MBRAUN LABmaster pro sp User manual

Inertgas-Systems
§Workstation LABmaster pro sp / dp
§Gas purifier MB-20-G / MB-200G-W
§MOD box MB200MOD
with touch panel TP700
Operating Manual
Document number: 2611275-EN V5.0 • 12/04/2018
Sales number: 1501101 ... 1501132 (LABmaster), 1500111 (MB-20-G), 1500114 (MB-200G-W), 1500050 ...1500092
(MOD Box)

MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
Legal information
Operating Manual
§Workstation LABmaster pro sp / dp
§Gas purifier MB-20-G / MB-200G-W
§MOD box MB200MOD
with touch panel TP700
M. Braun Inertgas-Systeme GmbH
Dieselstr. 31
85748 Garching
Germany
Website: www.mbraun.de
Phone: [phone]
Fax. [phone]
Email [email protected]

Table of Contents
Document number: 2611275-EN Sales number: 1501101 ... 1501132 (LABmaster), 1500111 (MB-20-G), 1500114
(MB-200G-W), 1500050 ...1500092 (MOD Box)
MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
Page
1
Table of Contents
1 General information ...................................................................... 1- 1
1.1 Entries referring to the system .................................................... 1- 1
1.2 Scope of delivery .......................................................................... 1- 1
1.3 Type plate ...................................................................................... 1- 2
1.4 Liability........................................................................................... 1- 3
1.5 Warranty......................................................................................... 1- 4
1.6 Modifications ................................................................................. 1- 4
1.7 Service address............................................................................. 1- 4
1.8 Included description of optional features................................... 1- 5
1.9 About this operating manual ....................................................... 1- 6
1.9.1 General............................................................................1- 6
1.9.2 Availability of instructions ................................................1- 6
1.9.3 Safety warnings in this manual........................................1- 6
1.9.4 Conventions used in this manual ....................................1- 7
1.9.5 Units used........................................................................1- 8
1.9.6 Terms used......................................................................1- 8
1.9.7 Abbreviations...................................................................1- 9
1.9.8 Glossary ........................................................................1- 10
1.9.9 Disclaimer......................................................................1- 11
2 Inert gas technology ..................................................................... 2- 1
2.1 Overview ........................................................................................ 2- 1
2.2 Components .................................................................................. 2- 2
2.2.1 Glovebox .........................................................................2- 2
2.2.2 Antechamber ...................................................................2- 6
2.2.3 Gas purifier......................................................................2- 9
2.2.4 System control...............................................................2- 11
2.2.5 Vacuum pump ...............................................................2- 13
2.3 Functional description................................................................ 2- 14
2.3.1 Gas flow general............................................................2- 14
2.3.2 Single reactor systems (sp)...........................................2- 16
2.3.3 Optional: double purifier (dp).........................................2- 17
2.3.4 Optional: solvent filter....................................................2- 17
2.3.5 Box pressure control......................................................2- 19
2.3.6 Vacuum antechamber ...................................................2- 22
2.4 MBRAUN standard platforms..................................................... 2- 25
2.4.1 MB-20-G and MB-200G-W............................................2- 25
2.4.2 LABmaster pro workstation ...........................................2- 25
2.4.3 MOD box systems .........................................................2- 26
2.4.4 Technical data ...............................................................2- 26
2.4.5 Noise level.....................................................................2- 28
2.4.6 On-site conditions..........................................................2- 28
3 Safety ............................................................................................. 3- 1
3.1 Intended use .................................................................................. 3- 1
3.2 Improper use ................................................................................. 3- 2
3.3 Statement of the manufacturer .................................................... 3- 3

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MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
3.4 Qualification of personnel............................................................ 3- 4
3.5 Duties of the operating personnel............................................... 3- 4
3.6 Duties of the operating company ................................................ 3- 5
3.7 Behaviour in case of emergency ................................................. 3- 6
3.8 Process materials ......................................................................... 3- 6
3.8.1 Classification and assessment of substances.................3- 6
3.8.2 MBRAUN-Hazard classes ...............................................3- 7
3.8.3 Examples of a rough classification ..................................3- 9
3.9 Safe handling of solvents, chemicals and gases..................... 3- 11
3.10 Controller ..................................................................................... 3- 12
3.11 Gas purifier regeneration ........................................................... 3- 12
3.12 Regenerative solvent filter ......................................................... 3- 12
3.13 Residual risks.............................................................................. 3- 12
3.13.1 Risk of overpressure and negative pressure.................3- 12
3.13.2 Risk of electrical hazard ................................................3- 13
3.13.3 Risk of suffocation .........................................................3- 14
3.13.4 Risk of combustion and explosion.................................3- 14
3.13.5 Risks when operating a damaged system.....................3- 14
3.13.6 Risk of environmental damage......................................3- 14
3.14 Safety symbols affixed to the inert gas system ....................... 3- 15
4 Transport, installation and commissioning................................ 4- 1
4.1 Transport ....................................................................................... 4- 1
4.1.1 Important transport labels................................................4- 1
4.1.2 Storage conditions...........................................................4- 2
4.1.3 Long-haul carriage ..........................................................4- 2
4.1.4 On-site transport and unpacking .....................................4- 2
4.1.5 Moving a glovebox...........................................................4- 4
4.1.6 Moving a gas purifier .......................................................4- 6
4.1.7 Moving a LABmaster .......................................................4- 8
4.1.8 Rolling the equipment into position ...............................4- 10
4.2 Installation ................................................................................... 4- 10
4.2.1 Definition of the clean room volume ..............................4- 11
4.2.2 Preparing the site ..........................................................4- 12
4.2.3 Media supply overview .................................................4- 14
4.2.4 System cooling ..............................................................4- 20
4.2.5 Installation vacuum pump..............................................4- 21
4.2.6 Connecting the system..................................................4- 21
4.2.7 Installation of the analysers...........................................4- 29
4.2.8 Final inspection..............................................................4- 30
4.3 Commissioning ........................................................................... 4- 30
4.3.1 Switching on the system................................................4- 30
4.3.2 Inertisation of the glovebox ...........................................4- 31
5 Human machine interface ............................................................ 5- 1
5.1 Introduction ................................................................................... 5- 1
5.2 Touch panel ................................................................................... 5- 1
5.3 Explanation of symbols and colours .......................................... 5- 2
5.4 Start screen ................................................................................... 5- 4

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MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
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5.5 Screen components...................................................................... 5- 6
5.6 Functions screens ........................................................................ 5- 6
5.7 Alarm screen ................................................................................. 5- 7
5.8 Menu Screen selection screen..................................................... 5- 8
5.8.1 Parameter screens ..........................................................5- 8
5.8.2 Trend screens..................................................................5- 9
5.8.3 Service screen...............................................................5- 10
5.9 User level / password concept................................................... 5- 13
5.9.1 Logon.............................................................................5- 13
5.9.2 Logout............................................................................5- 14
5.10 Default parameter values ........................................................... 5- 14
6 Operating mode principles........................................................... 6- 1
6.1 Service book.................................................................................. 6- 1
6.2 Starting up the system ................................................................. 6- 1
6.3 Gas purifier operating modes ...................................................... 6- 3
6.4 Glovebox operating modes.......................................................... 6- 4
6.5 Antechamber operating modes ................................................... 6- 4
6.6 Shut down system ........................................................................ 6- 4
7 Gas purifier operation................................................................... 7- 1
7.1 Safe operation ............................................................................... 7- 1
7.1.1 Parameter limits...............................................................7- 1
7.1.2 Select regeneration gas hydrogen concentration............7- 1
7.1.3 Solvent and solvent filters ...............................................7- 1
7.2 Navigation overview ..................................................................... 7- 2
7.2.1 Purification unit................................................................7- 2
7.2.2 Analysers.........................................................................7- 5
7.2.3 Regenerative solvent filter (optional)...............................7- 6
7.3 Circulation ..................................................................................... 7- 8
7.3.1 Manual activation and deactivation .................................7- 8
7.3.2 Automatic circulation activation .....................................7- 12
7.4 Solvent filter operation (optional).............................................. 7- 13
7.4.1 Manually operated solvent filters (activated carbon only)
.......................................................................................7- 13
7.4.2 PLC-controlled solvent filters.........................................7- 14
7.4.3 Solvent analyser (optional)............................................7- 16
7.5 Regeneration operation.............................................................. 7- 16
7.5.1 Regeneration sequence ................................................7- 17
7.5.2 Reactor regeneration.....................................................7- 18
7.5.3 Solvent filter regeneration .............................................7- 21
7A ECO Mode ....................................................................................7A- 1
7A.1 Overview ......................................................................................7A- 1
7A.2 Glovebox operation with the ECO Mode feature......................7A- 1
7A.2.1 Regeneration................................................................ 7A- 2
7A.2.2 Dedicated vacuum pumps for antechamber................. 7A- 2
7A.3 Safety ...........................................................................................7A- 3

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MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
7A.4 Operation .....................................................................................7A- 3
7A.4.1 Navigation..................................................................... 7A- 3
7A.4.2 Parameters................................................................... 7A- 4
7A.4.3 Reduced Blower speed ................................................ 7A- 5
7A.4.4 The different blower speeds ......................................... 7A- 6
7A.4.5 Vacuum pumps............................................................. 7A- 7
7A.4.6 Antechamber with dedicated vacuum pump ................ 7A- 7
7A.4.7 Box light........................................................................ 7A- 8
8 Glovebox or enclosure operation................................................ 8- 1
8.1 Overview ........................................................................................ 8- 1
8.2 Safe operation ............................................................................... 8- 1
8.2.1 Overpressure safety ........................................................8- 2
8.2.2 Harmful or hazardous process materials.........................8- 2
8.2.3 Process-related particle formation...................................8- 2
8.2.4 Mechanical hazards.........................................................8- 3
8.2.5 Reactor damage by ambient air ......................................8- 3
8.3 Inertisation..................................................................................... 8- 3
8.4 Working with gloves and glovebreaks........................................ 8- 4
8.5 Monitoring gas concentration...................................................... 8- 5
8.5.1 Display H2O and O2 concentration.................................8- 5
8.5.2 Glovebox trend screen ....................................................8- 6
8.5.3 Activation and deactivation of analysers .........................8- 7
8.5.4 Analyser operating hours ................................................8- 8
8.6 Setting glovebox parameters....................................................... 8- 8
8.7 Activation / Deactivation of glovebox functions ...................... 8- 10
8.8 Glovebox during circulation ...................................................... 8- 10
8.8.1 Glovebox pressure ........................................................8- 11
8.8.2 Rough leakage detection...............................................8- 12
8.8.3 Solvent vapours in glovebox atmosphere .....................8- 12
8.9 Glovebox during regeneration................................................... 8- 13
8.10 Glovebox purge........................................................................... 8- 13
8.10.1 Manually start and stop .................................................8- 15
8.10.2 Automatic start and stop................................................8- 15
8.11 Additional function and equipment from MBRAUN................. 8- 17
8.11.1 Additional equipment.....................................................8- 17
8.11.2 Additional safety equipment ..........................................8- 18
8.12 Operating company’s process equipment ............................... 8- 18
8A O2 and H2O analysers ................................................................8A- 1
8A.1 Overview of a O2 and a H2O analyser.......................................8A- 1
8A.2 Safety ...........................................................................................8A- 2
8A.2.1 Intended use................................................................. 8A- 2
8A.2.2 Improper use MB-OX-SE1............................................ 8A- 2
8A.2.3 Improper use of the moisture analyser......................... 8A- 2
8A.3 Oxygen analyser .........................................................................8A- 2
8A.3.1 Description.................................................................... 8A- 2
8A.3.2 Technical data .............................................................. 8A- 3
8A.3.3 Installing the oxygen analyser ...................................... 8A- 3
8A.3.4 Maintenance................................................................. 8A- 4

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MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
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8A.4 Moisture analyser........................................................................8A- 4
8A.4.1 Description.................................................................... 8A- 4
8A.4.2 Technical data .............................................................. 8A- 5
8A.4.3 Installing the moisture analyser.................................... 8A- 5
8A.4.4 Maintenance for the H2O analyser............................... 8A- 6
8A.4.5 Storing an MB-MO-SE1 analyser ............................... 8A- 10
8A.5 Mounting an analyser ...............................................................8A- 10
8A.6 Disassembling or replacing the analyser ...............................8A- 11
8A.7 Returning analysers to MBRAUN ............................................8A- 12
8A.7.1 Return service ............................................................ 8A- 12
8A.7.2 Returning a faulty analyser......................................... 8A- 12
8A.7.3 Returning an analyser for calibration.......................... 8A- 14
8A.8 Declaration about Decontamination.pdf .................................8A- 15
8B Freezer .........................................................................................8B- 1
8B.1 Overview ......................................................................................8B- 1
8B.2 Specifications..............................................................................8B- 2
8B.3 Operation .....................................................................................8B- 2
9 Antechamber operation (Vacuum antechamber) ....................... 9- 1
9.1 Safe operation ............................................................................... 9- 1
9.2 Vacuum pump ............................................................................... 9- 2
9.3 Antechamber door operation....................................................... 9- 2
9.3.1 Main antechamber...........................................................9- 3
9.3.2 Mini antechamber............................................................9- 4
9.4 Manual loading and unloading of the mini antechamber.......... 9- 6
9.4.1 Transferring material in....................................................9- 6
9.4.2 Transferring material out .................................................9- 8
9.5 PLC-controlled loading and unloading ....................................... 9- 9
9.5.1 Touch panel navigation .................................................9- 10
9.5.2 Parameters....................................................................9- 12
9.5.3 Trend curve ...................................................................9- 14
9.5.4 Antechamber cycle operation........................................9- 14
9.5.5 Loading and unloading ..................................................9- 17
9.6 PLC-controlled door interlock ................................................... 9- 17
9.7 Optional antechamber features ................................................. 9- 20
10 Additional equipment ................................................................. 10- 1
10.1 Introduction ................................................................................. 10- 1
10.2 Safety ........................................................................................... 10- 1
10.3 Additional options....................................................................... 10- 1
10.3.1 Optional glovebox equipment........................................10- 2
10.3.2 Optional antechamber equipment .................................10- 4
10.4 Customer-specific components ................................................ 10- 4
10.5 Equipment from other manufactures ........................................ 10- 4
10A myMBRAUN App .......................................................................10A- 1
10A.1 Setting up the myMBRAUN app...............................................10A- 1
10A.1.1 Prerequisites............................................................... 10A- 1

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10A.1.2 Preparatory steps ....................................................... 10A- 1
10A.1.3 Main menu of the app................................................. 10A- 1
10A.1.4 Registering ................................................................. 10A- 2
10A.2 Functions ...................................................................................10A- 7
10A.2.1 Settings....................................................................... 10A- 7
10A.2.2 Monitoring................................................................... 10A- 8
10A.2.3 Information................................................................ 10A- 11
10A.3 Legal notice .............................................................................10A- 11
10A.4 Account information ...............................................................10A- 11
10A.5 Attachement ............................................................................10A- 11
10A.5.1 White Paper_Data Protection.pdf............................. 10A- 13
11 Troubleshooting.......................................................................... 11- 1
11.1 Eliminating faults ........................................................................ 11- 1
11.1.1 PLC................................................................................11- 1
11.1.2 Gas purifier....................................................................11- 1
11.1.3 Glovebox .......................................................................11- 1
11.1.4 Antechamber .................................................................11- 3
11.2 Stack light (optional)................................................................... 11- 4
11.3 ACK Warning and alarm messages........................................... 11- 4
11.3.1 Acknowledgement of a message ..................................11- 4
11.3.2 Deletion of a warning message .....................................11- 5
11.4 Definition of alarm and warning messages .............................. 11- 5
11.5 Failure during regeneration ..................................................... 11- 18
11.5.1 Cancellation or power failure.......................................11- 18
11.5.2 Regeneration of an LMF..............................................11- 18
11.6 Leak test..................................................................................... 11- 18
12 Maintenance ................................................................................ 12- 1
12.1 Introduction ................................................................................. 12- 1
12.1.1 Document inspection and maintenance ........................12- 1
12.1.2 Spare parts kit ...............................................................12- 2
12.1.3 Who may do what?........................................................12- 2
12.1.4 Qualification of maintenance personnel ........................12- 2
12.2 Maintenance plan overview........................................................ 12- 3
12.2.1 System in general..........................................................12- 3
12.2.2 Non-regenerative LMF...................................................12- 3
12.2.3 Regenerative LMF.........................................................12- 4
12.2.4 Gloves ...........................................................................12- 4
12.2.5 Mini Antechamber..........................................................12- 4
12.2.6 Main Antechamber ........................................................12- 5
12.2.7 Vacuum pump ...............................................................12- 6
12.2.8 Gas purifier....................................................................12- 6
12.2.9 Glovebox .......................................................................12- 7
12.3 Maintenance contract with MBRAUN ........................................ 12- 8
12.3.1 Analyser calibration .......................................................12- 8
12.3.2 Safety E-check service..................................................12- 8
12.4 Safety during maintenance work............................................... 12- 8
12.5 Preparations for inspection and maintenance work................ 12- 9
12.5.1 Shut down and de-energization.....................................12- 9

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12.5.2 General advice for maintenance work.........................12- 10
12.6 Maintenance works ................................................................... 12- 11
12.6.1 Glovebox .....................................................................12- 11
12.6.2 Gloves .........................................................................12- 12
12.6.3 Particle filter.................................................................12- 16
12.6.4 Calibrating and cleaning analysers .............................12- 17
12.6.5 Antechamber ...............................................................12- 17
12.6.6 Reactor........................................................................12- 17
12.6.7 Vacuum pump .............................................................12- 18
12.6.8 Non-regenerative LMF (optional) ................................12- 18
12.6.9 Optional and 3rd party components ............................12- 20
12.7 Completing maintenance ......................................................... 12- 20
12.8 Returning components for service purposes ........................ 12- 21
12.9 Decommissioning ..................................................................... 12- 21
12.10 Annex ......................................................................................... 12- 22
12.10.1 Declaration about Decontamination.pdf ......................12- 23
13 Spare parts .................................................................................. 13- 1
13.1 Introduction ................................................................................. 13- 1
13.2 Gas purifier .................................................................................. 13- 1
13.2.1 Front view......................................................................13- 1
13.2.2 Rear view.......................................................................13- 2
13.2.3 Box purge function (optional) ........................................13- 4
13.2.4 ECO Mode.....................................................................13- 4
13.2.5 Solvent filter (optional)...................................................13- 5
13.3 Glovebox...................................................................................... 13- 7
13.3.1 Chassis and lighting ......................................................13- 7
13.3.2 Gloves and glove parts..................................................13- 7
13.4 Particle filter .............................................................................. 13- 10
13.5 Analyser ..................................................................................... 13- 10
13.6 Antechamber ............................................................................. 13- 11
13.6.1 Main antechamber, ∅ 390...........................................13- 11
13.6.2 Mini antechamber Ø 150 mm ......................................13- 12
13.7 Vacuum pump ........................................................................... 13- 12
13.7.1 Oil sealed vacuum pump.............................................13- 12
13.7.2 Dry vacuum pump .......................................................13- 13
13.8 Touch panel TP700 ................................................................... 13- 13
13.9 Foot switch ................................................................................ 13- 14
14 3rd party documentation ............................................................ 14- 1
14.1 List of attached 3rd party documentation ................................ 14- 1
15 Certificates................................................................................... 15- 1
15.1 Declarations................................................................................. 15- 1
16 Electrical and wiring diagram(s)................................................ 16- 1
16.1 Safety ........................................................................................... 16- 1
16.1.1 Basic rules for working with electrical systems..............16- 1
16.1.2 Electrical safety check...................................................16- 1

Table of Contents
Page
8
MB-20-G/MB-200G-W_MB-LABmaster_MB-200 MOD_TP700
Operating Manual - V5.0 - 04/2018 - STD
16.2 Wiring diagramms....................................................................... 16- 2