Knick Protos 3400X User manual

Latest Product Information: www.knick.de
Protos 3400(X)
Process Analysis System
Communication Module Protos MS 3400(X)-160
For Memosens Sensors
The Art of Measuring.
Aktuelle Produktinformation: www.knick.de
Analysenmesssystem
Protos 3400(X)
Betriebsanleitung Messmodul Protos CONDI 3400 (X)-051
zur Leitfähigkeitsmessung mit induktiven Sensoren
Deutsch
The Art of Measuring.
Aktuelle Produktinformation: www.knick.de
Analysenmesssystem
Protos 3400(X)
Betriebsanleitung Messmodul Protos CONDI 3400 (X)-051
zur Leitfähigkeitsmessung mit induktiven Sensoren
Deutsch
User Manual
English
MEMO SENS

Trademarks
The following trademarks are used in this manual without further marking:
CalCheck®, Calimatic®, Protos®, Sensocheck®, Sensoface®, Unical®, VariPower®, Ceramat®, SensoGate®
are registered trademarks of Knick Elektronische Messgeräte GmbH & Co. KG, Germany
Memosens®
is a registered trademark of
Endress+Hauser Conducta GmbH & Co. KG, Germany
Knick Elektronische Messgeräte GmbH & Co. KG, Germany
SMARTMEDIA®
is a registered trademark of Toshiba Corp., Japan
©2017 Subject to change without notice
Return of Products under Warranty
Please contact our Service Team before returning a defective device. Ship the cleaned device to
the address you have been given. If the device has been in contact with process fluids, it must be
decontaminated/disinfected before shipment. In that case, please attach a corresponding certificate,
for the health and safety of our service personnel.
Disposal
Please observe the applicable local or national regulations concerning the disposal of
“waste electrical and electronic equipment”.
Knick
Elektronische Messgeräte GmbH & Co. KG
Beuckestr. 22
14163 Berlin, Germany
Phone: [phone] - 0
Fax: [phone] - 200
Web: www.knick.de
Email: [email protected]

3
Table of Contents
Protos MS 3400(X)-160 Module
Return of Products under Warranty .................................................................................... 2
Disposal ......................................................................................................................................... 2
Trademarks ................................................................................................................................... 2
Intended Use.................................................................................................... 7
Safety Information .......................................................................................... 8
Application in hazardous locations: MS 3400X-160 module ..................................... 8
Conformity with FDA 21 CFR Part 11.................................................................................. 9
Software Version ......................................................................................................................10
Modular Concept .....................................................................................................................11
Short Description .......................................................................................... 12
Short Description: FRONT Module ....................................................................................12
Short Description: Menu Structure....................................................................................13
Short Description: BASE Module........................................................................................15
Terminal Plate................................................................................................ 16
Wiring and Memosens Cable........................................................................ 17
Parameter Setting: Operating Levels .......................................................... 18
Administrator level ..................................................................................................................18
Operator level............................................................................................................................18
Viewing level..............................................................................................................................18
Parameter Setting: Locking a Function ...........................................................................19
Configuring the Measurement Display ....................................................... 20
Documenting Parameter Setting .......................................................................................22
ProgaLog 3000 Software (Option) forConfiguration and Documentation .......24
Module Configuration: Operating Mode..................................................... 28
Memosens PH Parameter Setting ................................................................ 29
Activating the Cal Tolerance Band (Memosens PH) ....................................................32
Memosens PH Calibration / Adjustment ..................................................... 36
Calibration methods ...............................................................................................................38
Temperature compensation.................................................................................................39
HOLD Function During Calibration ...................................................................................40
Calimatic automatic buffer recognition...........................................................................42
Calibration with manual entry of buffer values ...........................................................44
Product calibration .................................................................................................................46
Calibration by entering data from premeasured electrodes ...................................48

4
Table of Contents
Protos MS 3400(X)-160 Module
Memosens PH Maintenance ......................................................................... 50
Sensor monitor .........................................................................................................................50
Temp probe adjustment........................................................................................................50
Memosens PH Diagnostics Functions.......................................................... 51
Message list................................................................................................................................51
Logbook.......................................................................................................................................51
Sensor monitor .........................................................................................................................52
Cal record ....................................................................................................................................52
Sensor network diagram.......................................................................................................53
Sensor wear................................................................................................................................53
Calibration timer.......................................................................................................................54
Adaptive calibration timer....................................................................................................54
Tolerance adjustment.............................................................................................................54
Memosens PH/ORP Parameter Setting........................................................ 55
Memosens ORP Parameter Setting.............................................................. 57
Memosens ORP Calibration / Adjustment................................................... 62
ORP related to the standard hydrogen electrode (SHE)............................................62
Temperature dependence measured against SHE (standard hydrogen
electrode)....................................................................................................................................63
Memosens ORP Maintenance....................................................................... 64
Sensor monitor .........................................................................................................................64
Temp probe adjustment........................................................................................................64
Memosens ORP Diagnostics Functions ....................................................... 65
Message list................................................................................................................................65
Logbook.......................................................................................................................................65
Sensor monitor .........................................................................................................................66
Cal record ....................................................................................................................................67
Memosens OXY (TAN required).................................................................... 69
Activating an Additional Function.....................................................................................70
Parameter Setting (Memosens OXY) ........................................................... 71
Calibration / Adjustment (Memosens OXY) ................................................ 75
Recommendations for calibration .....................................................................................77
HOLD Function During Calibration ...................................................................................78
Automatic calibration in water ...........................................................................................80
Automatic calibration in air..................................................................................................82

5
Table of Contents
Protos MS 3400(X)-160 Module
Product Calibration (Calibration with Sampling) ........................................................84
Data entry of premeasured sensors .................................................................................86
Zero correction..........................................................................................................................87
Maintenance (Memosens OXY) .................................................................... 88
Sensor monitor .........................................................................................................................88
Temp probe adjustment........................................................................................................88
Sensor maintenance ...............................................................................................................88
Diagnostics (Memosens OXY) ...................................................................... 89
Sensor monitor .........................................................................................................................89
Cal record ....................................................................................................................................90
Sensor network diagram OXY .............................................................................................90
Sensor wear monitor...............................................................................................................90
Memosens COND Parameter Setting........................................................... 91
Concentration Table (Memosens COND).........................................................................97
USP Function (Memosens COND) ......................................................................................98
pH Value Calculation (Memosens COND)........................................................................99
Calculation Blocks (Memosens COND).......................................................................... 101
Memosens COND Calibration / Adjustment.............................................. 105
Temperature compensation.............................................................................................. 107
HOLD Function During Calibration ................................................................................ 108
Automatic calibration with standard calibration solution..................................... 110
Manual entry of cal solution ............................................................................................. 112
Product calibration ............................................................................................................... 114
Data entry of premeasured sensors............................................................................... 116
Sensor calibration ................................................................................................................. 117
Memosens COND Maintenance.................................................................. 118
Sensor monitor ...................................................................................................................... 118
Temp probe adjustment..................................................................................................... 118
Memosens COND Diagnostics .................................................................... 119
Sensor monitor ...................................................................................................................... 119
Cal record ................................................................................................................................. 120
CONDI Parameter Setting ........................................................................... 121
Concentration Table (CONDI)............................................................................................ 127

6
Table of Contents
Protos MS 3400(X)-160 Module
CONDI Calibration / Adjustment ................................................................ 129
Temperature compensation.............................................................................................. 131
HOLD Function During Calibration ................................................................................ 132
Automatic calibration with standard calibration solution..................................... 134
Manual entry of cal solution ............................................................................................. 136
Product calibration ............................................................................................................... 138
Data entry of premeasured sensors............................................................................... 140
Zero Correction (CONDI)..................................................................................................... 141
Calibrating the sensors ....................................................................................................... 141
CONDI Maintenance ................................................................................... 142
Sensor monitor ...................................................................................................................... 142
Temp probe adjustment..................................................................................................... 142
CONDI Diagnostics ..................................................................................... 143
Sensor monitor ...................................................................................................................... 143
Cal record ................................................................................................................................. 144
Calculation Blocks (for all Process Variables)............................................ 145
Logbook.................................................................................................................................... 147
Factory Setting....................................................................................................................... 147
Configuring a Current Output.......................................................................................... 148
Current Outputs: Characteristics ..................................................................................... 149
Output Filter............................................................................................................................ 151
NAMUR Signals: Current Outputs ................................................................................... 152
NAMUR Signals: Relay Contacts....................................................................................... 153
Relay Contacts: Protective Wiring ................................................................................... 154
Relay Contacts, Usage ......................................................................................................... 155
Relay Contacts: Sensoface Messages............................................................................. 156
Rinse Contact.......................................................................................................................... 157
Icons in the measurement display.................................................................................. 158
Limit Value, Hysteresis, Contact Type............................................................................. 158
OK1, OK2 Inputs: Specifying the Level.......................................................................... 159
Selecting Parameter Set (A, B) via OK2 Input ............................................................. 160
Signaling Active Parameter Set via Relay Contact.................................................... 160
Specifications............................................................................................... 161
Index ............................................................................................................ 163

7
Intended Use
The module provides an RS-485 interface for connecting Memosens sensors.
An analog current input can accept a signal from a pressure transmitter for
pressure compensation of oxygen sensors. A galvanically isolated switch-
ing input allows the connection of monitoring equipment, such as a flow
monitoring system.
The MS 3400X-160 module is intended for operation in locations subject to
explosion hazards which require equipment of Group II, device category 2(1),
gas/dust.
Current input
(OXY: pressure transmitter
or ow, for ex.)
Memosens sensor
• pH
• pH/ORP
• OXY (with TAN)
• COND
• CONDI
• ORP
1
2
3
4
5
7
9
Shield

8
Safety Information
Application in hazardous locations
CAUTION!
Never try to open the module! If a repair should be required, return the module
to our factory.
If the specifications in the user manual are not sufficient for assessing the safety
of operation, please contact the manufacturer to make sure that your intended
application is possible and safe.
Application in hazardous locations: MS 3400X-160 module
The module is approved for operation in hazardous locations.
Observe all applicable local codes and standards for the installation of electrical
equipment in hazardous locations. For orientation, please refer to
IEC 60079-14, EU directives 2014/34/EU and 1999/92/EC (ATEX), NFPA 70 (NEC),
ANSI/ISA-RP12.06.01.
• When installing the device in a hazardous location, observe the specifica-
tions of the EC-Type-Examination Certificate and, if applicable, of the Control
Drawing (download: www.knick.de).
• Before commissioning you must prove that the device may be connected
with other equipment, such as a supply unit including cables and wires.
• In hazardous locations the device shall only be cleaned with a damp cloth to
prevent electrostatic charging.
• Devices and modules which have already been used shall be subjected to
a professional routine test before they may be operated in another zone or
another type of protection.
Be sure to observe during installation:
• Switch off power supply before replacing or inserting a module.
• Protect the signal inputs of the modules against electrostatic discharge.
• Before commissioning it must be proved that the device may be connected
with other equipment.

9
In their directive “Title 21 Code of Federal Regulations, 21 CFR Part 11,
Electronic Records; Electronic Signatures“ the US American health agency FDA
(Food and Drug Administration) regulates the production and processing of
electronic documents for pharmaceutical development and production.
This results in requirements for measuring devices used for corresponding
applications. The following features ensure that the Protos 3400 modular
process analysis system meets the demands of FDA 21 CFR Part 11:
Electronic Signature
Access to the device functions is regulated and limited by individually adjust-
able codes – “Passcodes“. This prevents unauthorized modification of device
settings or manipulation of the measurement results. Appropriate use of these
passcodes makes them suitable as electronic signature.
Audit Trail Log
Every change of device settings can be automatically recorded and docu-
mented in the Audit Trail Log on the SmartMedia card. The recording can be
encrypted.
Conformity with FDA 21 CFR Part 11

10
Software Version
MS 3400(X)-160 Module
Protos 3400 device software
The MS 3400(X)-160 module is supported by software version A.1 or higher.
Module software MS 3400(X)-160
Software version 2.x
Menu Display Device description
Device hardware and software
version
Provides information on all modules
installed: Module type and function,
serial number, hardware and software
version and device options.
Select the different modules (FRONT,
BASE, slots 1 - 3) using the arrow keys.
Device description
Return
22.7 °C
7.00 pH
Operating panel Protos
Module FRONT 3400-011
Hardware: 1.1, Software: A.2
Serial number: 08150815
BASE
Module FRONT
Query actual device/module software
When the analyzer is in measuring mode:
Press menu key, open Diagnostics menu: Device description
Options
Device description
Return
22.7 °C
7.00 pH
Digital sensors
Module MS 3400-160
Hardware: 1, Software: 2.0
Serial number: 471101147
BASE
Module FRONT
Options
Query module software
Module MS 3400-160,
"Digital sensors",
hardware and software version,
serial number – here installed in
slot3.

11
Modular Concept
Basic unit, measuring module, additional functions
Documentation
The basic unit is accompanied by a CD-ROM containing the complete
documentation.
Latest product information as well as user manuals for earlier software releases
are available at www.knick.de.
The Protos 3400(X) is an expandable modular process analysis system.
The basic unit (Front and Base modules) provides three slots which can be
equipped by the user with any combination of measuring or communication
modules. The software capabilities can be expanded by additional functions
(options). Additional functions must be ordered separately. They are supplied
with a device-specific TAN for function release.
3 module slots
for free combination of
measuring and communication
modules
Measuring modules
• pH / ORP / Temp
• O2/ Temp
• Noncontacting conductivity / Temp
• Contacting conductivity / Temp
• MS (Memosens interface)
Additional functions
Activation via device-
specific TAN
SmartMedia card
Data recording
ProgaLog 3000
Windows® software for
parameter setting and
data evaluation
Protos 3400(X) Modular Process Analysis System
Communication modules
• OUT (additional switching and
current outputs)
• PID (analog and digital controller)
• Profibus PA
• Foundation Fieldbus
• FIU (Memosens and probe controller)
(software occupies 2 slots)
• Unical/Uniclean probe controller

12
Short Description
Short Description: FRONT Module
Transflective LC graphic display
(240 x 160 pixels)
white backlighting, high resolution
and high contrast.
Red LED
signals failure (On) or maintenance
request/function check (blinking)
according to NE 44.
4 captive screws
for opening the analyzer
(NOTICE! Make sure that the gasket between FRONT
and BASE is properly seated and clean!)
Green LED
Voltage supply okay
5 self-sealing cable glands
M20 x 1.5
for entry of voltage supply and signal lines
2 softkeys
with context-sensitive functions.
User interface
with plaintext menus as recom-
mended by NAMUR.
Menu texts can be switched to:
German, English, French, Italian,
Swedish/Portuguese or Spanish.
Intuitively acquirable menu logic,
based on Windows standards.
Control panel
3 function keys
(menu, meas, enter)
and 4 arrow keys for menu selection
and data entries
Measurement display
Secondary displays
24.0°C 25.8°C

13
Measuring
Short Description: Menu Structure
Basic functions: Calibration, maintenance, parameter setting, diagnostics
Calibration Maintenance Parameter setting Diagnostics
Menu groups
1
2
3
1147 2958 1246
Operator level
1989
Administrator level
Passcode:
Selection of
further menu
items:
Module 1
Module 2
Module 3
BASE
Module 1
Module 2
Module 3
SYSTEM
FRONT
BASE
Module 1
Module 2
Module 3
Message list
Point of meas
description
Logbook
Device description
FRONT
BASE
Module 1
Module 2
Module 3
4
56
Legend:
1) Pressing the menu key accesses menu selection.
2) Pressing the meas key returns to measurement.
3) Menu groups are selected using the arrow keys
4) Press enter to confirm, enter passcode
5) Further menu items are displayed
6) Selected functions of the Diagnostics menu can be recalled
via softkey even when in measuring mode

14
Short Description: FRONT Module
View into the open device (FRONT module)
Terminal plates
of “hidden” modules
Each module comes with an adhesive
label containing the contact assign-
ments. This label should be sticked to
the inner side of the front (as shown).
Then, the terminal assignments remain
visible even if further modules are
inserted.
Slot for SmartMedia card
• Data recording
The SmartMedia card expands the
measurement recorder capacity to
>50,000 records.
• Exchange of parameter sets
5 parameter sets can be stored on the
SmartMedia card, 2 of them can be
loaded simultaneously to the analyzer
and be switched by remote control.
Parameter sets can be transmitted
from one analyzer to the other.
• Function expansions are possible
with additional software modules,
which are released using transaction
numbers (TAN).
• Software updates
The circumferential sealing
guarantees IP 65 protection and allows
spray cleaning / disinfection.
NOTICE! Be sure to keep it clean.
Replacing the front module
Pull off power cord and ground wire.
To separate the FRONT module from
the BASE module, turn the retaining screws
of the pivot hinge by 90°.

15
Short Description: BASE Module
View into the open device (BASE module, 3 function modules installed)
BASE module
2 current outputs (free assignment of
process variable) and 4 relay contacts,
2 digital inputs.
VariPower broad-range power supply unit,
20 ... 265 V AC/DC, suitable for all public
mains supplies in the world.
Power supply units, Ex version:
100 ... 230 V AC or
24 V AC/DC
Important notice concerning SmartMedia card
The SmartMedia card may be inserted or replaced with the power supply
switched on. Before removing a memory card, you must “close” it in the main-
tenance menu. When closing the device, make sure that the sealing is properly
seated and clean.
Module equipment
Module identification: Plug & Play.
Up to 3 modules can be combined as
desired. Several input and communica-
tion modules are available.
WARNING!
Do not touch the terminal compartment,
there may be dangerous contact voltages!

16
Terminal Plate
Attaching the terminal plates
The terminal plates of the lower modules can be
sticked to the inner side of the door. This facilitates
maintenance and service.
Terminal plate of MS 3400-160 module:

17
Terminal Wire color Wiring for Memosens or M12 cable
1Brown (BN) Power supply +
2 Transparent Shield
3Green (GN) RS485 (A)
4Yellow (YE) RS485 (B)
5White (WH) Power supply – (GND)
Wiring and Memosens Cable
The connecting cable consists of an inductive connector for digital Memosens®
sensors (bayonet lock). It allows connecting the ferrule-terminated wires from
the sensor loop of the transmitter.
Specifications
Material PEEK
Cable diameter 6.3 mm
Cable 2x2, twisted wire pairs
Length up to 100 m
Ambient temperature -20 °C ... 135 °C
Ingress protection IP 68
Order Codes
Cable type Cable length Order code
Memosens® cable 3 m CA/MS-003NAA
5 m CA/MS-005NAA
10 m CA/MS-010NAA
20 m CA/MS-020NAA
Other lengths available on request.
M12 cable 5 m CA/M12-005NA
10 m CA/M12-010NA
20 m CA/M12-020NA

18
Menu Display Viewing level, Operator level,
Administrator level
Open parameter setting
From the measuring mode:
Press menu key to select menu.
Select parameter setting using arrow
keys, press enter to confirm.
Administrator level
Access to all functions, also passcode
setting.
Releasing or blocking functions for
access from the Operator level.
Parameter Setting: Operating Levels
Viewing level, Operator level, Administrator level
Note: HOLD mode (Setting: BASE module)
Functions which can be blocked for
the Operator level are marked with
the "lock" symbol.
The functions are released or blocked
using the softkey.
Operator level
Access to all functions which have
been released at the Administrator
level. Blocked functions are displayed
in gray and cannot be edited (Fig.).
Viewing level
Display of all settings.
No editing possible!
Menu selection
Return to meas
25.6 °C
11.03 pH
Select: [enter]
Lingua
Parameter setting
Return
25.6 °C
11.03 pH
Viewing level
Administrator level (All Data) adm
(Operation Data) opl
(All Data) view
Operator level
Module FRONT (Administrator)
Return
25.6 °C
11.03 pH
Language
Measurement display
KI recorder
English
Measurement recorder
Release
Module FRONT
Return
25.6 °C
11.03 pH
Measurement display
KI recorder
English
Measurement recorder
Language

19
Menu Display Administrator level:
Enabling / locking a function
Example: Blocking access to the
calibration adjustments from the
Operator level
Open parameter setting
Select Administrator level.
Enter passcode (1989).
Select “Memosens PH” (for example)
using arrow keys,
press enter to confirm.
Parameter Setting: Locking a Function
Administrator level: Enabling/locking functions for Operator level
Note: HOLD mode (Setting: BASE module)
Select “Cal preset values” using arrow
keys, “Block” with softkey.
Now, the “Cal preset values” line is
marked with the “lock” icon.
This function cannot be accessed from
the Operator level any more.
The softkey function changes to
“Release”.
Open parameter setting
Select Operator level, passcode (1246),
select “Memosens PH”, for ex. Now, the
locked function is displayed in gray and
marked with the “lock” icon.
Memosens PH (Administrator)
25.0°C
Return
Sensor data
Cal preset values
11.03 pH
Delta function
Messages
TC process medium
Input filter
Block
Memosens PH (Administrator)
25.0°C
Return
Sensor data
Cal preset values
11.03 pH
Delta function
Messages
TC process medium
Input filter
Release
Memosens PH (Administrator)
25.0°C
Return
Sensor data
Cal preset values
11.03 pH
Delta function
Messages
TC process medium
Input filter
Parameter setting (Administrator)
System control
Return
25.6°C
Module BASE 3400-021
82.3 % Air
Memosens PH
Module FRONT 3400-011
Module MS 3400-160

20
05/23/2010 9:32
Configuring the Measurement Display
Select menu: Parameter setting/Module FRONT/Measurement display
Pressing meas (1) returns the analyzer to the measuring mode from any
function.
All process variables coming from the modules can be displayed. The table on
the next page describes how to configure the measurement display.
Secondary displays
Additional values, also date and
time, can be displayed depending
on the modules installed.
Measurement display
Typical measurement display
1
Softkeys
In measuring mode, the softkeys
allow selection of values for the
secondary displays or control of
functions (user defined).