Teledyne 5800 Operating instructions

5800 Refrigerated
Sampler
Installation and Operation Guide
Part #69-5803-086 of Assembly #60-5804-051
Copyright © 2012. All rights reserved, Teledyne Isco
Revision H, August 2016

Foreword
This instruction manual is designed to help you gain a thorough understanding of the operation of
the equipment. Teledyne Isco recommends that you read this manual completely before placing the
equipment in service.
Although Teledyne Isco designs reliability into all equipment, there is always the possibility of a
malfunction. This manual may help in diagnosing and repairing the malfunction.
If a problem persists, call or e-mail Teledyne Isco technical support for assistance. Simple
difficulties can often be diagnosed over the phone. For faster service, please have your serial
number ready.
If it is necessary to return the equipment to the factory for service, please follow the shipping
instructions provided by technical support, including the use of the Return Material
Authorization (RMA) specified. Be sure to include a note describing the malfunction. This will
aid in the prompt repair and return of the equipment.
Teledyne Isco welcomes suggestions that would improve the information presented in this manual
or enhance the operation of the equipment itself.
Teledyne Isco is continually improving its products and reserves the right to change product
specifications, replacement parts, schematics, and instructions without notice.
Contact Information
Customer Service
Phone: [phone] (USA, Canada, Mexico)
[phone] (Outside North America)
Fax: [phone]
Email: [email protected]
Technical Support
Phone: Toll Free [phone] (Syringe Pumps and Liquid Chromatography)
Email: [email protected]
Return equipment to: 4700 Superior Street, Lincoln, NE 68504-1398
Other Correspondence
Mail to: P.O. Box 82531, Lincoln, NE 68501-2531
Email: [email protected]

Isco 5800 Refrigerated Sampler
v
Isco 5800 Refrigerated Sampler
Safety Information The Isco 5800 Refrigerated Sampler is a “definite purpose”
device, intended for use only with compatible Isco equipment.
Except as described in this manual, do not use this product with
any other manufacturers’ equipment, or for any other purpose.
Use for any purpose not described in this manual could cause
personal injury or property damage.
Electrical Requirements The sampler requires either 100 VAC/50 Hz, 115 VAC/60 Hz, or
230 VAC/50 Hz AC power. See , on page 20. Refer to the
nameplate and ratings label inside the refrigerator
compartment. The power input is through the mains power cord
at the back of the sampler. The sampler’s compressor is protected
by an internal thermal cut-out. Additionally, the sampler
controller circuitry is protected by an internal 5.0 ampere PTC
(Positive Temperature Coefficient) device.
WARNING
Electrocution hazard. Never manipulate electrical switches
or power connections with wet hands or when your feet are
in contact with water.
WARNING
AC electrical power must meet the applicable electrical
code requirements for your installation and must be
provided with an earth ground connection. If necessary,
consult with a certified electrician to ensure that AC power
is provided in accordance with the local electrical code.
The AC power cord of this device is equipped with a three-prong
grounding plug designed to mate with a grounded power outlet.
Grounding minimizes the possibility of electrical shock.
It is the user’s responsibility to ensure that the AC power source
is properly grounded. If in doubt, have the outlet checked by a
qualified electrician.
If the available AC power outlet only accepts two prongs, or if it
is determined that the outlet is improperly grounded, the outlet
must be replaced by a qualified electrician before attempting to
power this device.
WARNING
Never modify the AC power cord or use a three-prong to
two-prong adapter.
WARNING
If this device’s power cord is frayed or otherwise damaged,
discontinue its use immediately. The AC power cord is not
user-serviceable and must be returned to the factory for
repair or replacement.

Isco 5800 Refrigerated Sampler
vi
General Warnings Before installing, operating, or maintaining this equipment, it is
imperative that all hazards and preventive measures are fully
understood. While specific hazards may vary according to
location and application, take heed in the following general
warnings:
WARNING
This instrument has not been certified for use in
“hazardous locations” as defined by the National Electrical
Code.
WARNING
Avoid hazardous practices! If you use this instrument in
any way not specified in this manual, the protection
provided by the instrument may be impaired; this will
increase your risk of injury.
WARNING
Servicing of this product without proper training and
qualifications can potentially expose you to electrical and
mechanical hazards that can result in serious or fatal injury.
Servicing must be performed only by trained and qualified
personnel.
WARNING
Removing a module exposes you to electrical and
mechanical hazards. Always disconnect from AC power
before attempting to remove any module. Only trained
service personnel may remove or replace these modules.
WARNING
The sampler has a safety interlock that prevents the pump
from operating when the pump housing band is open. The
pump is extremely powerful and can injure you severely if
the sampler activates the pump during
maintenance/servicing. Remove power from the sampler
before opening the pump housing.
Additional safety information can be found in Appendix B.

Isco 5800 Refrigerated Sampler
vii
Hazard Severity Levels This manual applies Hazard Severity Levels to the safety alerts,
These three levels are described in the sample alerts below.
CAUTION
Cautions identify a potential hazard, which if not avoided, may
result in minor or moderate injury. This category can also warn
you of unsafe practices, or conditions that may cause property
damage.
WARNING
Warnings identify a potentially hazardous condition, which
if not avoided, could result in death or serious injury.
DANGER
DANGER – limited to the most extreme situations
to identify an imminent hazard, which if not
avoided, will result in death or serious injury.

Isco 5800 Refrigerated Sampler
viii
Hazard Symbols The equipment and this manual use symbols used to warn of
hazards. The symbols are explained below.
Hazard Symbols
Warnings and Cautions
The exclamation point within the triangle is a warning sign alerting you of
important instructions in the instrument’s technical reference manual.
The lightning flash and arrowhead within the triangle is a warning sign alert-
ing you of “dangerous voltage” inside the product.
Pinch point. These symbols warn you that your fingers or hands will be seri-
ously injured if you place them between the moving parts of the mechanism
near these symbols.
Symboles de sécurité
Ce symbole signale l’existence d’instructions importantes relatives au
produit dans ce manuel.
Ce symbole signale la présence d’un danger d’électocution.
Risque de pincement. Ces symboles vous avertit que les mains ou les
doigts seront blessés sérieusement si vous les mettez entre les éléments
en mouvement du mécanisme près de ces symboles
Warnungen und Vorsichtshinweise
Das Ausrufezeichen in Dreieck ist ein Warnzeichen, das Sie darauf
aufmerksam macht, daß wichtige Anleitungen zu diesem Handbuch
gehören.
Der gepfeilte Blitz im Dreieck ist ein Warnzeichen, das Sei vor “gefährlichen
Spannungen” im Inneren des Produkts warnt.
Vorsicht Quetschgefahr! Dieses Symbol warnt vor einer unmittelbar drohen-
den Verletzungsgefahr für Finger und Hände, wenn diese zwischen die
beweglichen Teile des gekennzeichneten Gerätes geraten.
Advertencias y Precauciones
Esta señal le advierte sobre la importancia de las instrucciones del manual
que acompañan a este producto.
Esta señal alerta sobre la presencia de alto voltaje en el interior del pro-
ducto.
Punto del machacamiento. Sus dedos o manos seriusly serán dañados si
usted los coloca entre las piezas móviles cerca de estos símbolos.

ix
Isco 5800
Refrigerated Sampler
Table of Contents
Section 1 Introduction
1.1 Sampler Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
1.2 Features. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2
1.3 Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4
Section 2 Installation
2.1 Unpacking the Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
2.2 5800 Sampler Installation Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
2.3 Positioning the Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
2.4 Connecting Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5
2.4.1 Backup Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5
2.5 Installing a Bottle Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-6
2.5.1 Installing the Distributor Arm and Discharge Tube . . . . . . . . . . . . . . . . . . 2-7
2.5.2 24 Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-8
2.5.3 4 10L (2.5 Gal) Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-11
2.5.4 2 Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-11
2.5.5 4, 20L (5 Gal) Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-12
2.5.6 1 Bottle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-12
2.6 Attaching the Suction Line. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-14
2.6.1 Vinyl Suction Line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-14
2.6.2 FEP-lined Suction Line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-15
2.7 Attaching a Strainer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-16
2.7.1 Alternative to Strainers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-17
2.7.2 Maximum Unanchored Length . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-17
2.8 Routing the Suction Line and Strainer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-17
2.9 Connecting the Sampler to External Devices . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-18
2.9.1 Standard Isco Instrument Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-18
2.9.2 Other Device Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-19
2.10 Configuring and Programming the Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-21
2.11 Locking the Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-21
Section 3 Programming
3.1 Control Panel Description. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
3.2 Getting Started . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2
3.3 Configuring the Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-3
3.3.1 Set Clock . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-3
3.3.2 Bottles and Sizes-Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
3.3.3 Suction Line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
3.3.4 Liquid Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-5
3.3.5 Flow Mode Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-6
3.3.6 Enable Pin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-6
3.3.7 Refrigeration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-7
3.3.8 Output Pins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-7
3.3.9 Tubing Life . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8

Isco 5800 Refrigerated Sampler
Table of Contents
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3.3.10 Program Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
3.3.11 Language . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
3.3.12 System IDs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
3.3.13 Run Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
3.3.14 Exit Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
3.4 Sampling Program Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
3.5 Programming Steps. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15
3.5.1 Program Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15
3.5.2 Pacing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15
3.5.3 Sample Every
__ Hours, __ Minutes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16
3.5.4 Sample Every
__ Pulses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16
3.5.5 __ Bottles per Sample Event . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18
3.5.6 Switch on Time or Number of Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18
3.5.7 Switch Bottles/Sets Every __ Hours, __ Minutes . . . . . . . . . . . . . . . . . . . . 3-19
3.5.8 First Switch Time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-19
3.5.9 __Samples per Bottle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-19
3.5.10 Run Continuously? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-19
3.5.11 Enter Sample Volume Use Defined Sample . . . . . . . . . . . . . . . . . . . . . . . 3-20
3.5.12 Volumes Dependent on Flow? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-20
3.5.13 Sample Volume __ ml . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-20
3.5.14 Flow Pulses,
Analog Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-20
3.5.15 10 ml for Every
__ Pulses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
3.5.16 Sample Volume at
20 mA: __ ml . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
3.5.17 __ Composite Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
3.5.18 Suction Head . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
3.5.19 Pause & Resume . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-22
3.5.20 No Delay to Start
Set Start Time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-23
3.5.21 Auto Re-Run . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.5.22 First Sample At: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.5.23 Start Flow Count At: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.5.24 Select Days: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.5.25 First Valid Day . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.5.26 Maximum Run Time
__ Hours . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
3.6 Programming Examples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
Section 4 Operation
4.1 Start a Sampler Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1
4.1.1 Start Time Delay . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1
4.1.2 The Run State . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
4.1.3 Completed Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
4.2 Pause or Stop a Running Program. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3
4.3 Post Sampling Activities. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3
4.3.1 View the Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3
4.3.2 Retrieve the Temperature Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5
4.3.3 Sampling Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7
4.3.4 Remove Sample Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7
4.4 Grab Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-8
4.5 Calibrate Sample Volumes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9
4.6 Operate the Pump Manually . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-10