizationtimerisresetandthe7daypolarizationperiodisinitiated.Asmallasteriskatthe
bottomrightcornerofthedisplayisusedtoindicatethatthepolarizationtimercircuitisactive
evenwhenthemeterisoff.IftheExStikisnotusedformorethansevenday,a3minutewaiting
periodisrequiredbeforeameasurementcanbemade.
Turn‐OnDiagnostics
1. WhenthemeteristurnedONtheLCDdisplays“SELF”and“CAL”whilethemeterrunsa
diagnosticroutine.
2. DuringthistimethemeterisrecallingtheUserCalibrationdata,performingselfdiagnostics
&initializingthecircuitry.
3. Afterthisfunctioniscomplete,themeterproceedstothenormalmeasurementmode.
4. TheDO600shouldbecalibrateddailyformeasurementaccuracy.
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Calibration
1. Calibrationshouldbeperformedonadailybasis.
2. TurnthemeterON
3. PressandholdtheMODE/HOLDbuttonuntil%isdisplayedontheLCD.
4. Ifthemeterhasnotbeenusedforseven(7)daysorlonger,allowtheelectrodetofully
polarize.Thismaytake2‐3minutes.
5. Placetheelectrodecapontotheelectrode.Thespongecontainedinthecapshouldbeonly
moistened(notsoaked)with(distilledwater)orcleantapwater.Besurethattheelectrode
membraneiscleananddryorthecalibrationwillbeincorrect.Thereneedstobeanairgap
betweenthemembraneandthesponge.Nevertouchthemembrane,asskinoilwillaffect
theelectroderesponse.
6. WaituntilthereadingstabilizesthenpressandholdtheCAL/RECALLbuttonuntilCALis
showninthelowerdisplay.Thereadingswillblink“101.7”and“SA”willappear.
7. Whenthecalibrationiscomplete“End”willappearandthenthemeterwillreturntothe
normalmeasurementmode.Turnoffthemeter.
Note:The“SA”willnotappearifthecalibrationfails.
8. Optional’zerooxygen’calibration(improvesmeasurementaccuracyforveryloworvery
highDOmeasurements):
Placetheelectrodeinazerooxygencalibrationsolution,suchas5%sodiumsulfite,waitfor
stabilityandpresstheCAL/RECALLbuttonuntilCALisshownintheinthelowerdisplay.
Stabilityinazerosolutionmaytakemanyminutes,dependingonelectrodehistory.
Note:SodiumSulfitecanbecomedepositedontheelectrodeandonthe“coined”surface
oftheelectroderetainingcollar.ThepresenceoftheSodiumSulfitewillnegativelyaffect
futureDOmeasurementsuntilsuchatimewhereALLofitisremovedfromtheelectrode.
9. OptionalElectronicZerocalibration.IftheDO600isnotmakingstablemeasurementsor
youarereplacingtheelectrodewithanewassembly,performthisZerocalibration.
Turnoffthemeter,removetheelectrodebyunscrewingtheretainingringandpulloffthe
electrode.
TurnonthemeterandwaitfortheSelfcalibrationtocomplete.
SettheModeto%.
PressandHoldtheCALbuttonuntilCALappearsonthedisplay.Whenthecalcycle
completes,thedisplayshouldread0.0%.
Turnoffthemeter.
Re‐attachtheelectrode.PerformtheelectrodecapcalibrationfromStep5.
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Measurements
1. Covertheelectrodewiththeelectrodecap.Thespongecontainedinthecapshouldbe
moistened(notsoaked)with(distilledwater)orcleantapwater.
2. PressingtheON/OFFbuttonturnsthemeterONorOFF.WhenturnedON,themeter’s
displayswitchesonandtheSelfCalibrationutilityruns(seeabove).
3. Ifthisisthefirsttimethemeterispoweredup,waitapprox.3minutesfortheprobeto
polarize(pleasedisableauto‐poweroff;Instructionsfordisablingauto‐poweroffare
providedinalatersection).Formoredetails,pleasereadtheStartupPolarizationPeriod
paragraphearlierinthismanualbeforecontinuing.
4. SelectthedesiredunitsofmeasurebypressingandholdingtheMODE/HOLDbuttonuntil
theproperunitsareshowninthedisplay.Removetheelectrodecoverandplacethe
electrodeinthesampletobemeasured.Stirtheelectrodeinthesampletoremoveany
trappedairbubblesfromthemembranesurface.Donotsubmersetheelectrodetothe
pointthatthesampleliquidreachesthemeter’selectrodecollar.
5. Allowthemetertimetosettletothefinalmeasurementvalue.
Note:Thelargerthedifferenceintemperaturebetweentheelectrodeandthesolutionthe
longeritwilltakeforthereadingtostabilize.Stabilizationtimecanvaryfromthirty(30)
secondstofive(5)minutes.
MeasurementUnits
Themetercanbesettomeasureeither%saturation,mg/l,orpartspermillion(ppm).
Tochangethemode:
1. PressandholdtheMODE/HOLDbuttonfor2secondsandthedisplaywillbegintoscroll
throughthedifferentunitsofmeasure:
%saturation;D.O.inmg/l;D.O.inppm(partspermillion)
2. Whenthedesiredunitsaredisplayed,releasetheMODE/HOLDbuttonandtheunitwill
returntonormaloperatingmode.
Note:The“HOLD”functioncannotbeonwhenchangingthemeasurementfunction.If“HOLD”
isdisplayedinthelowerleftcornerofthedisplay,brieflypresstheMODE/HOLDbuttontoturn
itoff.
TemperatureUnits(ºF/ºC)
1. WiththeunitOFF,pressandholdtheCAL/RECALLbutton.
2. WiththeCAL/RECALLbuttondepressed,momentarilypresstheON/OFFbuttontoturnthe
unitON.
3. TheCAL/RECALLbuttoncanbereleasedwhen‘SelfCal’isshowninthedisplay.
SalinityCompensation
1. WiththeunitON,momentarilypresstheCAL/RECALLbuttontwiceinquicksuccession
(‘SAL’isshowninthelowertemperaturedisplay).
2. MomentarypresstheMODE/HOLDbutton.EachpressoftheMODE/HOLDbuttonincreases
thecompensationby1ppt(partperthousand);theavailablerangeis0to50ppt.
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3. MomentarilypresstheCAL/RECALLbuttontosavethecompensationsettingandreturnto
thenormalmeasurementmode.
AltitudeCompensation
1. WiththeunitON,momentarilypresstheCAL/RECALLbuttontwiceinquicksuccession
(‘SAL’isshowninthelowertemperaturedisplay.
2. PressandholdCAL/RECALLagainfor2secondstoentertheAltitudeMode(‘Ald’willbe
showninthelowertemperaturedisplay).
3. Thefactorydefaultvalueissealevel.EachpressoftheMODE/HOLDbuttonincreasesthe
compensationby1000ft.Themaximumvalueis20presses(20,000ftabovesealevel).
4. MomentarilypresstheCAL/RECALLbuttontosavethecompensationsettingandreturnto
thenormalmeasurementmode.
Auto‐PowerOFFFeature
Theautopowerofffeatureautomaticallyshutsthemeteroff10minutesafterthemostrecent
buttonpress.Todisablethisfeature,refertotheDisableAuto‐PowerOFFsection.
DisableAuto‐PowerOFFFeature
WiththeunitON,momentarilypresstheCAL/RECALLbutton,thenquicklypressandholdboth
theMODE/HOLDandON/OFFbuttonsuntil‘off’isdisplayed.TorestoretheAutoPowerOff
Feature(autopowerOFFenable)simplyturnthemeteroffandonagainusingtheON/OFF
button.
LowBatteryIndication
Whenthebatteryvoltagefallsbelowtheoperatingthreshold,‘BAT’willappearonthedisplay.
RefertotheMaintenancesectionforbatteryreplacementinformation.
StoringReadings
1. PresstheMODE/HOLDbuttontostoreareading.Thestoragelocationnumberwillbe
displayedonthelowerdisplay,whilethemaindisplayshowsthestoredreading.Themeter
willentertheHOLDmodeandthe“HOLD”indicatorwillappearontheLCD.
2. PresstheMODE/HOLDbuttonagaintoexittheHOLDmodeandreturntonormal
operation.ThenexttimeMODE/HOLDismomentarilypressedanotherreadingisstored
andsoon.
3. Ifmorethan25readingsarestored,previouslystoredreadings(startingwithreading
number1)areoverwritten.
RecallingStoredReadings
1. MomentarilypresstheCAL/RECALLbuttonandthenwithin4secondsmomentarilypress
theMODE/HOLD.Thelaststoreddatapointlocationwillbedisplayed(1to25).Eachtime
theMODE/HOLDbuttonismomentarilypressedthenextmostrecentlystoreddatapoint
willbedisplayed.
2. Afterthelastdatapointstoredisdisplayed,pressingtheMODE/HOLDbuttonagainreturns
thedisplaytothebeginningofthelist.
3. PressingtheCAL/RECALLbuttonatanytimestopsthedataretrievalprocessandreturnsthe
metertothenormalmeasurementmode.
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ClearingStoredReadings
1. WiththeunitONpressandholdtheON/OFFbuttonfor4seconds
2. When“clr”isshowninthemaindisplaythememoryiscleared.
MeasurementandDisplayConsiderations
TheDO600usesapolarographicsensor,whichconsumesoxygenatthesensingsurface.
Thisrequiresaconstantmovementofthesampleacrossthemembranetomaintaina
constantdissolvedoxygenlevel.Itisrecommendedthattheprobebemovedinthesample
asthemeasurementismade,orifinalaboratoryenvironment,thesamplebestirredusing
astirplate.
IfyouaremeasuringDOinasmallcontainer,theprobewillconsumeoxygenasitis
measuringandthemeasurementvaluewillcontinuetogolower.
Iftheunitappearstobelocked(displayfrozen).ItispossiblethattheDataHoldmodehas
beeninadvertentlyaccessedbyapressoftheMODE/HOLDbutton(HOLDwillbedisplayed
inthebottomleftoftheLCD).SimplypresstheMODE/HOLDbuttonagainorturnthe
meteroffandbackonagain.
Ifthemeterdoeslatchupandnobuttonpressesreviveit,removethebatteriesandrestart.
Formaximumaccuracy,allowsufficienttimeforthetemperatureoftheprobetoreachthe
temperatureofthesamplebeforetakingareading.Thiswillbeindicatedbyastable
temperaturereadingonthedisplay.
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Maintenance
BatteryReplacement
1. Twistoffthebatterycompartmentcover.
2. Holdingthebatteryhousinginplacewithafinger,pulloutthebatterycarrierusingthetwo
smalltabs.
3. Replacethefour(4)CR2032batteriesobservingproperpolarity.
4. Replacethebatterycarrier,reattachthebatterycompartmentcapandtightensecurely.
Neverdisposeofusedbatteriesorrechargeablebatteriesinhouseholdwaste.
Asconsumers,usersarelegallyrequiredtotakeusedbatteriestoappropriate
collectionsites,theretailstorewherethebatterieswerepurchased,orwherever
batteriesaresold.
Disposal:Donotdisposeofthisinstrumentinhouseholdwaste.Theuseris
obligatedtotakeend‐of‐lifedevicestoadesignatedcollectionpointforthedisposal
ofelectricalandelectronicequipment.
OtherBatterySafetyReminders
oNeverdisposeofbatteriesinafire.Batteriesmayexplodeorleak.
oNevermixbatterytypes.Alwaysinstallnewbatteriesofthesametype.
ElectrodeReplacement
1. Toremovetheelectrode,firstturntheinstrumentOFFandthenunscrewandremovethe
electroderetainingcollar.(turnthecollarcounter‐clockwisetoremove).
2. Gentlyrocktheelectrodefromsidetoside,pullingitawayfromthemeteruntilit
disconnects.
3. Toattachanelectrode,alignthepositioning“keys”ontheelectrodeandthemainbody
housingandthencarefullypushtheelectrodeintothemetersocketuntilitisfullyseated.
4. Tightentheelectroderetainingcollarfirmlyenoughtosealtheelectrodewiththemeter.
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DOBondedMembraneCapreplacement
ImportantNote:Donottouchthemembraneasskinoilswillinterferewiththeoxygen
permeabilityrateofthemembrane.Usecautionwhenreplacingthebondedcap.
1. Itisrecommendedthattheelectroderemainattachedtothemeterduringthis
replacementprocess.
2. Toremovethebondedcapfromtheelectrode,unscrewthecapfirmlyandcarefully
counter‐clockwisefromtheelectrode(seediagrambelow).
3. Discardtheusedcap.PleaseNote:Theinstallationofabondedcapcausesthemembrane
tobetightlystrechedoverthecathode.Onceabondedcapisremovedreinstallationisnot
possibleasthemembranewillnolongerbeproperlystrechedoverthecathode.
4. RinsetheoldelectrolytesolutionfromtheCathodeandAnodebeforecontinuing.
5. UsethesuppliedPolishingPaper(SeeAccessoriestable)toclean,polish,shine,and/or
removescratchesfromthecathode.Besuretomoistentheclothbeforepolishingthe
cathode.Donotover‐polishthesensitivegoldcathode.
6. Setthenewreplacementbondedcaponaflatsurface.Leavethecapinthisposition
throughoutthereplacementprocess.
7. Fillthebondedcapwiththeelectrolytesolutionuptothebottomofthethreadsonthe
insideofthecap.
8. Tapthesideofthebondedcaptohelpjarfreeanytrappedairbubblesfromtheelectrolyte
solution.
9. Keepingthecapinafixedpositiononaflatsurface,carefullyinserttheelectrodeintothe
newbondedcapbyfirstdippingandremovingtheelectrodeseveraltimesfromthecap.
Witheachdip,pushtheelectrodeprogressivelydeeperintothebondedcap.Finally,screw
theelectrodeslowlyontothebondedcap(clockwise)untilfullytightened.Thedippingand
removaltechniqueminimizestheintroductionofairbubblesintotheelectrolytesolution.
Airbubblesintheelectrolytecancompromisemeasurements.
10. Duringthetighteningofthebondedcap,excesselectrolytesolutionwillleakout,thisis
normalanddesireablesinceitminimizestheintroductionofairpockets.Cleanoffthe
excesselectrolytebeforeuse.
Cathode
Electrode
Bonded Cap
Anode
Air Vents
BONDED CAP
Clockwise to tighten
Counter-clockwise to loosen
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Specifications
Display2000count,Dualfunction3½digitLCDwithBargraph,
Displaysize:24mmx20mm
SensorPolarographictype
MembraneBondedmembranecapwiththreadedfitting
OperatingTemp.Range0to50°C(32to122°F)
ATCRange0to50°C(32to122°F)
SalinityCompensation0to50pptin1ppt(partperthousand)increments
Altitudecompensation6000m(0to20,000ft)in300m(1000ft)increments
MeasurementStorage25tagged(numbered)datasetswithrecall
BatteryPowerFour(4)CR2032buttonbatteries
LowBatteryIndication‘BAT’appearsontheLCD
AutoPowerOffAfter10minutesofinactivity(APOoverrideavailable)
Dimensions/Weight36x173x41mm(1.4x6.8x1.6”);110g(3.8oz)
MeasurementRangeResolutionAccuracy
%Saturation0to200.0%0.1%±2.0%FS(fullscale)
DissolvedOxygen
Concentration
0to20.00mg/l0.01mg/l±2%FS
0to20.00ppm0.01ppm±2%FS
Temperature0to50°C0.1°C±1.0°C
32to122°F0.1°F(0to99ºF);
1.0°F(>100°F)
±1.8°F
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Appendices
TroubleshootingGuide
SymptomPossibleCausesAction
Unitwillnotpoweron‐Batteriesnotinplace
‐Deadbatteries
‐Batterypolarityincorrect
‐ReplaceBatteries
‐ReplaceBatteries
‐Reorient/Replace
Batteries
“BAT”indicatorshownon
display
‐Batteriesareweak ‐ReplaceBatteries
UnstableReadings ‐Insufficientelectrolytein
probe(Airbubblespresent
whenprobeisinverted.)
‐Electrolyteisdepleted
‐Replaceelectrolyte,and
membranecapassembly.
Readingsdriftdown ‐Insufficientstirring(the
probeconsumesoxygenat
themeasuringsurface,
requiringconstantsample
movementacross
membrane)
‐Moveprobeinsampleor
stirsample
SlowResponse ‐Dirtyordamaged
membrane
‐Replaceelectrolyteand
membranecap
Electrodecannotbe
calibrated
‐Depletedelectrolyte
‐Dirtyordamaged
membrane
‐Replaceelectrolyteand
membranecap
Electrodecannotbe
calibratedafterreplacing
theelectrolyteand
membranecap
‐Dirtyprobe(Cathodeisnot
ashinygoldcolor)
‐Cleancathodewith
Polishingpaper*perform
theelectronincZero
calibration
Samplereadingisfrozen‐Unitisin“HOLD”mode
‐Unitislocked
‐ReleaseHOLD
(momentarillypress
Mode/Holdbutton)
‐Removebatteries,press
ON/OFFbutton,replace
batteriesandrestart
*PolishingpaperisavailableintheDO603membranekit
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OperationalMatrixfortheModelDO600
Function/
Resulting
Action
Power
Status
Mode
Setting
RequiredButtonPressSequenceComments
On/OffAnyAnyMomentarypressoftheON/OFFbutton
WaterSaturated
AirCalibration
OnAnyPlaceElectrodeinCalibrationCap
Press&holdCAL/RECALLbuttonfor2seconds
ZeroCalibrationOnAnyPlaceElectrodeinZeroSolution,waitforstabilityPress
&holdCAL/RECALLbuttonfor2seconds
Alsoworkswithprobe
removed(Calatzerocurrent)
StoreReadingOnAnyMomentarypressoftheMODE/HOLDbuttonStoresandholdsreading
“HOLD”displayed
HoldRelease
On
WhileIn
Hold
Mode
MomentarypressoftheMODE/HOLDbutton
EnterMemory
RetrievalOnAny
MomentarypressoftheCalbuttonfollowedby
amomentarypressoftheMODE/HOLDbutton
(w/in4seconds)
Ifnodataisstoredin
memory,“End”isdisplayed
briefly,andthenreturnsto
lastmode.
ScrollStored
ReadingsOnMemory
RecallMomentarypressoftheMODE/HOLDbutton
ExitMemory
RetrievalOnMemory
RecallMomentarypressoftheCAL/RECALL
ClearStored
MemoryOn
Any
Measure‐
mentMode
PressandholdtheON/OFFbuttonfor4seconds“clr”isdisplayed.
Change
Measurement
Mode
OnAny
PressandholdtheMODE/HOLDbuttonforat
leasttwoseconds(themodeswillscrolluntil
thebuttonisreleased)
EnterSalinity
CompensationOnAnyPressandreleasetheCAL/RECALLbuttontwice
(momentary)insuccession(DisplaysSAL)
Changing
Salinity
CompensationOnSAL
MomentarypressoftheMODE/HOLDbutton
(eachbuttonpressincreasestheratioby1ppt
(partperthousand),thevaluecyclesfrom0to
50)
ExitSalinity
CompensationOnSAL
PressandreleaseCAL/RECALLbuttonfor2
secondstoenterAltitudeCompensation,Or
PressandreleaseCalButtononemoretimeto
entermeasurementmode
Itisnecessarytopressthe
CAL/RECALLbuttontosave
changes.Iftheunittimesout,
nochangesaresaved.
EnterAltitude
CompensationOnAnyor
SAL
PressCAL/RECALLtwice(momentary).Unit
entersSalinityMode.PressCAL/RECALLfor2
secondstoenterAltitudeCompensationMode.
(DisplaysAld)
Unittimesoutin5
secondsifnobuttonis
pressed,revertsto
previousmode.
Changing
Altitude
Compensation
OnAld
MomentarypressoftheMODE/HOLD
button(eachbutton‐pressincreasesaltitudeby
1,000ft,thevaluecyclesfrom0to20)
ExitAltitude
CompensationOnAldMomentarypressCAL/RECALLbuttontoexit
andsavechanges.
Itisnecessarytopressthe
CAL/RECALLbuttontosave
changes.Iftheunittimesout,
nochangesaresaved.
Change
Temperature
UnitsOffn/a(off
mode)
PressandholdtheCAL/RECALLbuttonthen
momentarilypresstheON/OFFbutton.Release
theCAL/RECALLbuttonafterthe"SELFCAL"
lights
Override
AutopowerOffOnAny
PressCAL/RECALLbutton(momentary)then
simultaneouslypressandholdtheMODE/HOLD
andON/OFFbuttonsforfor2seconds.
DefaultReset
Off
n/a(off
mode)
SimultaneouslypressON/OFF,CAL/RECALLand
MODE/HOLDmomentarily.“dFLt”willbe
displayed.
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Re‐orderandAccessoriesInformation
PartNumberDescription
DO600ExStikIIDissolvedOxygenMeter
DO600‐KExStikIIDissolvedOxygenMeterKit–containsDO600,DO603,EX050
cable,andweight,andCA895case
DO605ReplacementProbe,ExStikIIDissolvedOxygenMeter
DO603MembraneKitforDO600
Contains:6MembraneCaps,15mLKCLFillingSolution,Polishing
Paper
EX010ExtensionCable3feet(1Meter)&ProbeWeight
EX050ExtensionCable16feet(5Meter)&ProbeWeight
DO610ExStikIIDO/pH/ConductivityMeterKit
Contains:EC500pH/Conductivity/Salinity/TDSExStikIIMeter,DO600
DissolvedOxygenExStikIIMeter,SingleusepHbufferpouches4,7,
and10pH,SampleCupswithCap,WeightedBaseforSampleCups,and
Batteries,allpackedinaCarryingCase
CA895SmallSoftVinylPouchwithBeltLoopforExStikandExStikII
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