PAC R6000S User manual

R6000S
Operation Manual
Revision G
www.paclp.com

Copyright
Copyright © 2015 by Petroleum Analyzer Company, L.P.
All text, graphics, design, and other works contained herein are the copyrighted works of
Petroleum Analyzer Company, L.P. (PAC). All rights reserved. Any redistribution or reproduction of any
materials contained herein is strictly prohibited without the express written permission of the copyright
holder.
The PAC trademark, the PAC service mark, PAC’s logo trademark, the Antek trademark, and Petroleum
Analyzer Company, L.P.’s distinctive color trademark as used on its instruments and in these materials
are trademarks, service marks, registered trademarks, and/or registered service marks of Petroleum
Analyzer Company, L.P. in the U.S. and other countries and are its sole and exclusive property.
Microsoft, Encarta, MSN, and Windows are either registered trademarks or trademarks of Microsoft
Corporation in the United States and/or other countries.
Other trademarks contained within these materials are the property of their respective owners.
Information
The information contained within these materials is subject to change without notice. PAC makes no
warranties or guarantees, either expressed or implied in these materials, including the warranty of
merchantability or fitness for a particular purpose. At any time, PAC may modify these materials, its
instruments or its programs without notice and subsequent versions of these materials may contain
different information. These materials could contain technical inaccuracies and/or typographical
errors.
PAC does not assume responsibility for the accuracy of any translation of these materials.
About PAC
PAC develops advanced instrumentation for lab and process applications based on strong Analytical
Expertise that ensures Optimal Performance for our clients. Our analyzers help our clients meet
complex industry challenges by providing low cost of ownership, safe operation, high performance with
fast, accurate, actionable results, high uptime through reliable instrumentation, and compliance with
standard methods.
Our solutions are from industry-leading brands: AC Analytical Controls, Advanced Sensors, Alcor, Antek,
Herzog, ISL, Cambridge Viscosity, PSPI, and PetroSpec. We are committed to delivering superior and
local customer service worldwide with 16 office locations and a network of over 50 distributors. PAC
operates as a unit of Roper Technologies, Inc., a diversified technology company and a constituent of
S&P 500, Fortune 1000, and Russell 1000 indices.
Publication Date: November 10, 2015
Publication Time: 2 p.m.
Document Number: MAN R6000S
Part Number: MAN R6000S

R6000S Operation Manual: Rev. G
PAC L.P., All Rights Reserved, 2015 Page 1 of 92
GENERAL DISCLAIMERS AND NOTICES
Thank you for purchasing a PAC™ product. This instruction manual should be read thoroughly and all
operators should be given adequate training before attempting to place this unit in service. Consult your
company’s training program(s) for correct training. Anyone using or encountering this product must read
and understand the stated Cautions, Dangers, Notes, Warnings, etc., in this document, and compliance
with these safety signals and the recommended operating and maintenance parameters is essential to
safe and satisfactory operation, preventive maintenance or service. Failure to follow these instructions
and safety signals could result in damage to property, personal injury, or death.
This manual contains confidential and proprietary information that is the property of PAC, L.P. The
information contained in this document is subject to change without notice. This document is for
information only. The manufacturer accepts no liability for errors contained herein or for incidental or
consequential damages arising from the furnishing, performance, or use of this material.
Unless otherwise specified, each reference to names or individual trademarks and service marks has the
sole purpose of illustrating the product described here. Contents of this publication may not be
reproduced in any form or by any means (including electronic storage and retrieval or translation into a
foreign language) without prior agreement and written consent from the copyright owner. All rights
reserved.
The instructions given herein cover generally the description, installation, operation, and maintenance of
subject equipment. PAC reserves the right to make engineering refinements that may not be reflected in
this manual. Should any questions arise which may not be answered specifically by these instructions,
they should be directed to PAC for further detailed information and technical assistance.
Your satisfaction and safety are important to PAC, and a complete understanding of this manual is
necessary to attain these objectives. As the ultimate user of this apparatus, it is your responsibility to
understand its proper function and operational characteristics.
This unit should be used only for its intended operation; alterations will void the Warranty.
This manual contains confidential and proprietary information that is the property of PAC L.P. This
manual and all information disclosed herein shall not be used to manufacture, construct, or fabricate the
goods disclosed herein; shall not be exploited or sold; shall not be copied or otherwise reproduced in
whole or in part and shall not be revealed or disclosed to others or in any manner made public without the
express written permission of PAC L.P.
Copyright ©2015, by PAC, LP Houston, Texas.
Printed in the United States of America
All rights reserved.
Contents of this publication may not be reproduced in any form
without permission of the copyright owner.
01.02.2015

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IN THIS MANUAL
This manual describes the correct operation for the PAC R6000S. Within this manual the PAC R6000S
will be referred to as R6000S.
The below section provides an overview of this manual. A full Table of Contents follows this section.
Front Matters: Provides warranty information, contact information, Notices, Cautions, Warnings,
environmental information, and other basic information.
Chapter 1, Introduction: A general introduction to the R6000S detailing the basic theory of operation.
Chapter 2, Installation: Steps to unpack, inspect and prepare the R6000S for use. Explains the optional
equipment available.
Chapter 3, Operation: Setup, calibration and operation information.
Chapter 4, Maintenance and Troubleshooting: Provides general maintenance instructions and
preventative maintenance schedules.
Chapter 5, Drawings and Documents: Assembly drawings and diagrams of key components of the
R6000S.

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TABLE OF CONTENTS
CONTACT US ...................................................................................................................15
SAFETY AND INFORMATIONAL MESSAGES ................................................................18
REFERENCES ..................................................................................................................22
DEFINITIONS OF TERMS.................................................................................................22
MAINTENANCE TOOLS NEEDED....................................................................................24
PERSONAL PROTECTION EQUIPMENT.........................................................................24
LOCK-OUT/TAG-OUT PROCEDURES.............................................................................25
ACRONYMS......................................................................................................................25
1. CHAPTER ONE: INTRODUCTION...........................................................................27
1.1 Intended Audience..................................................................................................... 27
1.2 Theory of Operation................................................................................................... 27
1.3 Model R6000S Specifications ................................................................................... 28
1.4 Component Description ............................................................................................ 29
1.4.1 Controls and Indicators.................................................................................... 29
2. CHAPTER TWO: INSTALLATION ...........................................................................35
2.1 Preinstallation Requirements ................................................................................... 35
2.2 Installation Procedures ............................................................................................. 36
2.2.1 Gas Fittings........................................................................................................ 36
2.2.2 Gas Connections............................................................................................... 36
2.2.3 Signal and Power Connections ....................................................................... 37
2.2.4 Pyrotube Installation......................................................................................... 39
3. CHAPTER THREE: OPERATION.............................................................................43
3.1 Initial Startup Procedure ........................................................................................... 43
3.2 Calibrating the Analyzer............................................................................................ 44
3.2.1 Set Zero.............................................................................................................. 44
3.2.2 Set Span............................................................................................................. 45
3.2.3 Normal Operation.............................................................................................. 45
3.2.4 Temperature Controller Settings..................................................................... 45
3.2.5 Adjusting Full-Scale.......................................................................................... 47
4. CHAPTER FOUR: MAINTENANCE AND TROUBLESHOOTING............................49
4.1 Routine Preventative Maintenance .......................................................................... 49
4.1.1 Maintenance Intervals....................................................................................... 49
4.2 Removal and Replacement Procedures .................................................................. 50
4.2.1 Sulfur Detector Removal and Replacement ................................................... 51
4.2.2 Photomultiplier Tube Removal and Replacement ......................................... 52
4.2.3 Pre-amplifier Assembly Removal and Replacement ..................................... 53
4.2.4 Fluorescence Chamber Assembly Removal .................................................. 54
4.2.5 UV Lamp Nulling Procedure............................................................................. 55
4.2.6 UV Lamp Replacement ..................................................................................... 56
4.2.7 UV / PMT Power Supply Removal and Replacement Procedure.................. 58
4.2.8 Thermoelectric Cooler Replacement............................................................... 59
4.2.9 Temperature Sensor Replacement.................................................................. 60
4.3 Gas Leak Testing ....................................................................................................... 61
4.4 Light Leak Testing Procedure................................................................................... 61

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4.5 Fluorescence Chamber Lens Cleaning Procedure................................................. 63
4.6 PMT High-Voltage Adjustment.................................................................................. 64
4.7 Troubleshooting and Service Guide ........................................................................ 64
4.7.1 Electrical / Electronic Component Replacement ........................................... 65
4.7.2 Troubleshooting Guide..................................................................................... 66
5. DRAWINGS AND DOCUMENTS..............................................................................77
5.1 Drawings..................................................................................................................... 77

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POLICY STATEMENT
This is the property of PAC L.P. This manual and all information disclosed herein shall not be used to
manufacture, construct, or fabricate the goods disclosed herein; shall not be exploited or sold; shall not
be copied or otherwise reproduced in whole or in part and shall not be revealed or disclosed to others or
in any manner made public without the express written permission of PAC L.P.
GENERAL INFORMATION
FCC Notice
This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant
to Part 15 of the FCC Rules. These limits are designed to provide reasonable protection against harmful
interference when the equipment is operated in a commercial environment. This equipment generates,
uses, and can radiate radio frequency energy and, if not installed and used in accordance with the
instruction manual, may cause harmful interference to radio communications. However, there is no
guarantee that interference will not occur in a particular installation. If this equipment does cause harmful
interference to radio or television reception, which can be determined by turning the equipment off and
on, the user is encouraged to try to correct the interference by one or more of the following measures:
Reorient or relocate the receiving antenna.
Increase the separation between the equipment and receiver.
Connect the equipment into an outlet on a circuit different from that to which the receiver is
connected.
Consult the dealer or PAC, L.P. for help.
User changes or modifications not expressly approved by PAC, L.P. could void the user’s authority to
operate the equipment.
Use only accessories provided with the R6000S or PAC approved options for continued FCC
compliance.

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Disposal
Correct disposal of Waste Electrical and Electronic Equipment in the end-of-life
Applicable in the European Union and other European countries with separate collection systems
This product is designed for exclusive professional use by commercial companies. This marking shown
on the product or its literature, indicates that it should not be disposed with other household wastes at the
end of its working life.
To prevent possible harm to the environment or human health from uncontrolled waste disposal, please
separate this from other types of wastes and recycle it responsibly to promote the sustainable reuse of
material resources.
Business users should contact the producer or the importer and check the terms and conditions of the
purchase contract. If you have a separate agreement with your producer or importer such that you will
take care of end-of-life disposal on your own, please ensure an environmentally sound disposal according
to the legal regulations for electric and electronic waste equipment in your country.
WARNING: This product should not be mixed with other commercial wastes for disposal.
The above WEEE symbol is the official marking for equipment under the WEEE scope. In some EC
Member states, "pure B2B equipment" is not necessarily marked with the waste bin symbol. To provide a
homogenous EC-wide procedure, PAC uses the marking in all EC Member states.
CE NOTICE
The symbol indicates PAC’s compliance with the European Union (EU) directives and standards
listed below:
EMC Directive 89/336/EEC
EN 55011: 1998 “Electrical equipment for measurement, control and laboratory use. EMC requirements.
Particular requirements. Test configurations, operational conditions and performance criteria for sensitive
test and measurement equipment for EMC unprotected applications”