Agilent Technologies Agilent G3215A User manual

Agilent Technologies
Agilent G3215A
Mass Spec Bench
User Guide
Revision A, May 2011

Mass Spec Bench User Guide
Notices
© Agilent Technologies, Inc. 2011
No part of this manual may be reproduced in
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tronic storage and retrieval or translation
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States and international copyright laws.
Manual Part Number
G3215-90001
Edition
Revision A, May 2011
Agilent Technologies, Inc.
5301 Stevens Creek Blvd.
Santa Clara, CA 95051
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Safety Notices
CAUTION
A CAUTION notice denotes a haz-
ard. It calls attention to an operat-
ing procedure, practice, or the like
that, if not correctly performed or
adhered to, could result in damage
to the product or loss of important
data. Do not proceed beyond a
CAUTION notice until the indicated
conditions are fully understood and
met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could result
in personal injury or death. Do not
proceed beyond a WARNING
notice until the indicated condi-
tions are fully understood and
met.

Mass Spec Bench User Guide 3
Contents
1 Introduction
General Information 6
Important Safety Warnings 8
Cleaning 9
Recycling the Product 10
Parts Identification 10
Site Preparation 12
2 Installation
Step 1. Unpack the Mass Spec Bench 14
Step 2. Prepare the pump tray 18
Step 3. Install the Rough Pumps inside Mass Spec Bench 22
Step 4. Attach the spray chamber exhaust hose 28
Step 5. Connect the power supply 28
Step 6. Verify the installation 29
Step 7. Move the Mass Spec Bench to its final position 31
3Operation
Front Panel Controls and Indicators 34
To handle temperature alarms 36
To change rough pump oil 37
4 Troubleshooting

4 Mass Spec Bench User Guide

5
Agilent G3215A Mass Spec Bench User Guide
Agilent Technologies
1
Introduction
General Information 6
Important Safety Warnings 8
Cleaning 9
Recycling the Product 10
Parts Identification 10
Site Preparation 12
This manual describes how to install, operate, and troubleshoot the Agilent
G3215A Mass Spec Bench.
The Mass Spec Bench is designed to accommodate the rough pump or pumps
used with your LC/MS or GC/MS System. It significantly reduces noise, while
two internal fans ensure that your pump does not overheat. The platform that
supports the rough pump is designed to be separated from the main frame of
the bench. This setup minimizes the vibration from the rough pump, which can
affect instrument performance of the LC/MS or GC/MS instrument. It is also
designed to capture any oil that leaks from the rough pump.
The Mass Spec Bench is compatible with BOC Edwards E1M18, E2M28 pumps,
and XDSi35 Dry Pumps. It is also compatible with Agilent MS40, TS600, and
TS800 pumps. These pumps are used with:
•Agilent 1100/1200 LC/MS Series instruments
•Agilent 6000 Series LC/MS Systems
•Agilent Single and Triple Quad GC/MS Systems
•Agilent 7500 Series ICP/MS
NOTE
The Mass Spec Bench is designed to be rolled on smooth hard surfaces found in the lab
environment. Moving the Mass Spec Bench on carpeted surfaces, rough surfaces, or
uneven surfaces can be difficult. Additionally, crossing thresholds can present problems as
the clearance on the pump tray feet is less than 3/4 of an inch.

1 Introduction
6 Mass Spec Bench User Guide
General Information
The Mass Spec Bench is designed to comply with the International
Electrotechnical Commission (IEC) 61010–1 safety standard.
The Mass Spec Bench Power Supply (part number 5188-1164) complies with
applicable safety and Electromagnetic Compatibility (EMC) requirements,
including:
•CISPR 11/EN 55011: Group 1, Class A
•IEC/EN 61326
•AUS/NZ
•Canada ICES-001/NMB-001
The Mass Spec Bench is designed and manufactured under a quality system
registered to ISO 9001.
Information
The Agilent Technologies Mass Spec Bench meets the following IEC
classifications: Installation Category II, Pollution Degree 2, and Equipment
Class III (except for the power supply provided, which is Equipment Class I).
The Mass Spec Bench is designed to be used with complete equipment. It is not
an electrical enclosure and does not have a protective conductor (ground)
terminal intended to be connected to an external protective earthing
(grounding) system.
The Mass Spec Bench is designed and tested in accordance with recognized
safety standards and is designed for use indoors. If it is used in a manner not
specified by the manufacturer, the protection provided by the instrument can
be impaired. Whenever the safety protection of the Mass Spec Bench has been
compromised, disconnect it from all power sources and secure it against
unintended operation.
Refer servicing to qualified service personnel. Substituting parts or
performing any unauthorized modification to the instrument can result in a
safety hazard.

Introduction 1
Mass Spec Bench User Guide 7
Symbols
You must observe warnings in the manual or on the instrument during all
phases of operation, service, and repair of this instrument. Failure to comply
with these precautions violates safety standards of design and the intended
use of the instrument. Agilent Technologies assumes no liability for the failure
of the customer to comply with these requirements. Table 1 lists the safety
symbols that can appear on Mass Spec Bench.
Table 1 Safety symbols
Description Symbol
See accompanying instructions for more information.
Indicates a hot surface.
Pinch hazard.
Indicates that you must not discard this electrical/
electronic product in domestic household waste.

1 Introduction
8 Mass Spec Bench User Guide
Important Safety Warnings
You must observe safety cautions and warnings during all phases of operation,
service, and repair of Mass Spec Bench. Failure to comply with these
precautions violates safety standards of design and Mass Spec Bench’s
intended use. Agilent Technologies assumes no liability for the failure of the
customer to comply with these requirements.
WARNING
To avoid creating a fire hazard:
• Do not store oil or solvents inside the sound enclosure.
• Do not leave any absorbent materials inside the enclosure to soak up oil.
WARNING
If a temperature alarm malfunctions or if the alarm has been on for an extended
period, Mass Spec Bench and the pump can be dangerously hot. Check that the
Mass Spec Bench and pump are cool before you touch them.
CAUTION
To avoid overheating and possible equipment damage:
•Do not block air flow to the fans while running Mass Spec Bench. Install Mass Spec
Bench with enough space behind it to allow good air intake.
•Mass Spec Bench must not recirculate hot air. Always position the back end of the
Mass Spec Bench where it can draw cool air.
CAUTION
Never run the rough pump(s) without also running Mass Spec Bench fans. Doing so
can significantly damage the LC/MS or GC/MS system when one or both of the rough
pumps turns off.

Introduction 1
Mass Spec Bench User Guide 9
Electromagnetic compatibility
This device complies with the requirements of CISPR 11. Operation is subject
to the following two conditions:
•This device must not cause harmful interference.
•This device must accept any interference received, including interference
that can cause undesired operation.
If you notice harmful interference to radio or television reception, and the
interference stops when you turn off the Mass Spec Bench, do these steps:
•Relocate the radio or antenna.
•Move the device away from the radio or television.
•Plug the device into a different electrical outlet, so that the device and the
radio or television are on separate electrical circuits.
•Make sure that all peripheral devices are also certified.
•Make sure that appropriate cables are used to connect the device to
peripheral equipment.
•Consult your equipment dealer, Agilent Technologies, or an experienced
technician for assistance.
•Changes or modifications not expressly approved by Agilent Technologies
could void the authority of the user to operate the equipment.
Sound emission certification for Federal Republic of Germany
•Sound pressure – Lp < 70 dB according to EN 27779:1991
•Schalldruckpegel – LP < 70 dB am nach EN 27779:1991
Cleaning
To clean the Mass Spec Bench:
1Clean the air intake grates with a damp cloth.
2Wipe out excess oil in the pump enclosure with a cloth. Dispose of dirty
cloths in accordance with local laws or regulations.
3Wipe the outer surfaces with a mild soap solution to remove any oil or dirt.

1 Introduction
10 Mass Spec Bench User Guide
Recycling the Product
For recycling, contact your local Agilent sales office.
Parts Identification
Table 2 lists the contents of the Mass Spec Bench kit. Figure 1 and Figure 2
depict the parts of the Mass Spec Bench.
Table 2 Contents list
Part Quantity Part number
Mass Spec Bench 1 G2581-80100
Power supply 1 5188-1164
User Guide 1 G3215-90001
Figure 1 Mass Spec Bench (front view).
NOTE
See Figure 25 on page 34 for a view of the front panel controls.

Introduction 1
Mass Spec Bench User Guide 11
Figure 2 Mass Spec Bench (rear view).
Fan
Vacuum Pump Hose and
Exhaust Hose Ports
NOTE
Power supply not shown.

1 Introduction
12 Mass Spec Bench User Guide
Site Preparation
Prepare the installation site to meet the criteria in Table 3.
Table 3 Site prep information
Criteria Description
Physical dimensions
Weight 20.5 kg (145 lbs)
Dimensions 129 × 91.4 × 81.2 cm (48 × 36 × 32 inches) (L × W × H)
Power supply
AC input voltage 100 to 240 VAC ±10%
DC output voltage +24 V
Output load
(max.)
1.25 A
Input frequency 47 to 63 Hz
Power
consumption
11 W
Rated current 450 mA
Temperature and humidity ranges
Ambient
temperature
5to35°C(41to95°F)
Humidity 15 to 95%
Altitude ≤ 3353 m (11,000 ft)

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Agilent G3215A Mass Spec Bench User Guide
Agilent Technologies
2
Installation
Step 1. Unpack the Mass Spec Bench 14
Step 2. Prepare the pump tray 18
Step 3. Install the Rough Pumps inside Mass Spec Bench 22
Step 4. Attach the spray chamber exhaust hose 28
Step 5. Connect the power supply 28
Step 6. Verify the installation 29
This chapter describes how to unpack, assemble, and install the rough pumps
inside the Mass Spec Bench.
If possible, position the Mass Spec Bench so that there is room to access the
rear of the instrument for repairs. See Table 3 on page 12 for table
dimensions.
Before you begin, make sure that you have:
•Pump oil pan (p/n G1946-00034)
•Tygon 1/2-inch I.D. exhaust tubing (p/n G1946-80077)
•Utility knife
•Wire cutter
•3/4-inch wrench (Spanner)

2 Installation
14 Mass Spec Bench User Guide
Step 1. Unpack the Mass Spec Bench
The Mass Spec Bench is packaged in a protective cardboard container that is
strapped to a wooden pallet. You must cut the metal shipping straps before
you can remove the unit from the pallet.
1Cut the metal shipping straps using wire cutters or sheet metal snips.
2Remove the outer straps and cardboard box. See Figure 3.
Figure 3 Mass Spec Bench container
WARNING
x
The metal straps have sharp edges. Be careful not to cut yourself.

Installation 2
Mass Spec Bench User Guide 15
3Cut the metal shipping straps that secure the Mass Spec Bench to the
wooden pallet. See Figure 4.
Figure 4 Mass Spec Bench on wooden pallet
WARNING
The metal straps have sharp edges. Be careful not to cut yourself.

2 Installation
16 Mass Spec Bench User Guide
4Remove the upper box that contains the pump tray.
Figure 5 Pump tray box
5Remove the protective plastic film and cardboard edge protectors.
WARNING
This box is heavy and must be lifted by two people.

Installation 2
Mass Spec Bench User Guide 17
6Pull the ratchet handle contained within the castor and turn the ratchet in
a clockwise direction to move up the pad. See Figure 6.
Make sure to retract the pad completely into the castor body. If the ratchet
spins freely, use your finger to hold the gear inside the castor.
The castors contain rubber vibration absorbing pads that are extended to
help secure the Mass Spec Bench to the pallet. Each castor contains a pad.
These pads must be retracted so that the castors touch the floor.
Figure 6 Ratchet handle pulled out
7When all four wheels are touching the pallet, lift the Mass Spec Bench off
the pallet.
Use at least four people (one on each corner of the bench) to lift to the floor.
WARNING
To avoid personal injury, do not try to lift the Mass Spec Bench without assistance.
The bench weighs over 70 kg (155 pounds). Always use good lifting practices
appropriate for the installation.

2 Installation
18 Mass Spec Bench User Guide
Step 2. Prepare the pump tray
The Mass Spec Bench is designed to accommodate up to two pumps in the
enclosure. The pumps must be oriented correctly to ensure proper air flow.
Improper air flow can damage the pumps due to overheating.
Depending upon the configuration, an LC/MS instrument can have a curved
fitting on the end of the vacuum hose. If the hose reaches the pump, the
vacuum hose is properly attached.
Note that these instructions assume a new instrument installation. If this
installation is for an installed instrument, the instrument must be vented
PRIOR to installing the vacuum pumps inside the enclosure.
1Open the cardboard box which contains the pump tray.
2Remove the pump tray surface.
Figure 7 Pump tray surface on top of the pump tray, inside of the pump tray box
WARNING
To avoid personal injury when you lift the pump tray:
• Use two people to lift the tray
• Be careful not to pinch your fingers.

Installation 2
Mass Spec Bench User Guide 19
3Lift the pump tray out of the cardboard box.
4Open the door completely to allow the most working space.
5Make sure you can identify the front of the pump tray.
The front of the pump tray is marked with an F. The front of the pump tray
also has a short lip design. The pump tray must be installed correctly or it
will not fit and will be very difficult to remove once installed.
Figure 8 Front of pump tray
6Tilt the pump tray sideways to fit the tray through the opening of the
enclosure. Then insert the pump tray with the rear tilted back. The two rails
will catch the pump tray. Let the pump tray drop into the front.

2 Installation
20 Mass Spec Bench User Guide
Figure 9 Installed pump tray
7When the pump tray has been installed inside the enclosure, install the
pump tray surface in the pump tray.
Center the pump tray surface as best as possible in the pump tray.
8Peel off the protective film and any stickers from the pump tray surface.
Figure 10 Peeling off the protective film
The plastic may tear when
you are peeling off the
protective film. All of the
protective film must be
removed.