Markes International U-RACK02 User manual

QUI-1081
Version 3
August 2019
www.markes.com
Canister Rack for
CIA Advantage-xr™
Instruction for use
Product reference:
Canister rack U-RACK02

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QUI-1081
Contents
1. Introduction .............................................................3
1.1 Important safety warnings ......................................3
1.2 Dimensions and weight ............................................3
2. Components.............................................................4
2.1 Assembly kit contents ..............................................4
2.2 Required items not supplied ....................................5
3. Assembly ..................................................................5
3.1 Prepare the support legs..........................................5
3.2 Fit the support legs...................................................6
3.3 Fit the canister support bars ...................................8
4. Connecting to a CIA Advantage-xr.........................10
4.1 Standard....................................................................10
4.2 Heated sample lines.................................................12
5. Connecting to a canister ........................................13
6. Spare parts and connection kits............................15
7. Contact details ........................................................15

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1. Introduction
The canister rack for CIA Advantage-xr (part no. U-RACK02) is a space saving
support for canisters attached to the CIA Advantage-xr. It is oor mounted and holds
up to 15 canisters (1 L to 6 L): 14 samples and 1 internal standard.
This manual contains assembly instructions for the rack and advice on connecting
to the CIA Advantage-xr and canisters.
1.1 Important safety warnings
Make sure you follow the precautionary notices presented in this manual. Safety and
other special notices appear in boxes and include the following.
WARNING This is the general warning safety symbol and safety alert word to
prevent actions that could cause personal injury.
CAUTION Highlights actions that may cause product damage. We use it to
highlight information necessary to prevent damage to hardware,
software, invalid test results, or to information that is critical for optimal
system performance.
NOTES Emphasises important information about a specic task.
1.2 Dimensions and weight
Select the laboratory space before your product arrives. Pay attention to the total
height requirements and ensure the product sits <1 m from the bulkhead plate on
the CIA Advantage-xr.
Physical properties
Height 1393 mm
Width 1038 mm
Depth 670 mm

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Top view
670 mm
1393 mm
1038 mm 200 mm
Front view Side view
WARNING Due to the dimensions and weight of the rack, care must be taken to
observe proper handling procedures to prevent injury.
2. Components
Take care when unpacking the canister rack and ensure all parts are present prior
to assembly.
2.1 Assembly kit contents
■1 × ASX-5008, part built assembly
■2 × ASX-5503, short support leg (~480 mm)
■1 × ASX-5504, long support leg (~665 mm)
■4 × TOF-1248, base adjustment screw
■6 × Z-SM820CSS, hex M8 x 20 mm socket cap screw
■6 × Z-WM8PSS, M8 washer
■6 × Z-NM8FSS, M8 nut
■1 × Z-7286, M8 (6 mm) hex key
■15 × ASX-1066, canister support bar

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■30 × Z-SM512HXSS, hex M5 x 12 mm set screw
■30 × Z-WM5ETSS, M5 shakeproof washer
■30 × Z-WM5PSS, M5 washer
■15.24 × Z-0412I, inert tubing
1/6
” o.d.
■15 × Z-0040, ⅛” ×
1/16
” ferrule
■15 × Z-1132, ¼” ×
1/16
” ferrule
2.2 Required items not supplied
■An 8 mm open jaw spanner, to tighten the M5 Hex Head Screws
■A 13 mm open jaw spanner, to tighten the M8 Nuts
■A tube cutting tool/deburrer to cut tubing lengths, or heated sample lines
■Ferrules and tubing to connect the canisters to the canister rack. See section 5
for further information.
3. Assembly
3.1 Prepare the support legs
3.1.1 Required items
■2 × ASX-5503, short support leg (~480 mm)
■1 × ASX-5504, long support leg (~665 mm)
■4 × TOF-1248, base adjustment screw
3.1.2 Instruction
TOF-1248 are the adjustable feet of the canister rack, they need to be placed into
the short and long support legs as shown below. Screw in the feet until they contact
the wall of the leg.

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ASX-5503, short support leg ASX-5504, long support leg
3.2 Fit the support legs
3.2.1. Required items
■1 × ASX-5008, part built assembly
■6 × Z-SM820CSS, hex M8 x 20 mm socket cap screw
■6 × Z-WM8PSS, M8 washer
■6 × Z-NM8FSS, M8 nut
■1 × Z-7286, M8 (6 mm) hex key
■A 13 mm open jaw spanner [not supplied]

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3.2.2 Instruction
Fit the prepared support legs to the part built assembly (ASX-5008) as shown below,
using the 6 × Z-SM820CSS, 6 × Z-WM8PSS and 6 × Z-NM8FSS.
Use the nut & washer on the inside of the part built assembly and screw the socket
cap screws through the support leg, before fully securing with the M8 hex key and
13 mm open jaw spanner.
Underside of ASX-5008, with prepared support legs
NOTES The long support leg should be positioned in the middle with the two
short support legs either side. The adjustable feet should not be on the
underside of the part built assembly.

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Inside of ASX-5008
3.3 Fit the canister support bars
3.3.1. Required items
■15 × ASX-1066, canister support bar
■30 × Z-SM512HXSS, hex M5 × 12 mm set screw
■30 × Z-WM5ETSS, M5 shakeproof washer
■30 × Z-WM5PSS, M5 washer
■An 8 mm open jaw spanner [not supplied]
3.3.2. Instruction
ASX-1066 are the canister support bars on the canister rack, there are 15 of them in
total and they can be tted in two positions:
Upper – to accommodate 1 L to 3 L canisters
Lower – to accommodate 3 L to 6 L canisters

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Canister support bar positions
Upper position
Lower position
NOTES If varying size canisters are to be used, it may be advisable to t half of
the support bars in the upper position and half in the lower position.
Fit the canister support bars in place using 30 × Z-SM512HXSS, 30 × Z-WM5PSS
and 30 × Z-WM5ETSS (two of each are required for each support bar).
Use the washers and screws on the inside of the part built assembly: screw the hex
screws through the body and into the canister support bars, before fully securing
with an 8 mm open jaw spanner.

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Inside of ASX-5008
NOTES Z-WM5PSS should be positioned closest to the inside wall, then
Z-WM5ETSS and then Z-SM512HXSS.
4. Connecting to a CIA Advantage-xr
4.1 Standard
Tubing:
1/16
” o.d. × 0.040” i.d.
CIA Advantage-xr: ⅛”
sample channel unions
Canister rack:
⅛” outlets on back

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4.1.1. Required items
■15.24 × Z-0412I, inert tubing
1/6
” o.d.
■15 × Z-0040, ⅛” ×
1/16
” ferrule, required to connect the CIA Advantage-xr to the
tubing [supplied with the CIA Advantage-xr]
■15 × Z-0040, ⅛” ×
1/16
” ferrule, required to connect the canister rack to
the tubing
■Tube cutting tool [not supplied]
■Tube deburrer or metal le [not supplied]
4.1.2. Instruction
The canister rack ships with 15.24 m of
1/16
” o.d. × 0.040” i.d. inert coated stainless
steel tubing, this length is to be used as sample lines between the rack and
CIA Advantage-xr.
[1] Position the rack within 1 m of the CIA Advantage-xr
[2] Measure the distance from each bulkhead union (on the back of the rack) to
the corresponding sample channel union on the CIA Advantage-xr
[3] Cut the tubing to appropriate lengths: ensure a clean cut and deburr all ends
[4] Fit the tubing to the sample channel unions on the CIA Advantage-xr using 14 ×
Z-0040
CAUTION Only tighten the unions nger tight plus ¾ turn, any further tightening
may cause the ferrule to deform, which in turn will cause a leak or
diminished ows.
NOTES An additional ferrule and length of tubing is provided to connect the
internal standard to the bulkhead union on the back of the CIA
Advantage-xr.
Fit the tubing to the bulkhead unions on the back of the canister rack using
15 × Z-0040
[5] Markes recommends running a ow test on the sample lines to ensure the
internal bore has not become deformed during connection, and
[6] Markes recommends running a pressurised leak check using. the CIA Advantage-xr.
Additional tubing and ferrules can be purchased if required, see section 6 for
relevant part numbers.

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4.2 Heated sample lines
Heated sample lines
CIA Advantage-xr: ⅛” sample
channel unions
Canister rack:
⅛” outlets on back
4.2.1. Required items
■15 × Z-0040, ⅛” ×
1/16
” ferrule, required to connect the canister rack to the
heated sample lines
■15 × Z-0040, ⅛” ×
1/16
” ferrule, required to connect the CIA Advantage-xr to the
heated sampling lines [Supplied with the CIA Advantage-xr]
■Heated sample lines (part no. U-HTLNKT) [not supplied]
4.2.2. Instruction
The canister rack ships with 15.24 m of
1/16
” o.d. × 0.040” i.d. inert coated stainless
steel tubing, this length is typically used as sample lines between the rack and
CIA Advantage-xr, but when using heated sample lines this is not the case. In this
case the heated sample lines are used in place of the inert tubing, leaving the tubing
for connecting the rack to the canisters.
The heated sample line accessory (part no. U-HTLNKT) comprises of 16 tubing links
in groups of four with an integrated thermocouple to ensure correct heating. As
there are only 15 positions available on the rack and 14 positions on the
CIA Advantage-xr, there will be spare lines which can be used as replacements.

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To connect the rack:
CAUTION Only tighten the unions nger tight plus ¾ turn, any further tightening
may cause the ferrule to deform, which in turn will cause a leak or
diminished ows.
NOTES An additional ferrule and length of tubing is provided to connect the
internal standard to the bulkhead union on the back of the CIA
Advantage-xr.
NOTES The labels tted to each of the lines are for identication purposes only
(they match up each end) and as such can be re-positioned if necessary.
Select two groups of four lines and t seven of them to the sample channel unions
numbered 1–7 on the CIA Advantage-xr, using 7 × Z-0040. There should be one
line spare.
[1] Select two groups of four lines and t seven of them to the sample channel
unions numbered 8–14 on the CIA Advantage-xr, using 7 × Z-0040. There
should be one line spare.
[2] Fit the tubing to the bulkhead unions on the back of the canister rack using
15 × Z-0040
[3] Markes recommends running a ow test on the sample lines to ensure the
internal bore has not become deformed during connection, and
[4] Markes recommends running a pressurised leak check using the CIA
Advantage-xr.
Additional ferrules can be purchased if required, see section 6 for relevant
part numbers.
5. Connecting to a canister
5.1.1 Introduction
Prior to connecting, ensure the canister support bars are in the correct position for
the canisters being tted. Use the upper position for canisters of sizes 1 L to 3 L and
the lower position for canisters of sizes 3 L to 6 L.
CAUTION Some 1 L canisters may require additional support to the bars. Only
connect the canister once it is securely held in place.
For more information on this see section 3.3.2

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Tubing:
1/16
” o.d. × 0.040” i.d.
Restek canisters:
¼” outlets
Canister rack:
¼” inlets on front
5.5.2 Required items
■15 × Z-1132, ¼” ×
1/16
” ferrule, required to connect the canister rack to
the tubing
■15 × ferrules, required to connect the canisters to the tubing [not supplied]
■15 × short lengths of
1/16
” o.d. × 0.040” i.d. tubing, inert or stainless
[not supplied]
NOTES Markes recommends the canister rack connection kit (part no. C-CRCK)
to connect 15 × ¼” outlet canisters to the canister rack. The kit
contains all tubing and ferrules required.
NOTES If you are using heated sample lines, you can use the tubing from the
canister rack assembly kit to connect the canisters. You will need a tube
cutting tool and deburrer to cut the lengths down to size. You would still
need to purchase ferrules.
Instruction
[1] Fit the short lengths of tubing to the bulkhead unions on the front of the
canister rack using 15 × Z-1132

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NOTES Inert or stainless tubing can be used, depending on the application.
Markes recommends matching your canister to your tubing. Fit the
canisters to the tubing using appropriate ferrules, e.g. Z-1132 for
¼” outlets
Additional tubing and ferrules can be purchased if required, see section 6 for
relevant part numbers.
6. Spare parts and connection kits
Part number Description
U-FV002 Ferrule, ¼” ×¼” graphite/vespel, pk 10
U-FV003 (Z-0040) Ferrule, ⅛” ×
1/16
” graphite/vespel, pk 10
U-FV009 (Z-1132) Ferrule, ¼” ×
1/16
” graphite/vespel, pk 10
SERZ-0412 Tubing,
1/16
” o.d. ×0.040” i.d., stainless steel, 1 m length
SERZ-0412I Tubing,
1/16
” o.d. ×0.040” i.d., inert coated stainless steel,
1 m length
U-HTLNKT Heated inert sample lines for CIA Advantage HL-xr & CIA
Satellite-xr (compatible with older series)
C-CRCK
Canister rack connection kit, for connecting 15 ×¼” outlet
canisters to U-RACK02.
Contains: 2 ×U-FV009 and 10m ×Z-0412
7. Contact details
For technical support, please contact your supplier in the rst instance. If they are
unable to resolve your query, please contact Markes International’s service
department:
E: suppor[email protected]
T: +44 (0) 1443230935
W: www.markes.com

QUI-1081
L-0148 (160819-3)
CIA-Advantage-xr™is a trademark of Markes International Ltd, UK.
Vespel®is a registered trademark of E. I. du Pont de Nemours and Company, USA.
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