Rigaku Smartlab SE + HyPix-400 User manual
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~Rigaku
,,..:!f
Smartlab
SE
Smartlab
SE
+ HyPix-400 System
Instrt1ction Manual
This manual describes the correct use
of
the product
as
well the usage precautions to
be
observed. To obtain
full-expected performance from the product, please read this manual thoroughly.
Also, store this manual at an easily accessible place so that you can promptly refer to
it
whenever it
is
necessary.
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of
the product and the contents
of
the printed
materials including the manual without notice in the future.
) The contents described in this manual may not
be
disclosed to a third patty or copied, in whole or in
part, without the written consent
of
Rigaku Corporation.
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be
responsible for the results
of
the use
of
this manual.
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Contents
C>\IE!r\lit!vv
................................................
~································
1
Components
and
Specifications
............
.,.
................................
3
Configuration
...............................................................................................
3
Names
of
Parts
.............................................................................................
4
Specifications
...............................................................................................
5
Detector
................................................................................................
5
Distance between sample and
detector
......................................................
6
Measurement range
................................................................................
6
Installation
.............................................................................
7
Installing
HyPix-400 on
Smartlab
SE
..........................................
...............
......
7
Installing
HyPix-400
(OD
and
10
measurement
mode)
.................................
7
Installing
HyPix-400 (2D
measurement
mode)
..........................................
13
Changing
from
horizontal
mount
to
vertical
mount
.....................................
15
Connecting cables
of
HyPix-400 and
PCs
.....................
..........
.........................
18
Operations····························~···············································
19
Starting
up
HyPix-400
..........
......
.................................................................
19
Setting
and
controlling
HyPix-400
..................................................................
22
HyPix-400
Detector
settings
...................................................................
22
HyPix
Adjustment
Part
...........................................................................
24
HyPix Calibration Part
............................................................................
24
Shutting
down HyPix-400
........
...
..................................................................
25
Troubleshooting
....................................................................
27
HyPix-400 is
not
recognized
.........................................................................
27
A
temperature
warning is displayed
...............................................................
29
Abnormalities
in profiles
or
images
................................................................
30
Window
damage
.......
......
.....................................................
....
...................
31
Item No. A00007626 I A00010204
Manual
No. ME15743A02
2019.
03
(2nd Edition)
Rigc.kuo
SmartLab SE + HyPix-400 System
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Rigc,okuo
HyPix-400 is a hybrid multi-dimensional pixel detector as an optional component
for SmartLab SE. The combination
of
SmartLaib SE and HyPix-400 enables not
only
20
measurement but also
10
and
OD
measurements.
This instruction manual describes the procedure for using HyPix-400 with
SmartLab SE.
HyPix-400 main
unit
External view
of
SmartLab
SE's
goniometerwith HyPix-400
SmartLab
SE+
HyPix-400 System 1
IConfiguration
HyPix-400 main
unit
Component
Q'ty
HyPix-400 main unit I
HyPix-400 mount holder for SmartLab SE (horizontal) I
HyPix server
pc*'
I
( HyPix server software*' l
LAN cable (between HyPix and server PC ) I
LAN card and cable*' (between server PC and control PC) I set
Power supply circuit'' l
Power cable•, (integrated with a trigger signal cable) I
*I Already installed on the SmartLab SE main unit or control PC.
HyPix-400
standard
accessories
Component
Q'ty
Protection cover I
Incident Soller slit Open I
2D
slit for
Cu
l
(
Filter
box
for HyPix-400 I
Al203 powder sample I
HyPix-400 optional accessories
Component
Q'ty
HyPix-400 mount holder for SmartLab SE (vettical)
Rigaku
SmartLab
SE+
HyPix-400 System 3
Components
and
Specifications
INames of Parts
HyPix-400 main
111Dit
(DHyPix-400 main unit A hybrid multi-dimensional pixel detector
~HyPix-400
mount holder A holder for installing the HyPix-400 in the
for SmartLab
SE
horizontal direction on SmartLab SE.
(horizontal)
@Protection cover Protects the detecting surface
of
HyPix-400.
4 SmartLab
SE+
HyPix-400 System
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Rigcakuo
Specifications
ISpecifications
Detector
Pixel size 100 µmx100 µm
Active area 9.6 mm x 38.5 mm
The number
of
pixels 96 x 385 = 36,960 pixels
Count rate per pixel >1 x
10
6 cps/pixel
Global count rate >3.7 x
10
10
cps
Readout mode Long
(31
bit) mode,
Diff
mode, 0-dead time
mode
Framing rate
131
fps (Diffmode), 87 fps (Long mode)
Energy range 4 to 30 keV
Counting efficiency 99% (at CuKa)
Energy resolution <25% (at CuKa)
Guaranteed operating
15
to 35°C (59 to 95°F)
temperature*1
Guaranteed operating
20to
65%RH
humidity
Guaranteed operating
Tc
o
rr
.±4
°C
(7°F)
temperature*2
Weight Approx. 900 g
(1
.98 lb.)
*1 All the detector functions operate normally within the range
of
guaranteed
operating temperature.
*2 All the specifications written in this manual are guaranteed within the range
of
guaranteed operating temperature. T
,o
rr
. indi.cates the corrected temperature.
SmartLab SE +HyPix-400 System 5
Components and Specifications
CAUTION
~
Distance between sample and detector
OD
and ID
measurement mode
20
measurement mode
300
mm
recommended
Within the range
of
150 to 300 mm (Standard)
The distance between the sample and detectoir can be extended up to
110
mm
by removing the positioning screw from the theta_d arm. In that case, some
of
the attachments may collide with HyPix-400. Confirm that the mounted
attachment and HyPix-400 do not collide with each other beforehand, and use
the distance at your own risk.
Positioning screw on the theta_d arm
Measurement range
i
2e
angle upper limit
160°
Other measurement ranges depend on the speciifications
of
SmaitLab SE.
6 SmartLab
SE+
HyPix-400 System
Rigcdc:._.
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Rig,t,,ku
Iinstalling HyPix-400 on Smar1Lab SE
Installing HyPix-400
(OD
and 1D measurement mode)
This section describes the procedure for installing HyPix-400 and rece1vmg
optical devices (hereafter called receiving optics) on Smai1Lab SE for the
OD
and
ID
measurement mode.
For the normal
OD
and
ID
measurement mode, mount the following devices on
the theta_d arm
of
SmartLab
SE
in order from the sample side: receiving slit box,
receiving optics unit # l (ROD), receiving optics unit #2 (RPS), and HyPix-400
main unit.
• The names
of
variable axes
of
the receiving slit
box'
1 are as follows:
Slit width:
Slit height:
RSI
Zr
•
The
filter
box'
2 does not have movable axe
s:
.
When the active area
of
HyPix-400
is
limited, it functions as a Vi1iual receiving
slit.
The name
of
this slit is
Virtual receiving slit (RS2):
Virtual receiving slit
Receiving
slit
(RS2)
(RS1
, Zr)
300mm
When
receiving slit box is
mounted
RS2.
Virtual receiving slit
(RS2)
When filter box is
mounted
Installation position ofHyPix-400
and
receiving optics for
OD
and
lD
measurement mode
*1
111e
receiving slit box contains a variable slit, slit height adjustment axis, and
KP
filter insertion slot,
and is available in both
OD
and
ID
measurement mode.
*2
The filter box contains a scattered radiation protector,
fi
xed slit with a wide aperture, and
KP
filter
insertion slot, and is mainly used for ID measurement mode.
SmartLab
SE
+HyPix-400 System 7
Installation
1 Mount HyPix-400
on
SmartLab SE.
G) Place HyPix-400 on the theta_d arm
of
SmartLab
SE
so that the
indicator
of
HyPix-400
is
positioned at 350 mm. Then fix it with the
Allen wrench provided.
Mounting HyPix-400
The indicator
of
HyPix-400 indicates +50 mm from the detection surface,
and thus the detection surface is positioned at 300 mm.
Indicator position
(The sample -detector distance is set a1t 300 mm in the above picture.)
We
recommend attaching the protection cover on the detection surface
of
HyPix-400.
It
prevents the detection surface from being damaged while
mounting the receiving optics or HyPix-400.
When using HyPix-400 with SmartLab SE in
OD
and ID measurement mode, set
the detector at 300 mm
of
the sample -detector distance.
8 SmartLab
SE+
HyPix-400 System
(
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Rigc,oku
Installing HyPix-400
on
SmartLab
SE
~
Connect the
"DETECTOR"
cable
to
the "DETECTOR" connector
on the receiving connector box.
Connecting the
DETECTOR
cable
2
Mount
the RPS
adapter
and receiving Soller slit.
G)
Mount the RPS adapter and receiving Soller slit at the front
of
the
HyPix-400, and fix them with the Allen wrench provided.
Mounting the RPS
adapter
and
receiving Sollerslit
SmartLab
SE+
HyPix-400 System 9
Installation
(2)
Connect the "RPS" cable to the "RPS" connector on the receiving
connector box.
Connecting the RPS cable
3 Mount the ROD adapter and PSA.
G) In the same way as step 2, mount the ROD adapter and PSA at the
front
of
the RPS adapter and the receiving Soller slit.
Mounting the ROD adapter and PSA
10 SmartLab SE + HyPix-400 System
Rigolku
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Rigcllkuo
Installing HyPix-400
on
SmartLab
SE
CZ)
Connect the
"ROD"
cable to the
"ROD"
connector on the receiving
connector box.
Connecting the
ROD
cable
4
Mount
the receiving slit box (
or
filter box).
CD
Push the receiving slit box (or filter box) against the positioning screw
on the theta_d arm, and fix it with the Allen wrench provided.
Pushing the receiving slit box against the positioning screw
SmartLab SE +HyPix-400 System
11
Installation
Mounting the receiiving slit box
AK~
filter can
be
inserted into the receiving slit box or filter box.
(2)
Connect the "RSl" cable to the "RSl" connector on the receiving
connector box.
Connecting the cable
5 Perform axial initialization.
Perform axial initialization via SmartLab Studio
II
after mounting the
receiving optics and HyPix-400. (Refer to "6.2 Initializing axes" in
"SmartLab Studio
II
XRD
Measurement Plugin User Manual".)
The protection cover must
be
removed
if
mounted before performing
measurements.
12 SmartLab
SE+
HyPix-400 System
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Riigc,,ku
Installing HyPix-400 on
SmartLab
SE
Installing HyPix-400
(20
measurement mode)
This section describes the procedure for installing HyPix-400 on SmartLab SE
for
20
measurement mode.
On the receiving side
of
20
measurement, no optics other than Pix-400 are
generally set. Therefore, HyPix-400 can be set at any position within the sample
-detector distance ranging from
150
to 300 mm.
On the incident side, the micro-area optics, CBO-
f,
CBO-µ, collimator, etc. need
to be set to form a point X-ray beam.
For setting the sample -detector distance, subtract 50 mm from the position to
which the HyPix-400's indicator points.
Co
ll
i
ma
to
r s
amp
le
/
''
----
----
-c"':':'=l=':51-
CBO
Incident
opt
ics
300mm
I
,,
L
1
Mount
HyPix-400 on
SmartLab
SE.
-300mm
(Variable)
Mount HyPix-400 on the theta_d arm, adjusting the sample -detector
distance with the indicator. Then fix it with the Allen wrench provided.
Installation position ofHyPix-400
and
indicator
for 2D measurement mode
(The sample -detector distance
is
set to
2:00
mm
in the above picture.)
SmartLab SE + HyPix-400 System 13
Installation
2 Connect the cables, referring to step
:z
to
4
of
"Installing HvPix-400
(OD
and ID measurement mode)
."
The
procedure
for installing
HyPix-400
is
now
completed.
After installing HyPix-400, update the configuration for the currently mounted
receiving optics in SmartLab Studio II.
The protection cover must be removed from the detection surface
of
HyPix-400
if
mounted before performing measurements.
For 2D measurement mode, the following incident optics are available 2D slit,
selection slit for micro area measurement (MA0.5 etc.), collimator,
CBO-f
and
point-focus optics. For details, refer to the SmartLab SE Instruction Manual
(MEI
1628*
).
The optics using the 2D slit are dedicated for
2D
measurement with the
para-focusing method. Set the sample -detector distance to 300
mm
which is
equal to the goniometer radius (the distance between X-ray source and sample)
of
SmartLab SE).
14 SmartLab
SE+
HyPix-400 System
Rigclllcu
(
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Installing HyPix-400 on
SmartLab
SE
Changing from horizontal mount to vertical mount
The HyPix mount holder for SmaitLab SE (horizontal)
is
included in the
standard components. Optionally, the ve1tical type is also available. This
optional holder
is
used when the user wants to mount the detector vertically on
the theta_d arm. The ve1tically mounted HyPix-400 is able to obtain data
of
a
wide 2theta range during a single exposure.
Horizontal
mount
(standard)
Vertical
mount
(optional)
This section describes the procedure for changing the HyPix mount holder from
horizontal mount to ve1tical mount.
1
Turn
the detector over so
that
its detection surface faces the
right
side.
Then
remove the
four
screws from
the
rear
side
of
HyPix-400
and
remove the
mount
holder (horizontal).
Removing the screws
and
mount
holder (horizontal) from the
rear
side
of
HyPix-400
SmartLab SE +HyPix-400 System 15
Installation
2
Attach
the
mount
holder
(vertical)
onto
the
rear
side
of
HyPix-400
and
fix
it
with
the
four
screws.
Hard limiter
Attaching
the
mount
holder
(horiwntal)
from
the
rear
side
of
HyPix-400
A hard limiter
is
attached
to
the HyPix-400 holder (vertical mount)
to
avoid
interference between the HyPix-400 and the incident optics. The 20 values for
limiter activation are
as
shown in the table below.
20 values
for
limiter activation
HyPix-400 20 values for limiter activation (deg)
Camera length
(mm)
OD
mode
ID
mode
150
150
142
200
155
150
250 156
152
300 160
155
*28 values vary slightly depending on the confiiguration
of
the incident optics.
The goniometer stops automatically when the limiter
is
activated during scans or
axis movement.
It
is
necessary to perform a forced initialization
of
the
Els
axis after
the goniometer has stopped.
For information on the forced initialization
of
axes, refer
to
"6.2 Initializing axes"
in the "Smar/Lab Studio IIXRD Measurement Plugin User Manual".
16 Smar!Lab
SE+
HyPix-400 System
Riigcakuo
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