EYELA SD-1010 User manual

Tokyo Rikakikai Co., Ltd.
R00
This manual is designed to use this unit safely with the best performance.
Keep this instruction manual beside the unit.
Important
Read carefully the chapter
[For safety operation] before operating
this unit.
SD-1010
Instruction
Manual
Spray Dryer
Spray Dryer

Precautions for your safety
However, if you know about them in advance, you
can prevent most of these accidents.
For that reason, this instruction manual defines
information on matters to be particularly noteworthy
in terms of safety according to their risk, and
indicate them with an alert mark and a signal word.
Please follow these instructions.
1. Warning signal words
This unit is not explosion-proof structured.
When a flammable sample or organic solvent is
used, handle it with care so that the liquid may not
be spilled over.
As hydrogen gas is used, please install and use
the equipment in a fume hood.
This product is used with its part being heated at
high temperature for its function and
characteristics.
A glass component used may get broken, if
mishandled, potentially leading to an unexpected
injury or accident.
We investigate enough possible hazards during the operation, however, it is very difficult
for us to find every hazardous occasion. Therefore this manual cannot describe all
hazardous operations.
However, if you carry out the handling method described in this manual, you can operate
and work more safely. Be sure to pay close attention to the handling of this product so
that accidents and product failures will not occur.
Alert Mark
Signal word Definition
Indicates a potentially hazardous situation which, if you use
incorrectly, could result in death or serious injury.
Indicates a potentially hazardous situation which, if you
use incorrectly, may result in injury or physical damage.
Warning
Caution
Indicates a hazardous situation which, if you use incorrectly,
could result in death or serious injury.
Warning

2.Warning label
A warning label is attached to the unit to refer to the most important clause.
The attached position is shown below.
Be careful to use the unit referring warning messages.
* When the warning label is worn and hardly show the message, change it with a new one.
Please order us a new label.
Explosion
Do not use this unit
to dry any explosive
materials such as
organic solvent.
Warning
Burning
Do not touch
evaporator or cyclone
while drying samples.
Caution
① ②
①
②

Read this manual carefully before operation.
Thank you for choosing products.
Introduct
ion
Table of
contents
This instruction manual describes the procedure of
installation, operation, troubleshooting,
maintenance/check-up, and disposal for
Spray dryer model
SD-1010.
1.For safety operation 1
2.Outline
2-1. Application 1
2-2. Specifications 2
2-3. Description of each part 3
3.Descriptions and functions of the control panel
3-1.Control panel 5
3-2.Safety and alarm functions 7
4.Installation
4-1. Installed place 8
4-2.Environmental conditions 8
4-3.Connection of utility 9
4-4.Connection of utility 10
5.Operation
5-1.Preparation
5-1-1.Attaching evaporating tube 11
5-1-2.Attaching cyclone 12
5-1-3.Attaching outlet temp. sensor 12
5-1-4.Attaching power collection container and
separator 13
5-1-5.Countermeasures against static electricity
13
5-1-6.Attaching silicone tubing 14
5-1-7.Connecting power cord 15
5-1-8.Connecting exhaust hose 15
5-1-9.Connecting air tubing 16
5-1-10.Connecting recorder cable 16
5-1-11.Replacing cap for nozzle 17
5-1-12.Installing agitator 18
5-2.Operation
5-2-1.Preparing sample and distilled water 19
5-2-2.Operation 20
5-2-3.Cleaning spray nozzle 24
5-2-4.Collection of fine powder 25
5-3.End of operation 25
6.Troubleshooting 27
7. Maintenance and Check-up
7-1.Cleaning and care of product 29
7-2.Cleaning and changing filter
7-2-1.Cleaning or changing inlet filter 30
7-2-2.Cleaning or changing outlet filter 31
7-3.Cleaning evaporating tube and cyclone 31
7-4.Cleaning spray nozzle 33
7-5.Replacing the evaporating tube and cyclone
accessories
7-5-1.Replacing parts at the connection 35
7-5-2.Replacing collection bottle fixing parts 36
8.Product disposition 37
9.Post-sale service 38
10.List of Disposable/Replacing Parts/Optional
Products
10-1. Disposable/replacing parts 39
10-2. Optional products 42

Part name Qty.
1 Main unit 1
2 Rectification board 1
3 Exhaust hose, cuff (2 pieces) 2.5m
4 Stainless steel diamond clamp (for exhaust hose) 2
5 Air piping connector(1/4') 1
6Air piping tube(OD6mm) 10m
7 Stirring bar 1
8 Silicone tubing for applying sample (3.15 x 5.2) 2m
9Silicone tubing for applying sample (3.7 x 6.1) 1m
10 Aluminum tape 10m
11 Cable for recorder(2m) 3
12 Sensor for outlet temperature 1
13 Evaporator set 1
14 Cyclone set 1
15 Collection bottle set 2
16 Instruction Manual 1
17 Warranty 1
This unit is packed in 2 cartons which are main unit and
accessory parts. Check quantities referring to the below
table.
P a c k i n g
2.Rectification board 3.Exhaust hose,cuffs
4.Stainless steel diamond
clamp 5.Air tube connector
6.Air tube 7.Stirring bar
8,9.Silicone tubing 10.Aluminum tape
11.Cable for recorder 12.Sensor for outlet
temperature
13.Evaporator set 14.Cyclone set
15.Collection bottle set

While operating unit, do not touch evaporator or cyclone
to prevent burning of your hands.
While operating unit, do not touch evaporator or cyclone.
Do not use this unit to fry flammable materials such as organic solvent.
This unit has a built-in heater, so it may ignite.
Do not use flammable materials such an organic solvent.
For safety operation
1
Please pay attention to safety as this product becomes hot
Warning
Caution
-1-
Evaporator
Cyclone
In his unit samples are sprayed through a nozzle and
dry by headed air to make dried fine particle.
Outline
2
Do not use flammable materials
such as organic solvent.
Do not use this unit to dry flammable materials such as
organic solvent.
This unit has a built-in heater, so it may ignite.
Dangerous
2-1 Application
Do not remodel. Do not use out of
applications.
Warning
Remodeling or using out of applications may occur electric
shock hazard or mechanical troubles.

2-2 Specifications
Product name Spray Dryer
Model SD-1010
Performance
Evaporating rate Max 1500ml/h
Drying air flow rate control range and
precision 40~200°C (Outlet temperature) • ±1°C
Drying air flow rate control range 0.2~ 0.75m3/min
Spraying air press. control range 20~250kPa (0.2~2.5kg/cm2)
Flow range of delivery pump 150~1700mL/h
Rotation rate and capacity of sample
agitator 100~1000rpm • 50mL~2L (Water) Upper agitation available (option)
Function
Inlet temperature display/Outlet
temperature display Digital display
Drying air volume display Digital display
Spraying pressure display Digital display
Safety features
Evaporating tube protection cover, leakage/overcurrent
breaker, overheat protector
Manual return at blackout, self-diagnostic function (
abnormal
temperature, abnormal air volume,
heater disconnected, abnormal pressure for solution being
sent)
Sprayed air line cleaning function Automatic operation with interval timer
Inlet temp. recorder output • Outlet temp.
recorder output 0~10mV (at50 ~ 250°C)
Drying air volume output 0~10mV(at0~1m3/min)
Composition
Heater 3kW
Delivery pump Tube pump
Spray nozzle Twin-fluid nozzle (nozzle hole diameter 0.71 mm in inside diameter)
Nozzle diameter changeable (option)
Spray air pump Spray air compressor (option)
Evaporating tube, cyclone,
Powder collection container, separator Hard glass
Sample agitator motor, magnet DC brushless motor, cobalt magnet
Suction blower Commutator blower
Standards
Diameter of tube used in delivery pump ID 3.15 xOD 5.2mm
Spray air connection bore, material ID 4x OD 6mm, soft urethane tube Union
Spraying air pressure Pressure:294kPA (3kg/cm2) , Flow rate:25L/min or more
Exhaust port size Exhaust port OD 50mm
Interval timer OFF or 1-20 min (automated intermittent time)
Ambient temperature range 5~35°C
Ambient humidity range 30~80%RH (no condensation)
Overall dimensions(mm)• Net weight 700W x 620D x 1500H mm • Approx.110kg
Power sonsumption and power source 19.1A 4.2kVA・AC220V Single phase50/60Hz
*The performance described demonstrates values "at room temperature 20ºC with rated supply voltage
50Hz using potable water and a silicon tube."
*No power plug is supplied.
-2-

2-3 Description of each part
[Front view]
-3-
[Rear view]
Evaporator
Separator
Powder collection container
Cyclone
Connecting tube
Duct
Sensor for outlet temperature
Protection cover
Blower exhaust port
Maintenance port
(Inside: Inlet filter)
Caster Adjuster
Maintenance port
(Inside: Outlet filter)
Cooling fan for control part
Cooling fan for main unit
For cooling blower
Air intake
Outside air inlet
((Silicon tube)
Connection collar

Spray nozzle
Pressure sensor
Delivery pump Sample agitator
(Magnetic stirrer)
Pole fixing screw
Recorder output terminals
Operation lamp of over temperature protector Reset switch of over temperature protector
Power switch
Ground terminal
Air connecting port
Electrical leakage breaker
Power cord
[Top face of operating portion]
[Right side of operating portion]
[Lower right side of housing]
-4-
Operating panel
Screw cover

Descriptions and functions of the control panel
3
3-1 Control panel
No. Description Function
1 Pump line alarm lamp It illuminates when the pressure of flow line attains to a certain pressure.
2 Pump operation lamp It illuminates while the pump is running.
3 Pump ON/OFF key Delivery pump Run/Stop
4 Jet cleaner operation lamp It illuminates when the jet cleaner is in operation
5 Jet cleaner manual operation key To operate manually a cycle of jet cleaning
6 Interval time setting dial To set interval time of jet cleaning
7 Spraying air supply lamp It illuminates when spraying air is supplied
8 Spraying air supply switch To open or close the air supply valve
9 Spraying pressure control knob To control spraying pressure
10 Drying air flow rate control knob To control drying air volume
11 Drying air flow alarm lamp It illuminates when the drying air volume is lower than a certain value.
12 Temperature controller/blower RUN/STOP
key To run/stop temperature controller/blower
13 Temp. control and blower operation lamp To control temperature. It illuminates when the blower is in operation
14 SET key To determine setting values for temperature control and various parameters
15 UP key To change setting values for temperature control and various parameters
16 DOWN key To change setting values for temperature control and various parameters
17 Heater alarm lamp It illuminates when the heater is disconnected
18 Temp. alarm lamp It illuminates when the inlet temp. exceeds the band of set point
19 Heating lamp It illuminates when the heater is active
20 Set value indication lamp It illuminates when the set value is displayed on the inlet temp. indicator.
21 Measured value indication lamp It illuminates when the measured value is displayed on the inlet temp.
indicator
22 Inlet temp. indicator It displays the inlet temperature of evaporating tube
23 Outlet temp.indicator It displays the outlet temperature of evaporating tube
24 Drying air flow rate indicator It displays drying air volume into the evaporating tube
25 Spraying pressure indicator It displays the spraying pressure of sample.
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