DAIHAN MaXterileTM 47 User manual

Man 202 (13 Aug. 2015)
Steam Sterilizers
Digital Fuzzy-controlled Autoclaves
Certifications by - - -
CE/MDD Marked Products.
ISO 9001 Certified.
PL Insurance.
Validation(IQ&OQ) Service.
Patented(No. 10-0554098) Jog Shuttle Control System.
User Manual
(Version 2.2.1)
written for
MaXterileTM 47/ 60/ 80/ 100
" MaXterileTM 60 "
Steam Sterilizers Digital Fuzzy-controlled Autoclaves, 60 Lit.
Sales & Basic A/S :
By the Nearest Official Distributors.
DAIHAN-Sci.com or ALL for LAB.com Shopping Mall
English Page : P. 11 ~ 27
Korean Page : P. 28 ~ 53

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European Declaration of Conformity
We, DAIHAN Scientific Co., Ltd.,
Daihan Bldg., 24-4, Sangwolgok-dong, Seongbuk-gu, Seoul, Korea,
Tel: [phone], Fax: [phone]
declare that in compliance with the above Directive, that the product(s)
detailed below have been manufactured in accordance with conformity assessment
module A1, “Internal product control with monitoring of final assessment”. (Category II)
Autoclave
1. Item: Vessel of Autoclave
2. Model names: MaXterile 47, MaXterile 60, MaXterile 80
3. Design Pressure: 2.5bar
4. Operation Pressure: 1.2~2 bar
5. Design Temperature: 140℃
6. Operation Temperature: 121 ~ 132℃
7. Hydrostatic Test Pressure: 3.6bar
Applicable Standards/provisions: EN ISO 13485:2003 and the provisions in Annex II of the EC-Directive
93/42/EEC, with the exemption of section 4
Signed: ____________________________ (Eun Taek Shu)
Date: 27, March 2015
Authority: President / CEO
For
DAIHAN Scientific Co., Ltd.,
Daihan Bldg., 24-4, Sangwolgok-dong, Seongbuk-gu, Seoul, Korea.
Tel: [phone], Fax: [phone]
DH-DC08005-R03

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European Declaration of Conformity
We, DAIHAN Scientific Co., Ltd.,
Daihan Bldg., 24-4, Sangwolgok-dong, Seongbuk-gu, Seoul, Korea,
Tel: [phone], Fax: [phone]
declare under our sole responsibility that the product
Autoclave
MaXterile 100
to which this declaration relates is in conformity
with the following standard or other normative document
EN 61326 EN 61000-3-2, EN 61000-3-3
EN 61010-1, EN 61010-2
following the provisions of the directives:
Low-Voltage Directive 2006/95/EC
EMC Directive 2004/108/EC
Signed: ____________________________ (Eun Taek Shu)
Date: 27, March 2015
Authority: President / CEO
For
DAIHAN Scientific Co., Ltd.,
Daihan Bldg., 24-4, Sangwolgok-dong, Seongbuk-gu, Seoul, Korea.
Tel: [phone], Fax: [phone]
DH-DC10037-R03

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Table of Contents
Page
1. General
1.1 Precautions Before Use ............................................................................ 5
1.2 Product Introduction ................................................................................ 6
1.3 Product Configuration .............................................................................. 7
2. Installation
2.1 Product Installation .................................................................................. 8
2.2 Product Specifications ............................................................................ 10
3. Product Usage
3.1 Product Usage ........................................................................................ 12
3.2 Names of Each Part ................................................................................. 15
3.3 Usage Instructions .................................................................................. 18
4. Products Management Methods
4.1 Accessories ............................................................................................ 24
4.2 Maintenance and Management ................................................................ 25
4.3 Troubleshooting ...................................................................................... 26
5. Product Assurance
5.1 Quality Assurance ................................................................................... 27

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1
1
I
N
1. General
1.1 Precautions Before Use
Thank you for purchasing the Steam Sterilizers Digital Fuzzy-controlled
Autoclaves.
This manual describes the performance and usage instructions of the product, and the
precautions in the handling. Please carefully read this manual, before using the
product. The following warnings should be strictly adhered to: (The following warning
sign is marked in the part that is required user attention, so please safely use the
product after being well-acquainted with the meaning.)
Warning
Failure to follow the instructions may result in injury.
Caution
Failure to follow the instructions may result in product failure.
Proximity Caution
Keep clear of the product during use.
Notification
Do not disassemble or modify the product or use it for purpose other than its
intended function.
Caution: High Temperature
High-temperature heating, pose a risk of burns.
Danger of Explosion
If volatile, explosive chemicals are used, there is a danger of explosion.
This symbol indicates Protective earth (ground).
This symbol indicates power “OFF” on the power on/off switch.
This symbol indicates power “ON” on the power on/off switch.
This symbol indicates the connection point of the neutral conductor on the
installed unit.
This symbol indicates alternating current Voltage.

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1. General
1.2 Product introduction
The temperature control method of this product is Fuzzy control method, and the maximum
power is supplied nearby the set temperature, and it has been designed so that excellent
temperature safety is maintained, at the same time that the power supplied to the heater is
properly controlled and the temperature deviation is minimized after reaching to the setting
temperature. This product was developed and manufactured considering the best possible ease
for use and safety, and has the following features.
-The exact control by a Digital Fuzzy Controller is provided.
-Because Jog Dial Knob and Push Button which are rigid and have excellent operability are
mounted, this product has high operating sensitivity and excellent accuracy.
-This product is equipped with the emission steam condensation mechanism, so steam is not
generated from the sterilizer after the sterilization operation, and the safety and
convenience are provided to the user.
-The stainless steel material processed by a press is used in order to maintain the aesthetics
of Chamber and the high level of hermeticity, and the outside overheating of the equipment
is protected against in the maximum limit by using the advanced insulator.
-The sterilization environment optimized by the Liquid-/Solid-Cycle Mode selectable
according to the form of sample is provided.
-Because this product is equipped with a high-quality LCD Display with back-light function, it
is easy to confirm its state.
-The safety device for overheating prevention, and over current and short circuit prevention
circuitry that preferentially consider the user’s safety are mounted.
-When it reaches at the sterilization time, Buzzer is operated for 30 seconds and it gives the
convenience to the user.
-“One-touch Lever Type Sliding Door” which anyone can easily open and close the door is
mounted in this product.
-Because this product is equipped with the Safety Electronic Door Closing System which is
not opened for safety during operating, and the door is not opened at the temperature of
80℃or more, and the safety for the user is provided.
-Two Wire Baskets suitable to each Model are supported.
-The safety is demonstrated by the safety certification of CE-MDD(Medical Device Directive)
medical devices.
-PL(Product Liability) Insurance

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1. General
1.3 Product Configuration
Component Photo
Component Name
No. of Configuration
MaXterileTM
47/60/80/100,
Steam Sterilizers, Digital
Fuzzy-controlled Autoclaves
1 Unit
Wire Basket Set
2 ea
Heater Cover
1 ea
Drain Bucket
1 ea
- Including a copy of the Operation Manual
* Model
-MaXterileTM 47 : Steam Sterilizers, Digital Fuzzy-controlled Autoclaves, 47Liter.
-MaXterileTM 60 : Steam Sterilizers, Digital Fuzzy-controlled Autoclaves, 60Liter.
-MaXterileTM 80 : Steam Sterilizers, Digital Fuzzy-controlled Autoclaves, 80Liter.
-MaXterileTM 100 : Steam Sterilizers, Digital Fuzzy-controlled Autoclaves, 100Liter.

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2. Installation
2.1 Product Installation
* Caution of Installation
1. Please be careful when transporting the product because it is heavy.
2. Please do not lay the product on the floor or subject it to shock. It can cause damage inside
the product.
3. Please install the product in a hard, flat, and stable place.
4. Please do not install the product in a place where it is exposed to direct sunlight, or in the
dangerous places.
5. To minimize the risk of short circuits, do not install the product (in the) places where it will
be subjected to the inflow of moisture or organic solvents on the regulator part or inside of
the body.
6. This product was manufactured for normal operation at a rated voltage, so please check the
voltage status before installing the product.
7. When installing and using the product, please certainly use the power cord provided with
the products.
* Installation Process
1. After receiving the unit and putting it on the specified place of use remove the wrapping.
2. After positioning the unit, lock the moving wheel in order to make position fixed and the
unit stable.
3. Check the unit whether there are eventual transport damages or not. In case there are
some transport damages found please inform the forwarder and your contractor. If there is
no damage, please go to next point 3.
4. Let the unit stand for a few minutes so that the all the internal parts and components of the
unit can be stabilized.
5. Open the door at the left side of the unit. You can find a room for pipe assembly and
electric distribution plane. Please check carefully if there is anything wrong including
disconnection of the electric wire, breakage of pipe or fitting element. In case there is any
kind of damage found, please inform the forwarder and your contractor. If you cannot find
anything wrong, please go to next point 5.
6. For normal use of the unit, confirm that the valve is open, and water drain valve is closed.
7. Connect the main power cord to the socket.
8. (NOTE) If you bye MaXterileTM 80R or MaXterileTM 100R, power consumption of the heater
in the vessel is too high to use normal wall socket. (Typical wall socket in EU and Asian
countries permits around 3kW maximum per socket) So, a big 3-pole plug (for single-phase
230V AC with ground) comes with power cord, and a socket with wiring connector is
supplied together as seen in the picture on the page 10. You have to wire the power supply
line of enough electric power (4kW for MaXterileTM 80R and 5kW for MaXterileTM 100R at
least) to the supplied connector before plugging.
9. If such a big power supply line is not available in the room where the unit is installed, you
have to contact the appropriate person who is in charge of electric facilities in your
company or organization.
2
2

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* Safety Symbols on a product
-Safety symbols stickers Attached to side of product. For meaning of each symbol, please
refer to Precautions Before Use, Safety Instructions.
-Product Liability (PL) Insurance Admission
DAIHAN Scientific (Co., Ltd.) is a member of Product Liability Insurance (PL
Insurance), so that its customers can trust our products, (believe and use its
products,) by preparing against the accident which can be occurred during using the
products by self-production.
[Contents] ………………………………………………………………………………………
Insurance Type: Product Liability Insurance
Publishing Office: Machinery Insurance Cooperative
Limit of Indemnity: 100 million won for Persons and Objects
Secured Area: Worldwide (excluding North America)
Emergency Contact: DAIHAN Scientific (Co., Ltd.) (TEL: [phone], FAX: [phone])
(TEL: [phone], FAX: [phone])
Safety symbols on units, for further
description of each symbol, please
refer to 3.1 Precautions for Use

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2. Installation
2.2 Product Specifications
Model
MaXterileTM
47
MaXterileTM
60
MaXterileTM
80
MaXterileTM
100
Capacity
47 Lit.
60Lit.
80Lit.
100Lit.
Temp. Range &* Accuracy
Ambient 5℃to 132℃, ± 0.5℃at 121℃
Pressure & Gauge
1.2 kgf/cm2at 121℃/ 2.0 kgf/cm2at 132℃, 0~3 kgf/cm2
Sterilization mode
Solid - or Liquid-mode
Heating Power/Consumption
2kW
3kW
2kW x 2
2kW x 2
Timer & Alarm
60 min, Error status & Timer-end
Display
Display LCD Display with Back-Light Function
Controller
Display Fuzzy-Control System (Fully Automatic)
Door & Closing System
Lever-type Sliding Door / Safety Electronic Door Closing System
Safety Circuit
Over-Temp./-Pressure/-Current protection, Sensor Error Detection
Material
Stainless Steel (#304)-Pressure Vessel, Powder Coated Steel-External
Basket
2ea of Stainless Steel Wire Baskets are Included
Basket Dimension(mm)
Φ270 x h240
Φ320 x h240
Φ370 x h240
Φ420 x h240
Dimension
(wxdxh)
Inner(mm)
Φ300 x h670
Φ350 x h650
Φ400 x h650
Φ450 x h630
Outer(mm)
680x470x880
680x470x900
780x580x900
780x580x900
Packing Size (mm)
800x700xh1,280 mm
940x800xh1,350 mm
Gross Weight (kg)
116 kg
120 kg
173 kg
173 kg
Power Supply
1Phase - AC 120V, 60Hz or
- AC 230V, 50/60Hz
1Phase - AC 120V, 60Hz or
- AC 230V, 50/60Hz
3 Phase with Terminal Block

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Functional Block Diagram

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3. Product Usage
3.1 Precautions for Use
Be careful to operate the device.
You must read this manual carefully and completely before using.
The device should only be operated by laboratory personnel especially trained for
this purpose and familiar with all precautionary measures required for working in
a laboratory.
If unexpected sound, smell or smog is generated after connecting electric power,
pull out the main plug and contact manufacturer or a supplier.
Only demineralised or distilled water must be used. If dirty water is used, it will
cause damage of all the components inside the vessel, inner surface of the vessel,
pipes, fittings and valves.
Prior to sterilization, check sterilizing chamber to ensure there is sufficient feed
water. No sterilization without feed water!
Autoclaves have been designed for the following purposes;
For sterilizing glassware, rubber items, pipette tips, instruments, filter bodies,
as well as consumables, waste in bags, and to destroy infectious or septic
materials.
For sterilizing liquids, solutions and culture mediums in open or lightly closed
vessels.
For sterilizing foodstuffs
For streaming liquids or for dissolving agar.
For non-pressurized disinfection of heat-sensitive culture media and solutions.
Liquids and foods must not be sterilized in pressure-sealed containers.
Easily combustible or toxic liquids must no be sterilized
Destruction bags must be open during sterilization, otherwise they may burst.
Before every sterilizing operation, check that the lid stiffener on the lid has moved
all the way into the lid clamp.
And check the lid screw handle is turned until it cannot be turned anymore.
Allow chamber pressure gauge to slow zero before opening the autoclave.
OPT sensor (SAFETY) knob should be set as operating temperature +20 ~ +30C.
Please be noted that the heater doesn’t work if the knob is set to 0 position.
Please avoid ultrasonic lamps.
The unit could be cracked or faded.
3

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You must wear the following protective items when opening the sterilizing chamber
and removing the sterilized articles;
-Apron
-Eye protectors
-Heat insulated gloves
Watch for hot surfaces and hot steam!
After sterilizing liquids;
-Danger from retardation of boiling.
-For open vessels containing up to 1 liter: wait at least 2.5 hours
-For open vessels containing up to 2 liters: wait at least 3 hours
-Do not remove flasks or bags until the chamber temperature drops below
70C.
Disconnect the power supply plug if the unit is not going to be used for an
extended period of time.
Step back when opening the sterilizer.
Do not put any objects insides.
When an object that is easy to be combustible is like a stone, a metal or paper
goes insides, it may cause a fire, an electric shock or a break down.
If do, pull out the mains plug from a socket and contact a manufacturer or a
supplier.
Do not disassemble or remodeling by yourself.
It may cause damage to the designed safety.
We do not have any duties for an accident, quality deterioration or a defect caused
by a customer.
All the mechanisms and electric/electronic devices in this machine are designed
and developed by the manufacturer. The devices could be disassembled and
serviced only by the engineers of manufacturer or by engineers approved by
manufacturer.
Please avoid ultrasonic lamps.
The unit could be cracked or faded.
Watch for hot steam and hot water.
Hot steam may escape when the lid is opened.
The lid handle should only be gripped at the experiment end.
Do not use outdoors avoid overheating or electrical faults. The use in the place
where the sun continuously shines and can get rained on it is prohibited. It may
cause overheating or electrical fault of the product.

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Please do not use flammable or volatile products in the vicinity of the product to
minimize the risk of firer. Please do not use the flammable spray such as lacquers
and paint, or volatile, flammable chemicals and its similar product, in the
proximity of the product. They may cause the ignition due to the spark of switch.
This product must be connected to a properly grounded power supply.
Only operate unit after checking the safety of the unit.
If unexpected sound, smell or smog is generated, pull the main plug out from the
wall socket and contact the technical assets of DAIHAN Scientific
Do not touch the device with wet hand while operation.
Do not turn on and off frequently. It could damage the compressor by overload.
Do not use tap water!
The following products are not suitable for sterilization;
Wooden items
Bonded parts
Plastic materials sensitive to hot water (e.g., screw tops)
Electrical equipment
Vessels or instruments made from steel or iron
Metering equipment, unless their suitability for stream sterilization is
specifically mentioned
Do not open sterilizing chamber until full sterilization operation cycle is finished.
When sterilizing liquids, do not fill vessels more than two-thirds full, as otherwise
liquids may boil over.
Do not sterilize pressure-sealed vessels. Explosion hazard!
Watch for broken glasses!
Do not hang onto or lean against the open lid. DO not climb onto the autoclave,
as this may cause the autoclave to tilt.
This Symbol indicates that this product is to be collected separately.
The following apply only to users in European countries:
This product is designated for separate collection at an appropriate collection
point. Do not dispose of as household waste.
This product is required to comply with the European Union’s Waste Electrical &
Electronic Equipment(WEEE) Directive 2002/96/EC
※All of the circuits, electrical or mechanical parts and configurations used in this product are
the technical assets of DAIHAN Scientific (Co., Ltd.). Only technicians of the technical support
team at DAIHAN Scientific (Co., Ltd.) or technicians approved through the education from
DAIHAN Scientific should be allowed to repair this product.

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③
⑤
⑥
④
⑦
3. Product Usage
3.2 Names of Each Part
Outside
NO
Names
Description
①
Leakage Breaker
Circuit Breaker
②
Power Switch
Power ON/OFF
③
Lever
Door Safety Lock and easy open
④
Lid Clamp
Door Locking
⑤
Control Panel
LCD Display
⑥
Pressure Gauge
manometer
⑧
Moving Wheel
Transport Device
<Table.3.2.1> Names of each part and description
①
②
< Figure 3.2.1> Steam Sterilizers Digital Fuzzy-controlled Autoclaves,
" MaXterileTM 80 "
< Figure 3.2.3>Back of "MaXterileTM 80 /100"
<Fig.3.2.2> Back of "MaXterileTM 47 /60"

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Inside
NO
Names
Description
⑧
Door Fastener
Door locking mechanism
⑨
Safety Knob
Prevent overheat
⑩
Manual purge valve
pressure pass Control Device
⑪
Water Drain Valve
Drain Control Device
⑫
Condenser
emission steam condensation mechanism
< Figure 3.2.4> Side of " MaXterileTM "
< Figure 3.2.5> Inside of " MaXterileTM "
<Table.3.2.2> Names of each part and description
⑧
⑨
⑩
⑪
⑫

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Controller
NO
Names
Description
①
LCD
Display Set-up Value and Current Status.
②
LED Lamp
Indicate operation of TIMER, HEAT, ERROR.
③
MAIN Button
Convert into mode of Timer, Heating, Printer, Locking.
④
SUB Button
Convert into mode of delay timer, offset function, Setting
Operating Information.
⑤
OPEN
Door open.
⑥
Jog Dial knob
Control that Reduces or Adds Values, and Does Start/Stop
Operation.
Time SV 00:00
Time PV 00:00
<Table 3.2.3> Controller for " MaXterileTM "
①
②
③
④
⑤
⑥
<Figure 3.2.6> Controller for Steam Sterilizers Digital Fuzzy-controlled Autoclaves, " MaXterileTM "

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3. Product Usage
3.3 Usage Instructions
-The SAFETY Knob is set for the user’s safety to the appropriate value at the time of the
factory shipment, so please do not change the Knob.
-When turning ON the power of this product, please turn ON the Main Power Switch,
after necessarily turning ON the Leakage Breaker located at the bottom of the rear
panel of this product.
-When the power is turned on, press the "OPEN" Button, and open the Door by pulling
the Lever.
-Check the level of distilled water in the pressure vessel, and please regulate to the level
that Heater Cover can be sunk.
* Operation method for Jog-Dial
-Jog-Dial can be manipulated for the setting in each mode by Turning and Push motion.
-If turning the Jog-Dial knob to clockwise or counter-clockwise, the setting values can be
adjusted, and if briefly pressing once the PUSH button, the Start or the Stop operation is
performed.
-The Turning of the Jog-Dial knob does not manipulated during operating, and if resetting
the set value, it can be adjusted by the Jog-Dial knob after stopping the product by
pressing briefly once the PUSH button.
-If pressing for 2 or 3 seconds the PUSH button, the set value is saved, and even if the
power is turned on again, that value is maintained. (If “0” value is saved, the setting
value is initialized.)
①MAIN - Set Operation Time
-When the power is turned ON, the initial screen is the setting mode of the Timer set mode.
-TIMER LED is lighted during the operation of timer, and indicates that it is operating.
-The range of setting time is from 00:00 to 99hr and 59min (it is possible to adjust at 1min.)
and 00:00 indicates continuous operation..
< Fig 3.3.1. Set Operation Time Mode >
Time SV : 00:00
Time PV : 00:00
Set Time
Remain Time
Timer LED (Green)

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-If the timer operation is completed, the alarm will sound and heating will be stopped.
-The timer setting mode can be operated by referring to the jog-shuttle operation method.
* SUB - Set Delay Time
-If pressing the SUB button in the Set Operation Timer Mode, it is switched to the Set
Delay Time mode.
-The Delay Timer sets the reservation time and has the function that sets so that the
operation of Heating and Timer are performed after that time is elapsed.
-The proper use of the delay timer is to manipulate so that the reservation time is set for the
first time, and then the temperature and the operation timer is set and the set operation is
automatically operated after the reservation time is elapsed.
-The reservation time value is displayed over blinking on the display, and if pressing the
PUSH button by setting the reservation time value with the Jog-Dial knob, the value is fixed
on the Display, and the reservation timer is activated.
-After setting the reservation timer value, you can set-up the operation timer value by
pressing the MAIN button and then press Start button. And, you can set-up the temperature
by pressing the MAIN button again, and then press Start button. The Start button in the
condition that the reservation timer has been set-up, is the button for the operation of the
setting value after the reservation timer, not to immediately operate.
-As described above, if continuously setting the operation, Heating and Timer are operated
after the set reservation time as user intend.
-Since the delay timer is not set during the operation of Heating/Timer, the delay timer
should be set after stopping the operation of Heating/Timer.
-You can change or save the setting by using the operation method of the Jog-Dial, and
Start/Stop of operation can be performed.
-If pressing MAIN button, it is switched to the Set Operation Time Mode.
< Fig 3.3.2. Set Delay Time Mode>
DTim SV : 00:00
DTim PV : 00:00
Set Time
Remain Time
Timer LED (Green)

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②MAIN - Set Temperature
-If pressing once the MAIN button in the Set Operation Time Mode, it is switched to the
temperature setting mode.
-The setting temperature is entered by turning the Jog-Dial Knob to clockwise or counter-
clockwise. If the setting value is entered to above 0℃, the operation standby state is
displayed while blinking the HEATING indication of LCD Display.
-The HEATING indication of LCD Display is always displayed during the operation of
HEATING, and if the setting value is entered to above 0℃in the condition that the heating
is stopped, the HEATING indication indicates the standby status while blinking in long
interval.
-The range of the setting temperature is adjustable in the unit of 1℃, and can be set up to
132℃.
-You can change or save the setting by using the operation method of the Jog-Dial, and
Start/Stop of operation can be performed.
* SUB - Offset Temperature
-If pressing the SUB button in the Set Temperature mode, it is switched to the Set
Temperature Offset mode.
-Temperature compensation is the function that can add or reduce the constant value by
setting the compensation value in the case that user must experiment by matching the
thermometer which he/she is using as the experimental standard and the thermometer
indicated in this regulator.
-The scope of the compensative value is -10.0℃~ +0.0℃, and it is possible to adjust at 0.1℃
unit.
< Fig 3.3.3. Set Temperature Mode >
Temp SV : 0 ℃
Temp PV : 2 7 ℃
Heating LED (Red)
Set Temp
Present Temp
< Fig 3.3.4. Set offset value Mode>
Temp PV : 27.0 ℃
offset : 0.0 ℃
Heating LED (Red)
Present Temp
offset Temp