EYELA FDU-2200 User manual

R00
取扱説明書
Instruction
Manual
Freeze dryer
FDU-2200
This instruction manual is designed to use the product efficiently and safely.
Please keep this manual in a place easily accessible to every user.
Be sure to read “Safety precautions
carefully before use.
IMPORTANT
Tokyo Rikakikai Co., Ltd.

Safety precautions
1. Signal word for warning
Therefore, this manual categorizes the level of
importance and danger as below with alert mark and
signal word. Please follow the instructions and use
the product safely.
Wrong operation of the product may cause you
physical injury. However, if you have proper
information before use, you can avoid almost
all these troubles.
Alert mark
Signal word Definition
Mishandling the product may cause users serious personal injury or loss of life.
WARNING
Mishandling the product may injure users or cause property damage.
CAUTION
Though we are trying to look into conceivable risk of using the product, it is very difficult for us to
expect all. It means that all the instructions in this manual do not cover all the potential risks that may
be caused by the product. However, if you follow the instructions, you surely can handle and operate
the products safely. Please use extreme care when handling this product and try to prevent all the
potential accidents and mechanical failures.

2. Warning display on the product
For highly priority danger, warning label is attached
on the machine body. The position of the label is as below.
Please read the instructions carefully whenever using the machine.
※If you have any trouble reading the label
because of damage and etc., please replace
with new one. Contact us if your
require new label.
CAUTION
Do not touch
the cooling fin
with bare hands.

Thank you for choosing the product of
Introduction
This instruction manual describes the procedure of installation,
operation, troubleshooting, maintenance, check up, and disposal
of Freeze dryer, FDU-2200.
Please read this manual carefully before use.
Contents
1.For safety use
Items contained
in your carton
4 – 4 Utility connection
5.Operation
5 – 1 Preparation
5 – 2 How to operate
6.Troubleshooting
7.Maintenance・checking
7 – 1 How to replace consumable parts
7 ‐ 2 Operation test for electric leakage breaker
7 ‐ 3 Replacing fuse
7 ‐ 4 Cleaning and caring the product
8.Disposla of the product
9.After-sales service
2.Ouline of the product
2 – 1 Use application 2
2 – 2 Specification
2 – 3 Data on the product（Reference)
2 – 4 Options
2 – 5 Name of each part
3.Name and functions of operating portion
3 – 1 Control panel
3 – 2 Safety functions 12
4.Installation
4 – 1 Installation environment
4 – 2 Installation condition
1
2
3
9
4
8
Please check the type and the quantity of every part.
14
14
16
17
30
31
31
18
27
33
34
32
Filter for leaking
1Instruction Manual
7
1
Main unit
1
1
Fuse
2
2Recorder output cable
3
1
Filter for leaking
4
4
Caster holder
5
1
Trap barrier
6
QuantityName
No.
4 – 3 Installation 15
Caster holder Trap barrier

For safety use
1
This product is not designed with explosion-proof structure.
Use extreme care when handling it.
Solvent that can not be trapped may be vacuumed into the
vacuum pump, which may cause a fire or explosion.
Use extreme care when drying sample that includes
inflammable substance, such as organic solvent.
WARNING
Cooling fin
Do not touch the cooling fin with bare hands during maintenance work.
Edgy fin may cut your hands.
Do not touch the cooling fin with bare hands.
CAUTION
●Preliminary freeze the sample container.
●Change the oil in the vacuum pump regularly.
‑1‑

Outline of the product
2
2-1 Use application
Do not remodel the product.
Do not use it out of intended application.
Remodeling or using the product out of intended
Application may cause electric shock or
malfunction.
WARNING This product can be used for drying dilutional solution
such as protein, enzyme or extraction solution of biological
sample, or biogenic sample such as urine, blood serum and
etc.
2-2 Specification
Pirani gauge
Digital display 0.0〜533.3Pa
Recorder output Trap temperature 1℃/1mV Vacuum degree 1Pa/1mV
Voltage
Rated supply AC100V±10％、50/60Hz
Features
C
O
N
F
I
G
.
Model
Refrigerator（Output)
Service outlet
S
P
E
C
.
Mass
Product name
F
U
N
C
I
T
I
O
N
S
Refrigerant
Range of available ambient temperature
Freeze dryer
FDU‑2200
Trap cooling temp.
Dehumidifying amount
Trap defrosting function
Trap measurement (mm) material
Vacuum gauge
Defrosting by hot gas
153(Bore diameter)×225(Height)、SUS304
External measurement（mm）
−80℃
1 ℓ／Time
400Ｗ × 2
5〜35℃
450(W)×550(D)×935(H)
Approx.67kg
Cooling system Cooled into drum-shaped container
※1
Required displacement of vacuum
pump More 50/60L/min（50/60Hz）（option）
Other functions Vacuum pump control, display of the availability of freeze drying,
display of vacuum pump operation time,
Stop watch function, selecting power recover function,
Detecting abnormal vacuum degree（fixed value), Protection timer for
refrigerator
Displaying accuracy at 0.4〜4.0Pa ±2.0Pa
at 4.1〜10.0Pa ±3.0Pa
at 10.1〜15.0Pa ±4.0Pa
at 15.1〜40.0Pa ±7.0Pa
HFC（R404A)（Primary refrigerator）＋R23（Secondary refrigerator）
For vacuum pump（Max.6A ）For dry chamber（Max.2A ）
AC100Ｖ 12A
※2
※3
※1.Measured in the following condition; ambient temperature:20℃, NO load
※2.Protruding portion is not included.
※3.Capacty of service outlet is not included.
‑2‐

2-3 Data on the product（Reference）
・Attached 4 pear-shaped flasks (capacity:1ℓ) containing 250g of water to
the trap and calculated back the sublimation from the remaining amount of flask after
elapsing designated length of time.
Condition ・AC100V,50Hz
・Ambient temperature 20℃
（１）Data on sublimation speed
Sublimation
amount（ｇ） 900
1000
800
700
600
500
400
300
200
100
0
01234567891011
Time（h）
・Sublimation speed differs depending on room temperature, capacity and the shape of sample’s
container (pear-shaped flask and freeze dry bottle and etc.), type and quantity of sample, and
the condition of preliminary frozen sample.
Condition ・AC100V,50Hz
・Ambient temperature 20℃
（２）Data on trap temperature when subliming sample
20
30
Temperature（℃）
Room temperature
10
0
‑10
‑20
‑30
‑40
‑50 Displaying temperature of the unit
Recorder output）
‑60
‑70
‑80
‑3‑
・Data on trap temperature when subliming sample differs depending on room temperature,
capacity and the shape of sample’s container (pear-shaped flask and freeze dry bottle and etc.),
type and quantity of sample, and the condition of preliminary frozen sample.
‑90
The beginning of trap
012345678910
Time（h）

2-4 Options
‑4‑
■Test tube, ampoule bottle and manifold for vial container
Stainless T-shaped manifold with 12 (PMH-12) / 24 (PMH-24)
inlets for being applied sample. Samples in each inlet can be
freeze dried simultaneously.
※When using test tube or ampoule container,
appropriate adapter is required.
Model Catalogue No.
PMH‑24 119860
PMH‑12
PMH‑24
This option can be secured to the main unit of
FDU-2200. With this base, the main unit can be
moved with connecting vacuum pump.
(This optional accessory is available only for FDU-2200).
Secures Manifold (option) to the main unit of FDU-2200.
(This optional accessory is available only for FDU-2200).
209540FDU‑CRAMP2
Catalogue No.Model
FDU‑BASE
PMH‑8
■Manifold for flask
Stainless T-shaped manifold with four (PMH-4) /
eight (PMH-8) inlets for being applied sample.
Samples in each inlet can be freeze dried simultaneously.
Model Catalogue No.
PMH‑4
PMH‑8
119820
119830 PMH‑4
PMH‑12 119840
■Bearing for acrylic base
FDU‑CRAMP2
■Base for vacuum pump
209540FDU‑BASE
Catalogue No.
Model
DRC‑3L
■Airtight system dry chamber
Airtight preservation can be performed at the
top shelf after completing freeze drying. Other
shelves can be used as dry chamber.
BSC‑2L
Model Catalogue No.
BSC‑3L 119810
119790
BSC‑3L
BSC‑2L
■Dry chamber
Freeze drying can be performed in vial container
and petri dish.
DRC‑1N DRC‑2L
119730
DRC‑1N
DRC‑2L 119750
Model Catalogue No.
DRC‑3L 119770

⑧
⑨
⑦
②③
①
■Stopcock B, test tube, ampoule container
and etc.
④
⑥
⑤
Stopcock B 119930 11
Vacuum stopcock body B 144480 21
Liner B 143960
10
Vacuum cock B
B‑type Adapter for test tube 120510
1
10
7
Specification Catalogue No.
Product name
No. Qty
3
144490
Forφ8
Forφ6
120520
120530
5
120210
Ampoule container Pear‑shaped （1mℓ）
120220
20
20
1
1
4
5
6
Adapter for ampoule
container
Pencil‑shaped round bottom（1mℓ）
Pencil‑shaped flat bottom（1mℓ）
Flat bottom（2mℓ）120230
20
20
120221
Flat bottom（5mℓ）120240
20
Flat bottom（10mℓ）
Round bottom（2mℓ）
120250
120260
10
20
Round bottom（5mℓ）120270
20
Round bottom（10mℓ）120280
Sealing 145610
143970
143980
143990
144000
Test tube with rim φ10×75（3mℓ）
φ12×75（4mℓ）
φ12×90（5mℓ）
φ12×105（6mℓ）
φ12×120（7mℓ）
φ13×75（5mℓ）
φ13×90（6mℓ）
144010
144020
144030
144040
100
100
100
100
100
100
100
100
1
8
9
φ13×100（7mℓ）
φ15×85（8mℓ）144050
100
φ15×105（10mℓ）144060
100
φ16.5×165（20mℓ）
φ18×165（24mℓ）144100
144090
50
50
φ15×150（15mℓ）144070
50
φ16.5×105（12mℓ）144080
100
φ18×180（27mℓ）
φ21×200（42mℓ）
144110
144120
50
50
‑5‑

■Stopcock A, Freeze drying container, flask and etc.
‑6‑
⑳
⑪
⑩
⑫
⑬
⑭
⑮
⑯
⑲
22
21
24
Flask for sample 50mℓ
100mℓ
200mℓ
300mℓ
500mℓ
1000mℓ
116140
116150
116160
116170
116180
116190
1
1
1
1
1
1
Specification Cat.No.
Product name
No. Qty
Stopcock A
Vacuum stopcock body A
Liner A
Vacuum stopcock A
Adapter for flask
10
11
12
13
14
15
119920
144460
143950
144470
120470
144500
1
1
10
1
1
1
・
⑮
⑧
⑰
23
T 29
S
T 24
S
T 29
S
T 29
S
T 29
S
T 29
S
T 29
S
T 29
S