artisan LiQuilaz-S Series User manual

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LIQUILAZ®-S
Liquid Particle Counter
Operations Manual
P/N M10195
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[phone] 1-800-238-1801 FAX: [phone]
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Customer Response Center: 1-877-475-3317
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LiQuilaz®-S
Liquid Particle Counter
Operations Manual
P/N M10195 Rev M
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ii
LiQuilaz-S Liquid Particle Counter Operations Manual
P/N M10195 Rev M
© 2009 by Particle Measuring Systems, Inc.
All rights reserved
LiQuilaz®is a registered trademark of Particle Measuring Systems, Inc.
Kalrez®is a registered trademark of E. I. du Pont de Nemours and Company.
Flaretek®is a registered trademark of Entegris, Inc.
KEL-F®is a registered trademark of 3M
Micro-90® is a registered trademark of the International Products Corporation
Radiacwash™ is a trademark of Biodex Medical Systems, Inc.
Super Floss® and Oral-B® are registered trademarks of Procter & Gamble.
Teflon®is a registered trademark of E. I. du Pont de Nemours and Company.
All trademarks appearing in this manual are the property of their respective owners.
This confidential document contains proprietary information, which is protected by
copyright. All rights are reserved. No part of this document may be reproduced,
distributed, or transmitted in any form without the prior written consent of Particle
Measuring Systems. The information contained in this document is subject to change
without notice.
Quality Statement
The Quality Policy of Particle Measuring Systems is to strive to meet or exceed the needs
and expectations of our customers and to align the activities of all employees with the
common focus of customer satisfaction through continuous improvement in the quality of
our products and services.
Environmental Information
This equipment must be properly disposed of at end-of-life by means of an authorized
waste management system. Information regarding dismantling of the equipment and
location of any hazardous materials can be located on our web site at:
http://www.pmeasuring.com/support/papers/disassemblyinstructions.
DO NOT REPRODUCE OR DISTRIBUTE CONFIDENTIAL DOCUMENT
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iii
Manual Conventions
NOTE: A note in the text is used to highlight an item that is of operational
importance to the user.
It is important that you observe cautions and warnings while performing the procedures
described in this manual. Caution and warning labels are located on and inside the
instrument to alert you to potentially hazardous conditions. Please familiarize yourself with
this information.
WARNING
A warning in the text is used to notify the user of the potential for bodily injury or
death.
CAUTION
A caution in the text is used to highlight an item that if not done, or incorrectly
done, could damage the instrument and/or any materials or devices affected by
the instrument.
– — NOTICE — –
A notice in the text is an instructional communication regarding requirements or
policies issued by Particle Measuring Systems.
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iv
CE – Declaration of Conformity
- Declaration of Conformity
Application of Council Directive(s): 2004/108/EC, 2006/95/EC
Standard(s) to which Conformity is Declared: EMC EN 61326-1: 2006
Safety EN 61010-1: 2001
Manufacturer’s Name: Particle Measuring Systems, Inc.
Manufacturer’s Address: 5475 Airport Boulevard, Boulder, CO 80301 USA
Manufacturer’s Telephone/FAX: [phone]
Distributor’s Name: Particle Measuring Technique, Great Britain
Distributor’s Address Unit B1 South, Willow End Park
Danemoor, Malvern WR14 1XZ
Worchestershire, WR13 6NN United Kingdom
Distributor’s Telephone/FAX: [phone]
Type of Equipment: Particle Monitoring
Model No: LiQuilaz-SO2/SO3/SO5-HF
I, the undersigned, hereby declare that the equipment specified above conforms to the above
Directive(s) and Standard(s).
Signature: Signature:
Full Name: John Mitchell Full Name: David Hall
Position: Vice President Engineering Position: Managing Director
Place: Boulder Date: June 18, 2008 Place: Malvern Date: June 18, 2008
CAUTION
All I/O cables and accessories must meet current factory specifications in order for this unit
to remain in compliance with CE marking requirements. Consult the factory for details.
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LiQuilaz-S Liquid Particle Counter Operations Manual v
Table of Contents
Quality Statement - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -ii
Environmental Information - - - - - - - - - - - - - - - - - - - - - - - - - - - - -ii
Manual Conventions- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -iii
CE – Declaration of Conformity- - - - - - - - - - - - - - - - - - - - - - - - - -iv
Chapter 1: Getting Started - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 1-1
Specifications - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -1-2
Chapter 2: Unpacking and Installation - - - - - - - - - - - - - - - - - - - - - - - 2-1
Unpacking - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-1
Identifying Components and Connections - - - - - - - - - - - - - - - - - -2-1
Liquid Connections- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-1
Indicator Lights - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-1
Communications Connectors - - - - - - - - - - - - - - - - - - - - - - - -2-3
Installation Requirements - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-4
AC Fuse - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-4
Installation - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -2-5
Appendix A: Capillary Cleaning - - - - - - - - - - - - - - - - - - - - - - - - - - - - A-1
Cleaning the Capillary - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -A-1
Applying Additional Capillary Cleaning Techniques - - - - - - - - - - -A-2
Appendix B: Communication Protocol - - - - - - - - - - - - - - - - - - - - - - - B-1
Instrument Initialization - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-1
Sample Initiate - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-1
Data Processing- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-2
Slow Polling - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-2
Fast Polling - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-3
Slow Protocol - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-3
Slow Protocol Commands - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-6
Commands and Responses- - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-7
Format for Calibration String - - - - - - - - - - - - - - - - - - - - - - - -B-9
Fast Protocol- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-11
Formatting Data- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -B-13
Appendix C: International Precautions- - - - - - - - - - - - - - - - - - - - - - - C-1
WARNING- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-1
AVERTISSEMENT- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-1
WARNUNG - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-1
ATTENZIONE - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-1
PRECAUSION - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-1
Hazard Symbols- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-2
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vi LiQuilaz-S Liquid Particle Counter Operations Manual
Table of Contents
Symboles de risque - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-2
Warnschilder- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-3
Simboli di pericolo- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-3
Simbolos de peligro - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -C-4
Appendix D: 有毒或有害的物质和元素 - - - - - - - - - - - - - - - - - - - - - - - - D-1
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LiQuilaz-S Liquid Particle Counter Operations Manual vii
List of Figures
Figure 1-1: LiQuilaz-S Liquid Particle Counter- - - - - - - - - - - - - - - - - - - - - - - - - - -1-1
Figure 2-1: LiQuilaz-S Liquid Particle Counter (Front View) - - - - - - - - - - - - - - - - -2-2
Figure 2-2: LiQuilaz-S Liquid Particle Counter (Rear Panel)- - - - - - - - - - - - - - - - - -2-3
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viii LiQuilaz-S Liquid Particle Counter Operations Manual
List of Figures
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LiQuilaz-S Liquid Particle Counter Operations Manual Page 1-1
Chapter 1
Getting Started
The LiQuilaz®-S liquid particle counter is a sensor designed to measure particles in
liquids. The sensor contains the liquid handling and optical system as well as the
necessary electronics to measure the size of the particles sampled and to transmit
this information to the data display system. The sensor requires AC power,
connections to bring the liquid to the sensor, and a connection to the data display
system.
Particle Measuring Systems supplies several software packages supporting the
LiQuilaz-S liquid particle counter depending upon the application.
The following are the sensitivities of LiQuilaz-S sensors:
•0.5 μm (S05)
•0.3 μm (S03)
•0.2 μm (S02).
All models have a sapphire capillary.
Figure 1-1: LiQuilaz-S Liquid Particle Counter
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Page 1-2 LiQuilaz-S Liquid Particle Counter Operations Manual
Chapter 1: Getting Started
Specifications
LiQuilaz-S liquid
particle counter models
SO2 SO3 SO5
Size range 0.2–2.0 µm 0.3–3.0 µm 0.5–20.0 µm
Size channels 15
Flow rate (mL/min.) 50 ± 10% 80 ± 10% 80 ± 10%
Volume sampled 100%
Maximum
concentrationa
a. Greater than 90% accuracy (less than 10% coincidence loss) at maximum recommended
concenation
10,000 per mL
Sample temperatureb
b. 100°C for sulfuric acid
0–150 ° C
Zero count level ≤ 25 counts per liter ≤ 15 counts per liter ≤ 15 counts per liter
Maximum psi 100
Laser source Diode laser
Wetted surface
materials
Sapphire, Teflon®, Kalrez® 4079, or Kel-F®
Dimensions (l, w, h) 12.75 × 4.25 × 4.5 inches (32.4 × 10.8 × 11.4 cm)
Weight 6.1 pounds (2.8 kg)
Power 85–132 V, 50–60 Hz
220-240V, 50-60 Hz
Fuses 85–132 VAC: 0.75 Amp, 3 AG SB/250 V
220–240 VAC: 0.63 Amp, T5 x 20 mm 250 V
Communications RS-485
Calibration fluid DI water
Calibration Materials used are traceable to USA NIST and/or
Japanese Industrial Standards (JIS).
Environment Temperature: 10–35 ° C Humidity: non-condensing
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LiQuilaz-S Liquid Particle Counter Operations Manual Page 2-1
Chapter 2
Unpacking and Installation
Unpacking
To unpack your shipment
1Open the container.
2Carefully remove the instrument and inspect it for damage.
3If the instrument has been damaged in shipment, notify the shipper and Particle
Measuring Systems. Repackage the instrument in the original packing
materials.
4If the instrument is not damaged, store the packing materials.
Identifying Components and Connections
Liquid Connections
The liquid connections to the LiQuilaz-S liquid particle counter are made through
either the 3 mm connections directly on the sensor or through the Flaretek®
connections on the interface bracket. Refer to Figure 2-1, “LiQuilaz-S Liquid
Particle Counter (Front View).” Sensors configured to operate with samplers will
typically utilize 3 mm tubing. Sensors configured to operate online will typically
utilize 1/4” (6 mm) Flaretek fittings.
Indicator Lights
An activity light is located on the front panel next to the liquid connections. The
LED is illuminated upon detection of each particle, interrogation of the sensor, and
failure of the laser. This indicator is used to easily verify proper operation of the
unit.
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Page 2-2 LiQuilaz-S Liquid Particle Counter Operations Manual
Chapter 2: Unpacking and Installation
Figure 2-1: LiQuilaz-S Liquid Particle Counter (Front View)
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Identifying Components and Connections
LiQuilaz-S Liquid Particle Counter Operations Manual Page 2-3
Communications Connectors
Two DE9 (female and male) connectors on the rear panel allow connection to the
data display system. When one is used, the other is available for daisy chain
connection to other sensors on the network.
A standard IEC AC power entry module, with a power switch, is located on this
panel.
Figure 2-2: LiQuilaz-S Liquid Particle Counter (Rear Panel)
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Page 2-4 LiQuilaz-S Liquid Particle Counter Operations Manual
Chapter 2: Unpacking and Installation
Installation Requirements
AC Fuse
The fuse drawer in the sensor’s power entry module permits the use of either of two
types of fuse, depending on the line voltage.
To replace a fuse
1Unplug the power cord from rear panel of the LiQuilaz-S liquid particle counter.
2Use a small blade screwdriver, or similar tool, to remove the cover/fuse drawer
from the power entry module (located on the instrument rear panel).
3Choose the proper fuse according to the table below.
4Reinstall the cover/fuse drawer assembly.
Power 85–132 VAC, 50–60 Hz
or 220-240 VAC, 50-60 Hz
Data cable 5 wire RS-485 (DE9)
Pin 1 shield
Pin 2 Tx +
Pin 3 Tx -
Pin 4 Rx +
Pin 5 Rx -
Pin 6 sample +
Pin 8 sample −
Liquid connections 3 mm zero dead volume fitting
or 1/4-inch Flaretek
85–132 VAC 0.75 Amp
3 AG SB/250 V
220–250 VAC 0.63 Amp
T5 x 20 mm 250 V
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Installation
LiQuilaz-S Liquid Particle Counter Operations Manual Page 2-5
Installation
To install the particle sensor
1Connect a standard IEC AC power cord to the rear panel power module (Figure
2-2).
2Connect the DE9 data cable between the sensor and the data display system.
NOTE: If more than one sensor is to be connected to the data
display system, they can be daisy chained through this sensor.
If connection to an RS-232 communications port is to be made, it is
necessary to use an RS-232 to RS-485 converter in this line.
3Connect the liquid supply line to the appropriate connector on the front of the
sensor.
NOTE: Although there is no directional requirement by the sensor
for flow, Particle Measuring Systems recommends that the flow travel
into the bottom connection and out of the top connection. This will
help prevent bubbles from becomingtrapped in the samplecell by the
fluid flow.
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Page 2-6 LiQuilaz-S Liquid Particle Counter Operations Manual
Chapter 2: Unpacking and Installation
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LiQuilaz-S Liquid Particle Counter Operations Manual Page A-1
Appendix A
Capillary Cleaning
This is a basic guide to maintenance for LiQuilaz liquid particle counters.
Occasional cleaning is required of the liquid capillary and it is the customer's
responsibility to perform the cleaning when necessary. The need for capillary
cleaning and the general health of the capillary can be improved by continuously
running water through the system when not in use. In addition, the capillary should
never be allowed to dry out as this could permanently damage the capillary.
Cleaning the Capillary
To clean the liquid capillary using syringes
1Isolate the LiQuilaz liquid particle counter from its fluid source.
2Disconnect the fluid inlet and outlet fittings from the LiQuilaz liquid particle
counter.
3Select an appropriate cleaning solution.
WARNING
Before removing the LiQuilaz liquid particle counter from a CLS-700
sampler, make sure the sample inlet and outlet tubes are first
connected together, or directed into an appropriate drain. Failure to
do so could result in severe personal injury, as water from the
sampler will be forced out of the open tubing under pressure.
CAUTION
Do NOT remove the 4-40 socket head screws from the fittings. Doing so will
compromise the capillary seal and result in fluid leaking onto circuit boards
and extensive damage. Only remove 3mm zero dead volume fittings from
the inlet/outlet connections.
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Page A-2 LiQuilaz-S Liquid Particle Counter Operations Manual
Chapter A: Capillary Cleaning
NOTE: When selecting an appropriate cleaning solution, consider
the types of contamination that will have deposited onto the capillary
from the most recent fluid sampled. For instance, if DI water was
sampled last, bacteria, or particles are the most likely sources of
contamination. If solvents were sampled last, optical hazing due to
chemical impurities is most likely. Both of these situations can be
easily remedied using high-quality laboratory glassware cleaner such
Micro-90® or Radiacwash™. A 5% solution of glassware cleaner in
ultra-pure DI water should be used.
4Fill each cleaning syringe with 5ml of cleaning solution.
5Attach one cleaning syringe to the particle counter inlet, and the other to particle
counter outlet.
6Force the cleaning fluid back and forth between the two syringes for 30 seconds
to one minute.
7Remove syringes, being careful not to spill fluid into gaps between metal
sections of particle counter housing. Immediately wipe up any spills.
8Connect the LiQuilaz liquid particle counter inlet to a source of ultra-pure
deionized water. Direct the LiQuilaz liquid particle counter outlet to a drain
suitable for the cleaning fluid. Flush the cleaning fluid from particle counter for
3-5 minutes with DI water.
9Check the DC light using the provided software. If the DC light fails to meet the
following sensor specifications, repeat cleaning with syringes until successful.
10 If a series of cleaning attempts is unsuccessful in cleaning the syringe, follow
the cleaning procedure in “Applying Additional Capillary Cleaning
Techniques” or return the LiQuilaz liquid particle counter to Particle Measuring
Systems Service Department.
Applying Additional Capillary Cleaning Techniques
In cases where polymers were sampled, the most likely cause of contamination is
trace polymer dried to the capillary. In this case, the polymer will probably require
long term soaking in the appropriate solvent to facilitate removal of the
contaminant.
DC Light Specifications
LiQuilaz-S liquid particle counter, model S02 < 0.5 volts
LiQuilaz-S liquid particle counter, model S03/S05 < 0.03 volts
LiQuilaz-S liquid particle counter, model E20P > 7 volts
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