Micromeritics TriStar II 3020 User manual

INSTALLATION INSTRUCTIONS AND
CHECKLIST
302-42870-04
Sep 2017
(Rev A)
TRISTAR®II 3020 CONFIRM
SURFACE AREA AND POROSITY ANALYZER

TRADEMARKS
Alconox is a registered trademark of the Alconox Company.
Micromeritics is a registered trademark of Micromeritics Instrument Corporation.
Microsoft, Windows, and Windows 7 are registered trademarks of Microsoft Corporation.
Swagelok is a registered trademark of Swagelok.
TriStar is a registered trademark of Micromeritics Instrument Corporation.
Copyright
The software described in this manual is furnished under a license agreement and may be used or
copied only in accordance with the terms of the agreement.
______________________________________________________________________________
Copyright © 2008 - 2017. Micromeritics Instrument Corporation. All rights reserved.

CONTACT US
Micromeritics Instrument Corporation
4356 Communications Drive
Norcross, GA / USA / 30093-2901
Phone: [phone]
Fax: [phone]
www.Micromeritics.com
---------------
U.S.Inquiries
U.S. Sales Phone: [phone]
[e-mail]
---------------
Quotes, Orders, and Customer Satisfaction
Customer Service Phone: [phone]
[e-mail]
---------------
U.S. Instrument Service Department
U.S. Service Department Phone: [phone]
[e-mail]
---------------
Micromeritics Scientific Services
Customer Support Portal
http://techsupport.micromeritics.com/portal
Contact Us
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About this Manual
ABOUT THIS MANUAL
The following icons may be found in this manual:
NOTE- Notes contain important information applicable to the topic.
CAUTION - Cautions contain information to help prevent actions that may damage the
analyzer or components.
WARNING - Warnings contain information to help prevent actions that may cause per-
sonal injury.
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Table of Contents
Contact Us iii
About this Manual iv
1 Overview 1 - 1
Prepare for Installation 1 - 1
Dewar Precautions 1 - 2
2 Equipment Installation 2 - 1
Connect Ethernet Cable 2 - 1
Install the Vacuum Pump 2 - 2
Apply Power to the Analyzer 2 - 2
3 Application Installation 3 - 1
Add Users to Windows User Groups 3 - 6
Record User Information 3 - 7
Create User Profiles in the Administrator Utility 3 - 8
Create Password Configuration Parameters 3 - 9
Create Application User Profiles 3 - 10
Create a Service User Account 3 - 12
Start the Application 3 - 13
4 Analyzer Preparation 4 - 1
Manifold Evacuation 4 - 1
Specify Unit Selections 4 - 3
Gas Connections 4 - 4
Guidelines for Connecting Gases 4 - 5
Connect a Regulator and a Gas Line to a Gas Cylinder 4 - 6
Connect Gas to Analyzer 4 - 8
Clean and Verify the Gas Line 4 - 9
Specify Gas Ports 4 - 12
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5 Operational Verification 5 - 1
Transducer Verification 5 - 1
Verify 1000 mmHg Pressure Transducer Accuracy 5 - 1
Verify 10 mmHg Pressure Transducer Accuracy (Krypton Units only) 5 - 3
Create Sample Files 5 - 5
Step 1 - Clean and Label Sample Tubes 5 - 7
Determine the Sample Mass 5 - 9
Degas Samples 5 - 10
Install the Sample Tube 5 - 11
Fill and Install the Dewar 5 - 12
Reference Material Analysis 5 - 14
6 Installation Checklists 6 - 1
Exceptions 6 - 7
Signatures 6 - 8
Final Documentation 6 - 8
A Run Conditions A - 1
Automatic Blank Run Conditions A - 1
Manual Blank Run Conditions A - 1
Carbon Reference Material Run Conditions A - 4
B Worksheets B - 1
Sample Data Worksheet B - 2
User Information Worksheet B - 3
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1 OVERVIEW
Use these installation instructions and checklists to ensure that installation procedures are
completed properly.
It is recommended that installation procedures be performed in the order presented in
this document.
PREPARE FOR INSTALLATION
Before installation, ensure the operator has reviewed thoroughly the analyzer Pre-installation
Checklist. Ensure all required equipment and supplies are unpacked and the required personnel are
available.
When the equipment is received, unpack and inspect the contents of the shipping carton(s). Use the
packing list to verify that all products, accessories, software (if applicable), and documentation are
received intact and in the correct quantity. The shipping carton(s) and contents should be inspected
within a few days of receipt in the event damage or loss has occurred. Sort through all packing
material before declaring missing equipment or parts.
Save all shipping cartons where equipment is to be declared as damaged or lost. The
claims investigator must examine the cartons prior to completion of the inspection
report.
1 Overview
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1 Overview
DEWAR PRECAUTIONS
Always handle glass dewars with care. Any product incorporating a vacuum is a poten-
tial safety hazard and should be treated with caution. If in doubt, contact your safety
officer.
When handling dewars containing liquefied gases or cryogenic liquids:
lWear protective equipment:
ogoggles or face shield
oan insulated or rubber apron
oinsulated gloves
lWhen pouring liquefied gases from one container to another:
ocool the receiving container gradually to minimize thermal shock
opour the liquified gas slowly to prevent splashing
ovent the receiving container to the atmosphere
FOR GLASS DEWARS
lUse a plastic stirring rod when stirring substances in a dewar containing liquefied gases (or other
materials of extremely low temperature). Do not use a glass or metal stirring rod unless it has a
protective coating.
lDo not handle heavy objects above the dewar. If unavoidable, place a protective cover over the
dewar opening. If an object of sufficient weight is accidentally dropped into the dewar, shattering
may occur.
lIf the dewar has a protective mesh covering, do not remove it. This cover minimizes the risk of fly-
ing particles should the dewar be knocked over, dropped, or broken.
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2 EQUIPMENT INSTALLATION
CONNECT ETHERNET CABLE
CONNECT ONE ANALYZER
1. Plug one end of the Ethernet cable into the analyzer Ethernet port.
2. Plug the other end of the Ethernet cable into the computer Ethernet port.
CONNECT MULTIPLE ANALYZERS WITH AN ETHERNET SWITCH
Do not use the uplink port when using an Ethernet switch.
2 Equipment Installation
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2 Equipment Installation
INSTALL THE VACUUM PUMP
Log in to your customer portal to access the Vacuum Pump Guide (part number 062-42804-00) for
instructions on installing the vacuum pump.
APPLY POWER TO THE ANALYZER
1. Toggle the power switch to the ON position.
2. Check the power indicator on the front panel of the analyzer. The indicator will blink green to
indicate that power is applied to the analyzer. Once the application is running, the indicator will
stop blinking and remain illuminated.
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3 APPLICATION INSTALLATION
Configure an Ethernet port on the computer to communicate with the analyzer. The IP address must
be 192.168.77.100. Reference the computer operator manual for instructions on changing the
IPaddress.
The person installing the application must have Windows Administrator rights.The
administrator must create profiles for all users running Micromeritics TriStar IIConfirm.
The installation media contains the Micromeritics application and the Administrator Utility application.
The following tasks must be completed prior to application installation:
lThe Ethernet port for the analyzer must be set to 192.168.77.100
lConnect the analyzer to the configured port
lThe analyzer must be powered ON
If installing multiple analyzers, connect the Ethernet switch to the configured port and
the analyzers to the Ethernet switch. Refer to Connect Ethernet Cable on page2 - 1.
1. The Windows Administrator must create profiles for all users running the Confirm application.
Use the worksheet User Information Worksheet on pageB - 3 to record these profiles.
2. Insert the installation media into the computer. If the setup program does not immediately
start, navigate to the media device, then locate and double click the setup.exe file.
3. Click Next on the Welcome window. Do not proceed with this installation until all listed tasks
have been completed. Click OK.
3 Application Installation
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3 Application Installation
4. On the New Installation window, select the default location for file installation.
5. If a shortcut icon should be placed on the desktop, select the Add the application ... option.
6. Select Install this application for all Users to enable or prohibit users other than the installer to
access the application. Click Next.
7. On the Auxiliary Path Setup window, click Browse to select a new path for the listed option -
or accept the default..
8. Use the Seat number field if the application is installed on more than one computer. Enter a
number representing the computer. For example, if the application will only be installed on this
computer, enter 01. If installation will also be done on a second computer, enter 02, etc. The
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Seat number is used by the application to create a separate log file for each computer. Click
Next.
9. In the Step 1 group box on the Analyzer Configuration window, select the number of analyzers
to be attached to this computer.
If... Then...
installing the analysis program dur-
ing initial installation
Select the number of analyzers to be installed
using the analysis program for off-
line data reduction
Select 0
moving an analyzer from another
computer to this computer
Select 0.Refer to the section on moving a analyzer
in the Administrator's Utility for TriStar II3020 Con-
firm User Guide.
10. In the Step 2 group box on the Analyzer Configuration window, enter the serial number of
each analyzer to be attached to this computer. Click Next.
11. On the Ethernet Ports window, select one option from the following table:
3 Application Installation
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3 Application Installation
If... Then...
the configured port is listed Select the port, then click Next.
the configured port is not listed Click Specify and enter the remaining portion of the
IPAddress, then click Next.
The IP Address must be 192.168.77.100.
12. Calibration files are installed next.
If installing multiple analyzers, at the prompt, insert the media containing the calibration
files for the next analyzer.
13. On the Installation Complete window, read the notices, then click Finish.
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14. Remove the application media and store in a secure location. The original application media
contains the calibration files specific to the installed analyzer. Upgrade applications do not
contain calibration files.
15. If prompted, restart the computer after application installation.
3 Application Installation
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3 Application Installation
ADD USERS TO WINDOWS USER GROUPS
After reboot, the Windows Administrator must login and add application users to the four user
groups created during application installation. These user groups correspond to the four user profiles
that can be assigned in the Administrator Utility. Reference the computer operating system manual
for creating and editing user groups.
User Group Description
CfrAdministrator Contains the profile for the application Administrator.
It is recommended that at least two users to
this group.
MicDevelopers Contains users who will be assigned the Developer profile in the
Administrator Utility. The Developer profile enables users to
develop and enter analysis methods. A Developer has access to all
functions of the Micromeritics application.
MicAnalysts Contains users who will be assigned the Analyst profile in the
Administrator Utility. The Analysts profile enables users to perform
analyses using pre-defined analysis methods. An Analyst has
access to a limited set of the Micromeritics application features.
MicService Created for Micromeritics Service Personnel. These users will be
assigned the Developer profile in the Administrator Utility and have
full access to the functions of the Micromeritics application.
Although Service Personnel have the same access rights as
Developers, a separate user group is created for them because
Service Personnel have different directory and file access
permissions.
In addition to creating user groups, the Micromeritics application also sets the Windows directory and
file access permissions for each of these user groups.The default file permissions are included in the
Administrator Utility for TriStar II 3020 Confirm User Guide.
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RECORD USER INFORMATION
In addition to creating user groups, the Micromeritics application also sets the Windows directory and
file access permissions for each of these user groups.The default file permissions are included in the
Administrator Utility for TriStar II 3020 Confirm User’s Guide. These settings may be modified as
needed.
Reference the computer operating system manual for creating and editing user groups.
Developer Analyst
Create sample records from templates ü ü
Analyze samples ü ü
Generate reports ü ü
List and print sample records and templates ü ü
Perform routine maintenance ü ü
Enable manual control when the analyzer is idle ü ü
Change limited analysis conditions prior to performing an ana-
lysis
ü ü
Change report options after analysis ü ü
Create templates (analysis methods) for analyst use ü
Perform all other Micromeritics application functions ü
Record User Information
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3 Application Installation
CREATE USER PROFILES IN THE ADMINISTRATOR UTILITY
1. Go to Start > Programs > Micromeritics > Admin Util for TriStar IIConfirm.
2. In the User name field, enter cfradministrator.
3. In the Password field, enter Password. Click OK.
4. At the prompt Your password has expired, click OK and enter a new password. The pass-
word must contain a minimum of six alphanumeric characters. This password will be used to
log in to the Administrator Utility and the Micromeritics application. This will not affect the Win-
dows password.
5. Click OK.
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CREATE PASSWORD CONFIGURATION PARAMETERS
The Password parameters entered here apply to all Micromeritics application users.
On the Administrator Utility window, click the Configuration tab.
Field Description
Expire Enter the number of days when a user password will expire. This num-
ber of days goes into effect any time a password is changed. A zero
entry indicates the passwords will not expire.
Warn Enter the number of days prior to password expiration that a user will
be notified to change his password. A zero entry indicates this warning
will not be given.
Remember Enter the number of previous passwords to be stored in the password
history file for each user. This file is checked when a user enters a new
password to ensure that the password is unique. A zero entry indicates
this feature will not be used.
Disable account after Enter the number of times a user will be allowed to enter an invalid
password when attempting to log in before the application is locked. A
zero entry indicates this feature will not be used.
Must match Windows
user
Select to indicate the User ID must match the user Windows ID and
the user must be logged in to the Windows application. This ensures
that only the current Windows user can operate the Micromeritics
application. Otherwise, any user with the same access level
(Developer or Analyst) can log in to the application.
Application locked This field is selected when the application is locked. The application
locks automatically when the specified number of failed logon attempts
is reached.
Administrator Utility Fields
Create Password Configuration Parameters
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3 Application Installation
CREATE APPLICATION USER PROFILES
Refer to User Information Worksheet on pageB - 3 for the user names and profiles.
1. On the Administrator Utility window, click the User tab.
2. Click Add.
Fields Description
User Name Enter the user's Windows User ID.
FullName Enter the name that will:
ldisplay in the application,
lbe stored in the system log, and
lused as an electronic signature. This field must be unique.
Password Enter password as a temporary password that can be used to access
the application. This password is not saved in the password history file.
Add User Fields
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