Applied Membranes MYRON L COMPANY Ultrameter III 9PTK User manual

ULTRAMETER
III
™
Operation
Manual
MODEL 9PTK
27 April 11
®
2450 Business Park Dr., Vista, CA 92081 (760) 727-3711
(760) 727-4427
www.appliedmembranes.com [email protected]
Industry Leader in RO Expertise and Membrane Applications since 1983™
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i
THE 9P TITRATION KIT (WITH BLUDOCK OPTION)
COMES WITH EVERYTHING YOU SEE HERE
1
2
3
4
5
678910 11
12 13 14 15 16 17 18 19
20
21
22
PLEASE CHECK THE CONTENTS OF YOUR KIT!
Ultrameter1. III™ Model 9P
Cell Extender2. Model TKCE
Foam-lined hard carry case3.
4. Model FVMP-100
12 disposable pipette tips5.
6. Model ALK-1002OZ
7. Model HARD-2002OZ
8. Model PH42OZ
9. Model PH72OZ
10. Model PH102OZ
11. Model SS2OZ
2oz. bottle of alkalinity Reagent A112. Model H2SO4-12OZ
2oz. bottle of hardness Reagent C113. Model HCL-32OZ
2oz. bottle of hardness Reagent H114. Model NAOH2OZ
2oz. bottle of hardness Reagent H215. Model EDTA-LC2OZ
2oz. bottle of hardness Reagent H316. Model EDTA-HC2OZ
2oz. bottle of ORP ISA Sensor Conditioner17. Model ORPCOND2OZ
2oz. bottle of KCl-700018. Model KCL-70002OZ
2oz. bottle of 442-300019. Model 442-30002OZ
20. Model TPLuNgER
21. Model BDDO
22.
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1
I. INTRODUCTION
III™, one of the
The Ultrameter III
analysis. The Ultrameter III
download the memory or stored test data with its corresponding time,
CSV™.
relying on it.
III
Special note
the left of the Ultrameter III
easily be changed to NaCl.
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II. FEATURES and SPECIFICATIONS
A.
•
•
ORP/Free Chlorine mode selection•
•
• ±1% of / ±0.1% at calibration point
•
•
Waterproof to 1 meter/3 feet•
•
Prompts for easy pH calibration•
Factory calibrations stored in microprocessor•
•
microprocessor
User•
•
•
Memory stores 100 readings•
• Auto OFF
•
accessory package
B.
7.7 x 2.7 x 2.5 in.
Weight 352 g/12.4 oz.
pH/ORP Sensor Well Capacity 1,2 ml/0.04 oz.
Power 9V Alkaline Battery
Protection Ratings IP67/NEMA 6 (waterproof to
1 meter/3 feet)
EMI/EMC Ratings EN61326-1: 2006 + Annex A: 2008
CISPR 11: 2003
IEC 61000-4-2: 2001 and,
IEC 61000-4-3: 2002
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C.
Parameters Ranges Resolution Accuracy
Auto
Temperature
Compensation
Adjustable
Temperature
Compensation
Cond/TDS
Ratios
Prepro-
grammed
Adjustable
Cond/
TDS Ratio
Factor
0-9999 µS/cm
10-200 mS/cm
in 5
0.01 (<100 µS)
0.1 (<1000 µS)
1.0 (<10 mS)
0.01 (<100 mS)
0.1 (<200 mS)
±1% of
reading
0-71ºC
32-160ºF 0-9.99%/ºC
KCl, NaCl,
442™ 0.20-7.99
0-9999 ppm
10-200 ppt
in 5
0.01 (<100 ppm)
0.1 (<1000 ppm)
1.0 (<10 ppt)
0.01 (<100 ppt)
0.1 (<200 ppt)
±1% of
reading
0-71ºC
32-160ºF 0-9.99%/ºC
10KΩ-30MΩ
0.01 (<100 KΩ)
0.1 (<1000 KΩ)
0.1 (>1 MΩ)
±1% of
reading
0-71ºC
32-160ºF 0-9.99%/ºC
pH 0-14 pH ±.01pH ±.01pH 0-71ºC
32-160ºF
ORP ±999 mV ±1 mV ±1 mV
Free
Chlorine 0.00-10.00 ppm 0.01 ppm
<1ppm
±.5ppm
±.2ppm
Alkalinity
Titration 10-800 ppm 0.1(<100 ppm)
1(<800 ppm)
Hardness
Titration
0-1710 ppm
(0-100 grains)
0.1(<100 ppm)
1(<1710 ppm)
LSI
Titration -10 to +10 0.1
Temp-
0-71ºC
32-160ºF 0.1ºC/F ±0.1ºC
The Myron L Ultrameter III
Year Limited Warranty. The pH/ORP sensor has a Six (6) Month Limited
MYRON L COMPANY
2450 Impala Drive
Carlsbad, CA 92010-7226 USA
+1-760-438-2021
www.myronl.com
replacement of the Ultrameter III
no other responsibility or liability.
E. Ultrameter III Model
Ultrameter III Model 9P
PARAMETERS
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PLEASE NOTE:
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TABLE OF CONTENTS
9PTK Contents ............................................i
...................................... ii
...................................1
II. FEATURES and SPECIFICATIONS ....................2
................................2
.....................2
........................3
..........................3
E. Ultrameter III Model .......................3
III. RULES of OPERATION..............................8
A. Operation ...............................8
B. Characteristics of the Keys ..................8
C. Operation of the Keys ......................8
.........8
...........9
3. Alkalinity, Hardness and LSI Keys . . . . . . 9
4. pH and ORP/Free Chlorine Keys ......10
5. CAL/MCLR Key ...................10
.................10
IV. AFTIII ................ 11
......... 11
B. Maintenance of the pH/ORP Sensor.......... 11
...................... 11
A. Parameter Methods....................... 11
B. Titration Methods......................... 11
.................12
...............13
.............. 13
............14
.....................14
......................14
......................16
1. Hardness Unit Selection.............16
........16
...................18
....................19
........19
...........................20
I. ORP and Free Chlorine Modes..............21
1. ORP Mode Selection ...............21
................... 21
............ 22
VI. SOLUTION SELECTION............................22
..........22
.....................23
............23
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..............23
............24
Compensation (Tempco) ........24
2. ...24
....................25
VII. CALIBRATION....................................26
......................26
III .....26
1. Calibration Steps ..................26
2. Calibration Limits ..................27
....................27
.......27
.....28
............... 28
4. Reloading Factory Calibration
................28
5. Alkalinity Calibration................29
6. Hardness Calibration ...............30
7. pH Calibration ....................33
8. ORP Calibration ...................35
............. 35
VIII. CALIBRATION INTERVALS .........................35
......................35
B. Calibration Tracking Records ...............36
............36
Practices .........36
........................................36
A. Memory Storage .........................37
B. Memory Recall ..........................37
C. Clearing a Record/Memory Clear ............ 37
...................................38
A. Setting TIME ............................38
............................39
......40
.....41
..............41
....................................42
......................................43
SER CALIBRATION LINC™ FUNCTION ........44
A. Calibration of Ultrameter III
User mode ..........................44
.........44
C. Canceling User .......46
...........47
A. Software Installation ......................47
.........................47
..................48
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.........................49
....................49
B. Battery Replacement......................50
C. pH/ORP Sensor Replacement ..............50
........................50
.............................52
...................................54
.........54
................54
.................55
.......................55
................55
............ 55
................56
............... 56
I. Replacement pH/ORP Sensor ..............56
J. Pipette Kit with Replacement Tips............56
K. Replacement M’Pet Micropipette ............56
L. M’Pet Micropipette Replacement Tips.........56
Accessory Package ...................56
..................56
A. Standardized to 25°C .....................56
B. Tempco Variation.........................57
..........57
...............58
..........................59
......59
...........................59
...................59
C. When does it make a lot of difference?........60
................60
................61
...61
C. Finding ...61
FREE CHLORINE ......................62
A. pH ....................................62
...64
C. Free Chlorine ...........................65
...................66
A. Alkalinity and Hardness Titrations ............65
B. La .................66
C. Hardness Units ..........................66
.............................67
......................................68
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III. RULES of OPERATION
A. Operation
NOTE: The cell extender does not interfere with normal operation.
Auto off
MS key to store the
reading (ref. Memory Storage, pg. 37). It’s that simple!
B. Characteristics of the Keys
III
CAL
t
pg. 27; and ORP Mode Selection, pg. 21).
C. Operation of the Keys
1.
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2.
Precautions:
a.
of
b. RES Key
A press of
kilohms (KΩ) and 30 megohms (MΩ
only show [- - - -] in the display.
c.
A press of
Selection, pg. 22).
3. Alkalinity, Hardness and LSI Keys
NOTE:
extender.
a. Alkalinity Key
A press of
b. Hardness Key
A press of
c. LSI Key
A press of
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4. pH and ORP/Fr Chl Keys
Maintenance of the pH/ORP Sensor, pg. 11 and Cleaning Sensors, 2.
pH/ORP, pg. 50).
a. pH Key
A press of
right.
b. ORP Key
A press of
5. CAL/MCLR Key
allows
If
SEL
CAL
key.
CAL
3 seconds allows ORP mode selection (ref. pg. 21).
CAL
Once in CAL
MCLR
to allow clearing records (ref. Clearing a Record/Memory Clear, pg.
37).
6.
or
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IV. AFTER USING THE ULTRAMETER III
A.
B. Maintenance of the pH/ORP Sensor
and tap water (ref. pH and ORP Practices to Maintain Calibration, pg.
36). NEVER USE DISTILLED WATER
If all ORP solutions are reporting approximately the same value,
clean ONLY the platinum ORP electrode with an MLC ORP
conditioner-soaked cotton swab, being careful not to touch the
swab to the glass bulb of the pH sensor.
V. SPECIFIC RECOMMENDED MEASURING PROCEDURES
A. Parameter Methods
Selection, pg. 22.
NOTE:
B. Titration Methods
cell extender, and the .
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NOTE:
reagents. Flicking the cap or popping it off can
1.
Always use a clean tip when changing
solutions! To install a tip, press the wide end of
pipette.
NOTE:
positions.
of the
to depress the top of the pipette to the
FIRST STOP. Insert the tip end down into
m/ ⁄". Slowly release the
a sample: With the pipette in the REST
the cell wall or the sample.
100µl CE
Plunger Button
Plunger Rod
Shaft Coupling
Shaft Bottom
Disposable Tip
100 µL
100µl CE
Shaft Coupling
Disposable Tip
100 µL
Rest Position: The
UP.
resistance is felt.
Second Stop: The
Pipette Assembly
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being careful not to
touch the tip to the existing solution.
it
2. T
With the cell extender installed and
against the rim of the cell extender, rotate
the rim of the cell extender.
of the cell extender to dispel any clinging
the cell area.
3.
a. Agitate
AGit
b. Hold
HOLd
down into the cell extender then
rotate it from side to side.
AGit AGit
displays, swing the
and down 3 times.
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Agitate and hold as many times as prompted.
EdTAAGitHOLd
PrES CAL
CAL to
accept readings.
C.
the cell.)
3. Press or
.
condition.
drift from trace contaminants or absorption from atmospheric gasses, so
4. Press
NOTE: If reading is lower than 10 kilohms, display will be dashes:
E.
NOTE:
in the AUTO OFF setting (ref. AUTO OFF, pg. 43). Press ALK to start the
Err
to obtain a reading.
HOLdHOLd
displays, hold the 9P
still with bottom of case
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ide along the rim of the cell extender.
8. Press ALtdS
with the PPM PrES CAL
when the reading stabilizes.
9. Press CAL
Add A1 AGit t1
HOLd t
1
10. Using the pipette, add 100 µL of Reagent: A1, close the cell
PrES CAL
11. Press CAL Add
A1 AGit t2
HOLd.
12.
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CAL as prompted. An alkalinity
MS
ALK.
F.
1. Hardness Unit Selection
PPM3or grains of hardness.
HARD, then press and hold CAL HArdand SELare
displayed. Press UP or DOWN PPM
CAL to accept. This also sets
a clean tip installed, and two extra clean tips.
NOTE:
HARD to
AUTO OFF setting (ref. AUTO OFF, pg. 43).
to slide along the rim of the cell extender.
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