Agilent Technologies G6600 Guide

Purpose
The Brass Burner has two ceramic combustion tubes which require periodic
replacement: an inner and an outer tube.
Scope
This procedure applies to ceramic tube replacement in the Agilent Instruments
ABI 00003 Brass Burner.
Tools
•2 - 1/16” Open End Wrenches
•2 - 3/8” Open End Wrenches
•2 - 7/16” Open End Wrenches
Procedure
1. Turn off the Interface Controller and let the system cool down under
vacuum.
The Burner is extremely hot when running. Do not touch the burner until it has
cooled down.
2. Turn off the vacuum pump.
3. Remove the hydrogen line by disconnecting the Hydrogen Inlet Fitting at
the top of the Burner. Use a second wrench to hold the Adapter Tee to
avoid excess torque on the ceramic tubes.
4. Disconnect the black PFA transfer line from the Tee of the Burner
Interface.
5. Unscrew the Tee fitting and carefully pull the inner Tube/Tee assembly
from the Burner. If the existing Tube is broken then all fragments must
be removed from the burner.
Note
Ceramic Probe Replacement
Instructions
Accessory G6600-60034

2
6. Remove the ferrule attached to the top of the 1/8” ceramic tube.
7. Disconnect the Heater Cable from the heating element leads.
The heating element leads are very fragile. Do not bend them excessively or they
will be damaged.
8. Disconnect the thermocouple leads from the Interface Controller.
9. Remove the four horizontal socket head cap screws holding the Burner
Case.
10. Carefully lift the Burner Case up off of the base and set it aside.
11. Remove the white insulating disk and the fiber insulating toroid from the
Burner base.
12. Remove the 1/8” ceramic tube by loosening the nut in the Burner base.
Discard the used ceramic tube and ferrule. Remove any debris from the
inside of the connection.
Screw extractors may be useful in removing old ferrules from Burner fittings.
Note
Note

3
13. Insert the new 1/8” ceramic tube into the fitting with a new Vespel
ferrule. Slide the nut over the tube and tighten it until finger tight. Lift
the ceramic tube up 1 to 2 mm so that it will not be crushed by the
compression fitting. Tighten the nut snugly with the 7/16” wrench. This
connection must be fairly tight to ensure that the nut does not loosen
under heat stress, but excessive tightening can crack the ceramic tube.
14. Reinstall the fiber insulating toroid and the white insulating disk.
Carefully slide the Burner Cover over the large ceramic tube. It is often
useful to sight down the upper fitting to ensure that the ceramic tube is
properly aligned and will not break.
Failure to install the insulating disk may lead to leaks in the Burner.
15. Reinstall the four screws at the base of the Burner.
16. Unscrew the Hydrogen Inlet fitting from the Tee, and remove the 1/16"
tube and ferrule.
Note

4
17. Install a new 1/16" Vespel ferrule at the top of the Tee. Slide in a new
inner ceramic tube until approximately 1/8" (2 mm) extends out of the
top of the ferrule Retighten the Hydrogen Inlet fitting snugly. Do not
overtighten the fitting.
18. Replace the Tube and Tee assembly into the Burner, tightening finger
tight.
19. Check the flow of air and hydrogen following the Detector manual
instructions.
20. Reconnect the Heater Cable, Thermocouple, and all the tubing. Pressure
test the system following the instructions in the Detector manual. The
pressure may change slightly due to variation in tube dimensions.
21. Turn on the Interface Controller and allow the Burner temperature to
stabilize. Gently tighten all the fittings once the Burner temperature is
stable.

Copyright © 2007
Agilent Technologies, Inc.
2850 Centerville Road
Wilmington, DE 19808-1610
Printed in the USA Feb 2007