Rigaku Smartlab SE + HyPix-400 User manual

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~Rigaku
,,..:!f Smartlab SE
Smartlab SE + HyPix-400 System
Instrt1ction Manual

This manual describes the correct use of the product as well the usage precautions to be observed. To obtain
full-expected performance from the product, please read this manual thoroughly.
Also, store this manual at an easily accessible place so that you can promptly refer to
it whenever it is necessary.
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part, without the written consent
of Rigaku Corporation.
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Contents
C>\IE!r\lit!vv ................................................ ~································ 1
Components and Specifications ............ .,. ................................ 3
Configuration ............................................................................................... 3
Names
of Parts ............................................................................................. 4
Specifications
............................................................................................... 5
Detector ................................................................................................ 5
Distance between sample and
detector ...................................................... 6
Measurement range
................................................................................ 6
Installation ............................................................................. 7
Installing HyPix-400 on Smartlab SE .......................................... ............... ...... 7
Installing HyPix-400 (OD and 10 measurement mode) ................................. 7
Installing HyPix-400 (2D measurement mode) .......................................... 13
Changing
from horizontal mount to vertical mount ..................................... 15
Connecting cables
of HyPix-400 and PCs ..................... .......... ......................... 18
Operations····························~··············································· 19
Starting up HyPix-400 .......... ...... ................................................................. 19
Setting and controlling HyPix-400 .................................................................. 22
HyPix-400
Detector settings ................................................................... 22
HyPix
Adjustment Part ........................................................................... 24
HyPix Calibration Part
............................................................................ 24
Shutting down HyPix-400 ........ ... .................................................................. 25
Troubleshooting .................................................................... 27
HyPix-400 is not recognized ......................................................................... 27
A
temperature warning is displayed ............................................................... 29
Abnormalities in profiles or images ................................................................ 30
Window
damage ....... ...... ..................................................... .... ................... 31
Item No. A00007626 I A00010204
Manual No. ME15743A02
2019.
03 (2nd Edition)
Rigc.kuo
SmartLab SE + HyPix-400 System

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HyPix-400 is a hybrid multi-dimensional pixel detector as an optional component
for SmartLab SE. The combination of SmartLaib SE and HyPix-400 enables not
only 20 measurement but also 10 and OD measurements.
This instruction manual describes the procedure for using HyPix-400 with
SmartLab SE.
HyPix-400 main unit
External view of SmartLab SE's goniometerwith HyPix-400
SmartLab SE+ HyPix-400 System 1

IConfiguration
HyPix-400 main unit
Component Q'ty
HyPix-400 main unit I
HyPix-400 mount holder for SmartLab SE (horizontal) I
HyPix server pc*'
I
( HyPix server software*' l
LAN cable (between HyPix and server PC ) I
LAN card and cable*' (between server PC and control PC) I set
Power supply circuit'' l
Power cable•, (integrated with a trigger signal cable) I
*I Already installed on the SmartLab SE main unit or control PC.
HyPix-400 standard accessories
Component Q'ty
Protection cover I
Incident Soller slit Open I
2D slit for Cu
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Filter box for HyPix-400 I
Al203 powder sample I
HyPix-400 optional accessories
Component
Q'ty
HyPix-400 mount holder for SmartLab SE (vettical)
Rigaku
SmartLab SE+ HyPix-400 System 3

Components and Specifications
INames of Parts
HyPix-400 main 111Dit
(DHyPix-400 main unit A hybrid multi-dimensional pixel detector
~HyPix-400 mount holder A holder for installing the HyPix-400 in the
for SmartLab SE
horizontal direction on SmartLab SE.
(horizontal)
@Protection cover Protects the detecting surface
of HyPix-400.
4 SmartLab SE+ HyPix-400 System

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Specifications
ISpecifications
Detector
Pixel size 100 µmx100 µm
Active area 9.6 mm x 38.5 mm
The number of pixels 96 x 385 = 36,960 pixels
Count rate per pixel >1 x 10
6 cps/pixel
Global count rate >3.7 x 10
10
cps
Readout mode Long
(31 bit) mode, Diff mode, 0-dead time
mode
Framing rate
131 fps (Diffmode), 87 fps (Long mode)
Energy range 4 to 30 keV
Counting efficiency 99% (at CuKa)
Energy resolution <25% (at CuKa)
Guaranteed operating
15 to 35°C (59 to 95°F)
temperature*1
Guaranteed operating
20to 65%RH
humidity
Guaranteed operating
Tc o rr .±4 °C (7°F)
temperature*2
Weight Approx. 900 g (1 .98 lb.)
*1 All the detector functions operate normally within the range of guaranteed
operating temperature.
*2 All the specifications written in this manual are guaranteed within the range of
guaranteed operating temperature. T ,o rr . indi.cates the corrected temperature.
SmartLab SE +HyPix-400 System 5

Components and Specifications
CAUTION
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Distance between sample and detector
OD and ID
measurement mode
20 measurement mode
300
mm recommended
Within the range
of 150 to 300 mm (Standard)
The distance between the sample and detectoir can be extended up to
110 mm
by removing the positioning screw from the theta_d arm. In that case, some
of
the attachments may collide with HyPix-400. Confirm that the mounted
attachment and HyPix-400 do not collide with each other beforehand, and use
the distance at your own risk.
Positioning screw on the theta_d arm
Measurement range
i 2e angle upper limit 160°
Other measurement ranges depend on the speciifications of SmaitLab SE.
6 SmartLab SE+ HyPix-400 System
Rigcdc:._.