Micromeritics ACCUPYC III User manual

PRE-INSTALLATION INSTRUCTIONS AND
CHECKLIST
135-42870-01
Nov 2023
(Rev -)
ACCUPYC®III
GAS DISPLACEMENT PYCNOMETER

TRADEMARKS
AccuPyc is a registered trademark of Micromeritics Instrument Corporation.
Micromeritics is a registered trademark of Micromeritics Instrument Corporation.
T.A.P. is a trademark of Micromeritics Instrument Corporation.
Copyright
The software described in this manual is furnished under a license agreement and may be used or
copied only in accordance with the terms of the agreement.
____________________________________________________________________________
Copyright © 2023. Micromeritics Instrument Corporation. All rights reserved.

CORPORATE PROFILE
Micromeritics Instrument Corporation is the world’s leading supplier of high-performance systems
to characterize particles, powders and porous materials with a focus on physical properties,
chemical activity, and flow properties. Our technology portfolio includes: pycnometry, adsorption,
dynamic chemisorption, particle size, intrusion porosimetry, powder rheology, and activity testing
of catalysts. The company has R&D and manufacturing sites in the USA, UK, and Spain, and
direct sales and service operations throughout the Americas, Europe, and Asia. Micromeritics
systems are the instruments-of-choice in more than 10,000 laboratories of the world’s most
innovative companies and prestigious government and academic institutions. Our world-class
scientists and responsive support teams enable customer success by applying Micromeritics
technology to the most demanding applications. For more information, please visit
www.micromeritics.com.
AccuPyc III Pre-installation Instructions and Checklist
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CONTACT US
Micromeritics Instrument Corporation
4356 Communications Drive
Norcross, GA30093-2901 USA
Phone: [phone]
Fax: [phone]
www.Micromeritics.com
Instrument Service or Repair
Phone: [phone]
International: Contact your local distributor or call 1-770-662-3636
[email protected]
Micromeritics Application Support
[email protected]
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ABOUT THIS MANUAL
The following symbols or icons indicate safety precautions and/or supplemental information and
may appear in this manual:
NOTE— Notes contain important information applicable to the topic.
CAUTION — Cautions contain information to help prevent actions that may damage
the analyzer or components.
WARNING — Warnings contain information to help prevent actions that may cause
personal injury.
About this Manual
AccuPyc III Pre-installation Instructions and Checklist
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General Safety
GENERAL SAFETY
Do not modify this instrument without the authorization of Micromeritics Service Per-
sonnel.
Any piece of laboratory equipment can become dangerous to personnel when improperly
operated or poorly maintained. All employees operating and maintaining Micromeritics
instruments should be familiar with its operation and should be thoroughly trained and instructed
on safety.
nRead the operator manual for any special operational instructions for the instrument.
nKnow how the instrument functions and understand the operating processes.
nWear the appropriate personal protective equipment when operating this
instrument — such as eye protection, lab coat, protective gloves, etc.
nWhen lifting or relocating the instrument, use proper lifting and transporting devices
for heavy instruments. Ensure that sufficient personnel are available to assist in
moving the instrument. The AccuPyc 1350 weighs approximately 11.5 kg (25.3 lb).
nAlways pay attention to the safety instructions provided on each label affixed to the
instrument and do not alter or remove the labels. When inspecting the instrument,
ensure that the safety labels have not become worn or damaged.
nThe AccuPyc III sound level is <65dBA from the operator's normal position, and
approximately 75dBA at 20 cm from the back of the instrument. Hearing protection
is optional.
nProper maintenance is critical to personnel safety and smooth instrument
operation and performance. Instruments require regular maintenance to help
promote safety, provide an optimum end test result, and to prevent costly down
time. Failure to practice proper maintenance procedures can lead to unsafe
conditions and shorten the life of the instrument.
nImproper handling, disposing of, or transporting potentially hazardous materials
can cause serious bodily harm or damage to the instrument. Always refer to the
SDS when handling hazardous materials. Safe operation and handling of the
instrument, supplies, and accessories are the responsibility of the operator.
If you have an ICD or pacemaker, avoid close or prolonged contact with magnets or
their magnetic fields. Keep magnets at least six inches from where your device is
implanted.
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INTENDED USE
The AccuPyc Series Pycnometers are fast, fully automatic pycnometers that provide high-speed,
high-precision volume measurements and true density calculations on a wide variety of powders,
solids, and slurries. After analyses are started with a few touches, data are collected, calculations
are performed, and results displayed. A minimal amount of operator attention is required.
The instrument is intended to be operated by trained personnel familiar with the
proper operation of the equipment recommended by the manufacturer and as well as
relevant hazards involved and prevention methods. Other than what is described in
this manual, all use is seen as unintended use and can cause a safety hazard.
The instrument is intended to be used as per applicable local and national regulations.
TRAINING
It is the customer's responsibility to ensure that all personnel operating or maintaining the
equipment participate in training and instruction sessions. All personnel operating, inspecting,
servicing, or cleaning this instrument must be properly trained in operation and machine safety
before operating this instrument.
General Safety
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General Safety
ENVIRONMENTALLY FRIENDLY USE PERIOD
Part Name
Hazardous Substances
Lead
(Pb)
Mercury
(Hg)
Cadmium
(Cd)
Hexavalent
Chromium
(Cr (VI))
Polybrominated
biphenyls
(PBB)
Polybrominated
diphenyl ethers
(PBDE)
Cover o o o o o o
Power
Supplies o o o o o o
Printed
Circuit
Boards
o o o o o o
Cables, Con-
nectors &
Transducers
x o o o o o
Hazardous Substances Table
o Hazardous substance is below the specified limits as described in SJ/T11363-2006.
x Hazardous substance is above the specified limits as described in SJ/T11363-2006.
The Environmentally Friendly Use Period (EFUP) for all enclosed products
and their parts are per the symbol shown here unless otherwise marked. Cer-
tain parts may have a different EFUP (for example, battery modules) and are
marked to reflect such. The Environmentally Friendly Use Period is valid only
when the product is operated under the conditions defined in the product
manual.
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SYMBOLS THAT APPEAR ON THIS INSTRUMENT
When this symbol is displayed, refer to this manual for additional information.
General Safety
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General Safety
Table of Contents
About this Manual iv
General Safety v
1 Pre-installation Document Overview 1 - 1
Micromeritics Installed Instruments Only 1 - 2
Dates and Signatures 1 - 3
Projected Installation Date 1 - 3
Commitment Statement and Signature Form 1 - 3
2 Pre-installation Instructions 2 - 1
Unpacking and Inspection 2 - 1
Shipping Damage 2 - 1
Analyzer Space 2 - 2
Installation Configuration 2 - 2
Environmental Factors 2 - 3
Power 2 - 3
Temperature and Humidity 2 - 3
Gas Supply 2 - 5
Laboratory Equipment and Supplies 2 - 8
3 Pre-installation Checklists 3 - 1
Unpacking and Inspection Checklist 3 - 1
Analyzer Space Checklist 3 - 1
Installation Configuration Checklist 3 - 1
Environmental Factors Checklist 3 - 2
Gas Supply Checklist 3 - 3
Laboratory Equipment and Supplies Checklist 3 - 4
Application Related Issues Checklist 3 - 4
Personnel Security Clearance Checklist 3 - 4
AccuPyc III EU Declaration of Conformity DoC - 1
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AccuPyc III UK Declaration of Conformity DoC - 1
General Safety
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1 PRE-INSTALLATION DOCUMENT OVERVIEW
If a Micromeritics Service Technician performs this installation, additional charges
apply. Please see Contact Us on pageiii for information on how to contact
Micromeritics.
1 Pre-installation Document Overview
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1 Pre-installation Document Overview
MICROMERITICS INSTALLED INSTRUMENTS ONLY
APPLICATION RELATED ISSUES
To ensure a thorough installation, it will be helpful for Micromeritics to know which types of
samples will be tested. If known, list them in Application Related Issues Checklist on page3 -
4.
Please advise Micromeritics if samples require any pretreatment. If required, do you have the
proper equipment to pretreat your samples? Micromeritics offers application assistance through
our materials analysis laboratory (Micromeritics Particle Testing Authority).
HAZARDS AND PRECAUTIONS
Inform Micromeritics of any on-site conditions that may present hazards to Micromeritics
employees or equipment. Advise Micromeritics of any precautions that need to be taken.
SAFETY MEASURES
Inform Micromeritics of any safety equipment, requirements, or procedures necessary for
Micromeritics employees to enter and install the system at your facility.
PERSONNEL SECURITY CLEARANCE
If security clearances, insurance certificates, or any other special arrangements are required for
Micromeritics employees to enter your facility, see Personnel Security Clearance Checklist on
page3 - 4 to explain. Inform Micromeritics how much advance notice you require to obtain
clearance.
PROJECTED INSTALLATION DATE
Read this entire document carefully. Complete all checklists in this document. Sign and return all
checklists and the Dates and Signatures on the facing page to Micromeritics. Micromeritics will
contact you to confirm an installation date.
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DATES AND SIGNATURES
All checklists and this completed form should be returned only if Micromeritics will be
performing this installation.
PROJECTED INSTALLATION DATE
This is not a commitment for a specific installation date. After reading the site preparation
requirements in this document, enter a date your site will be prepared and a preferred date for
installation. After returning the checklist and signed form to Micromeritics, your Micromeritics
representative will contact you to confirm an installation date.
When would installation be most convenient? Date: __________/________/________
COMMITMENT STATEMENT AND SIGNATURE FORM
I have read this document and understand my responsibilities regarding preparations for the
installation of our analysis system. I believe this site is ready for the system to be installed.
Signature: Date:
Name (Printed):
Title (Printed):
Company:
City / State / Zip:
Phone Number: Fax Number:
E-mail:
Analyzer: Model: Serial No.:
Is the Customer Representative also the End User? Yes ______ No ______
RETURN THE COMPLETED CHECKLIST AND FORMS TO:
Micromeritics Instrument Corporation
ATTN:Service
4356 Communications Drive
Norcross, GA / USA / 30093-2901
Email: [email protected]
Dates and Signatures
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2 PRE-INSTALLATION INSTRUCTIONS
UNPACKING AND INSPECTION
When the equipment is received, unpack and inspect the contents of the shipping container(s).
Use the packing list to verify that all products, accessories, software (if applicable), and
documentation are received intact and in the correct quantity. The shipping container(s) and
contents should be inspected within a few days of receipt in the event damage or loss has
occurred. Sort through all packing material before declaring missing equipment or parts.
Micromeritics recommends saving all shipping containers until installation of the equip-
ment is complete. All shipping containers where equipment is to be declared as dam-
aged or lost must be examined by the claims investigator prior to completion of the
inspection report.
SHIPPING DAMAGE
If equipment is damaged or lost in transit, you are required to make note of the damage or loss on
the freight bill. The freight carrier, not Micromeritics, is responsible for all damage or loss occurring
during shipment. If damage or loss of equipment is discovered during shipment, report the
condition to the carrier immediately. Insurance claims must be made with the freight carrier, not
Micromeritics.
nKeep all software, manuals, and accessories with the equipment.
nReport any shipping damage immediately to the carrier and follow their directions.
nReport missing or wrong parts to Micromeritics, in addition to any shipping damage, only after
filing a claim with the carrier.
nMicromeritics will NOT file a claim for shipping damage.
nDo not discard shipping boxes and containers until installation is complete. If space is avail-
able, it is recommended that shipping containers be saved for future use in the event of return
to factory for repair.
2 Pre-installation Instructions
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2 Pre-installation Instructions
ANALYZER SPACE
An unobstructed lab work space that will accommodate the following specifications is needed:
SPACE REQUIRED FOR INSTALLATION
Height 20.5 cm (8.1 in.)
Width 26.5 cm (10.4 in.)
Depth 43.0 cm (16.9 in.)
Weight 11.5 kg (25.3 lbs.)
Physical
INSTALLATION CONFIGURATION
Standard installation requires the use of 1/8 in. copper or stainless steel gas supply lines, located
in the instrument accessories kit. A nonstandard installation will be created if another gas supply
line is used or if the gas cylinders cannot be placed within 6 ft (2 m) of the analyzer. There may be
additional costs associated with a nonstandard installation. Please contact the Micromeritics
Service Department at 1-770-662-3636 to discuss a nonstandard installation.
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ENVIRONMENTAL FACTORS
POWER
The AccuPyc III uses a 24 V, 11.7 amp power supply with an input range of 100-240 VAC (±10%),
280 VA, 50-60 Hz. Noise-free power of the correct voltage and frequency, with a safety earth
ground, should be available through a standard wall receptacle. There should also be sufficient
outlets and easy access to those outlets for all devices.
The external power adapter required for the AccuPyc III is Micromeritics' part number
003-40001-02. Use of any other power adapter could damage equipment and/or
cause harm to the operator. The AccuPyc III is intended to be powered from the
output of the approved power adapter rated Class I, manufactured by Mean Well, P/N
GST280A24-C6P. Micromeritics supplies a suitably rated approved power supply
cord appropriate for the applicable country with the power adapter.
The analyzer and peripheral devices must be installed on their own dedicated power
line. Other devices — such as motors, generators, or ovens — should not be placed
on the same power line.
This instrument does not have a power switch and must be disconnected from the
wall outlet when powering off; therefore it is important to position the instrument where
the wall outlet is easily accessible.
TEMPERATURE AND HUMIDITY
Temperature and humidity must be controlled to within:
Temperature: Stable between 10 to 35 °C (50 to 96 °F). Temperature change up to 2 °C per
hour.
Humidity: 10 to 80% relative (non-condensing) for laboratory temperature from 10 to 25 °C,
maximum RH decreasing linearly to 50% at 35°C.
Do Not:
nAllow room temperature or humidity to exceed limits.
nInstall the analyzer where it is exposed to direct sunlight.
nLocate the analyzer near air conditioning or heating vents.
Environmental Factors
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2 Pre-installation Instructions
VENTILATION
Adequate ventilation is required to ensure effective temperature control and system
longevity. Ensure that the underside and back of the instrument are free of obstruction
and receive sufficient air flow.
The air intake may gather dust and impede performance. The intake filter should be
inspected weekly and cleaned with a duster or compressed air, if necessary. If
extremely dirty, wash and dry overnight, especially if in a dirty environment.
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