EYELA A-1000S User manual

Instruction
Manual
A-1000S
Tokyo Rikakikai Co., Ltd.
Aspirator
R00
This manual includes important information concerning the maintenance of
the functionality of the product and safety use.
Please keep this instruction manual within easy reach of yourself whenever using the product.
IMPORTANT
Please read this manual carefully especially on
“Safety precautions”before use.

Safety precautions
1. Signal word for warning
Though we are trying to look into conceivable risk of using the product, it is very
difficult for us to expect all of it. It means that all the instructions in this manual
do not cover all the types of risks that may be caused by the product. However, if you
follow the instructions, you surely can handle and operate the product safely.
Please sue extreme care when handling this product and try to prevent all the potential
accidents and mechanical failures.
Alert mark
Signal word Definition
WARNING Mishandling the product may cause serious personal injury
or loss of life.
CAUTION Mishandling the product may injure users or cause serious
property damage.
・
Due to its function and characteristic,
a part of this product rotates rapidly
and suctions organic solvent. Contamination
of foreign substance and insufficient
drainage treatment may damage the product.
However, if you have proper information,
you can avoid almost all these troubles.
Therefore, this manual categorizes the
level of importance and danger as below
with alert mark and signal word.
Please follow the instructions and use
the product safely.

Thank you for choosing the product of
Introduction
This instruction manual describes the procedure of
setup, operation, troubleshooting, maintenance, check-up and disposal
of Aspirator, A-1000S.
Please read this manual carefully before use.
Please check the type and quantity of each part before setting up the instrument.
Check-up list of packing
Product
Contents
1 Pump 1
21
3Cover for bath 1
1
Instruction manual
4
1
2
5
6
A-1000S
7
Fuse 115V(3A)
220V 240V(2A)
1
Y-shaped joint
Contents
1. Outline of the product
1-1 Use application
1-2 Specification
1-3 Characteristic of water vapor pressure
1-4 Achievement level of vacuum degree(reference)
1-5 Option
1-6 Name of each part
1-7 Safety function
2. Setup
2-1 Setup environment
2-2 Utility connection
1
1
2
2
3
4
2
4
5
3. Operation
3-1 Preparation
3-2 How to operate
3-3 How to operate optional accessories
(Nozzle with vacuum gauge・Controlling
decompression valve)
3-4 How to operate optional accessories
(Cooling coil)
4. Troubleshooting
5. Maintenance・check-up
6. Disposal of the product
7. After-sale service
6
8
11
12
12
13
8
9
Vacuum hose 2
Bath
Pump Bath
Cover for bath

1
Outline of the product
1
1-2 Specification
This product is a decompression device that decreases the pressure of condenser,
such as rotary evaporator, test tube evaporator and centrifugal evaporator.
1-1 Use application
Do not remodel the product.
Make sure that it should not be
used out of intended use.
WARNING
Remodeling and improper use may cause
electric shock or breakdown.
Product name
Model
Maximum exhaust
velocity
Attainable vacuum
degree
Motor
Aspirator
Bath
Drainage system
External measurement
Power source input
Rated supply
Weight
Aspirator
A-1000S
Induction motor Output 150W
255 (W)×361 (D)×406 (H) mm
300W
AC115V 60Hz AC220V 50/60Hz AC240V 50Hz
6.7kg
Depends on saturated water vapor pressure
Suctioning nozzle
Metal
2 points External diameter 9mm
Over flow system
(External diameter of nozzle 17.5mm)
16 / 19 L/min(50/60Hz)
Polypropylene 10L
※ Attainable vacuum degree differs depending on dissolved gas or
impurity dissolving into water.
Feature Configuration Specification

2
1-4 Attainable vacuum degree(reference)
1-3 Characteristic of water vapor pressure
1-5 Option
(2)
※Nozzle with vacuum gauge is used for checking up
attainable vacuum degree of aspirator and controlling
vacuum degree.
Water
temperature (mmHg)
kPa
5℃
10℃
20℃
0.93 (7)
1.60 (12)
2.66 (20)
※Attainable vacuum degree differs depending on
dissolved gas or impurity dissolving into water.
Product name
Model
Cat. No.
Cooling coil
CCU(copper) CCS(SUS)
119050 119060
(1)
※ Cooling coil is used for cooling down the water in
the bath by connecting to external circulating nozzle
of low temperature circulator(CA-1112 and etc.)with
using hose.
Water
vapor
pressure
〔kPa〕
10 20 30 40
Water temperature〔℃〕
0
10
20
30
40
50
60
0
1
2
3
4
5
6
7
8Water vapor pressure
〔mmHg〕
0
External
diameter12mm
Product
name
Model
Cat. No.
Controlling
decompression valve
212380210550
Nozzle with
vacuum gauge
VG-1000VVG-1000
VG-1000 VG-1000V

3
1-6 Name of each part
Feed water nozzle
Cooling coil cap
Over flow nozzle
Suction nozzle
(2 points)
Cap nut
Assembly drawing
Main body
Pump casing
Shielding plate
Casing cover
Metal aspirator
(2 points)
F cheese
Manifold
Motor base
Power code
Bath
Fuse holder
(Only one fuse holder has 115V)
Cover for bath
Power code

Safety functions
Safety device Operation Reasons why safety device works
Fuse Gets fuse blew and cuts off
the power Excess current flows.
This product is equipped with safety functions as below.
However, when trouble occurs, please refer to “Troubleshooting”on page 10
and follow the proper instructions.
1-7 Safety functions
2-1 Setup environment
Setup2
Bad setup environment may damage
the product and worsen the function.
WARNING
Be careful with setup environment
Select the setup location as below.
No inflammable solid, liquid and gas around the unit.
Range of ambient temperature is from 5℃ to 35℃.
No dew condensation
Fewer humidity and dripping
Fewer dust
No direct sunlight
Good ventilation
Even and stable
Since the unit uses water, water leakage must flow into
drain when leak of water occurs.
●
●
●
●
●
●
●
●
●
4
Thermal protector Stops motor.
(Motor re-starts up when
temperature lowers).
Motor is heated exceptionally

2-2 Utility connection
(1)Check the voltage, phase and capacity of
power source connecting to the product.
Required power source is as shown on right
table.
(2)Make sure of the type of outlet and plug mains connector.
Model
A-1000S
Required power source
Capacity
AC115V 15A
Voltage
Excess current may burn cable or cause
fire.
WARNING
Do not use branching socket and
power strip.
Wrong connection may cause fire or
electric shock.
WARNING
Make sure of the voltage, phase,
capacity and the type of outlet. Do not connect earth wire to gas pipe or
water pipe for preventing electric shock.
WARNING
Connect earth wire properly.
When connecting to power source, do not
use branching socket and power strip.
5
AC220V
AC240V
7A
7A

3-1 Preparation
(1)Place the main body on the bath and
set it up on the point of use.
(2)Remove the cap of water supplying
nozzle.
(3)Install hose for drainage (bore diameter:
16mm) onto overflow nozzle and also install
water-supplying hose (bore diameter: 12mm)
onto water-supplying nozzle tightly for
preventing leak.
(4)Connect decompression system and suctioning
nozzle with using vacuum hose (bore diameter:
6mm).
※When reducing the pressure at only one point,
using two suctioning nozzles with Y-shaped joint
simultaneously can shorten the time required for
decompression.
Operation
3
6
Pump and aspirator that are clogged with
dust and cotton waste will worsen the
attainable vacuum degree. Also, they will
cause glitch on motor.
CAUTION
Make sure that no foreign
substance such as dust is adhered in
the bath.
If the organic solvent is dissolved into
the water, attainable vacuum degree will be
worsened or metal aspirator and driving part
will be damaged. Also, it may cause nasty
smell or fire.
When suctioning organic solvent,
use trap and do not let solvent
mix into the bath.
CAUTION
Notice 1 When water temperature in the bath
rises during the operation, it may worsen
the attainable vacuum degree, and water in
the bath may flow upstream. Therefore,
circulate the cooling water or conduct
overflow to keep the same water temperature
for avoiding the trouble. Also, use
store-bought backflow prevention valve. Water supplying hose
Hose for drainage
Over flow
nozzle
Water supplying
nozzle
Y-shaped joint
Vacuum hose
1. Connecting hose
Sucking in
※ When the solution can not perform overflow for
maintaining water temperature because of
effluent regulation, use cooling trap to
prevent the interfusion or change the water
in the bath regularly.
Notice 2 When the solvent mixes into the bath,
it will worsen the attainable vacuum
degree and may cause back-flow.
Also, when the solution vapors, it may
cause nasty smell or fire.
※ Attainable vacuum degree of the unit depends
on water temperature and water quality.
※ When water can not be overflowed, it is effective
to use immersion cooler or cooling water circulating
device combining with cooling coil, which is one of
the options.

7
Fill the water into the bath up to the point
where flow nozzle supplies water.
※If the water supply is too much, water may
overflow from the bath.
※Though the water supply is controlled
properly, it may be changed because of the
change of water pressure. Pay attention to
the water level during overflow.
2. Water supplying into bath
Make sure that the power switch is off before plugging the mains connector into outlet.
3.Connecting mains connector
Water-
supplying
Decreasing pressure at 2 points simultaneously
※ When releasing decompression at one
decompression container and sucking in air,
air bubble will be sucked into the pump
and attainable vacuum degree will be
worsened. In this case, water may flow
upstream into other decompression container.
When decreasing pressure in both containers,
set up stop cock in each decompression line
and close the stop cock before releasing the
decompression.
To drain
Stop cock
Decompression
container
Decompression
container

8
3-3 How to operate options
(Nozzle with vacuum gauge attached VG-1000、Controlling decompression valve
with vacuum gauge attached VG-1000V)
Vacuum gauge
Inlet nipple
Leak valve
Cap
3-2 How to operate
(1)Turn on power switch.
Pump rotates and metal aspirator exhausts
and starts reducing pressure.
※When starting it up, exhaust sound is loud
because of huge displacement.
※Use cover for bath if it is possible.
It prevents water scattering when releasing
decompression.
※After checking up that the suctioning
nozzle and decompression system are surely
connected, turn on power switch.
If they are not connected, water bubble
may overflow from the bath.
(2)When completing operation, turn off power
switch after releasing decompression.
(1)Turn cap nut and remove suctioning nozzle and
rubber packing on the one side.
Pay attention not to lose rubber packing.
(2)After removing cap nut, place rubber packing
on the part of motor base where screw is fixed,
and insert VG-1000 or VG-1000V and turn cap
nut to fix it.
※ Do not insert VG-1000 or VG-1000V
with a slope.
(3) Connect inlet nipple of VG-1000 or
VG-1000V to vacuum hose and also connect
to decompression system.
(4)To control vacuum degree, unloose the leak valve
slowly with reducing pressure and also reduce vacuum
degree gradually and set up at your desired
vacuum degree(VG-1000V).
※ Instruction for using VG-1000 and VG-1000V
When getting the condition back to normal
pressure, do not pull out vacuum hose with
a sudden jerk or get the condition back to
normal pressure hastily. Releasing
decompression rapidly may break a vacuum gauge.
When getting it back to normal condition,
please pull out the vacuum hose gradually from
inlet nipple or loosen the leak valve slowly.
(only for model VG-1000V).
Procedure after finishing operation
If you don not use the product for a long time,
turn off the power switch and unplug the mains
connector. Also, drain the water of the bath.
Cap nut
Rubber packing
Motor base
VG-1000V
VG-1000
Turn
and
fix
Vacuum gauge
Inlet nipple
Cap
※This unit is equipped with backflow
prevention valve that prevents backflow
caused by huge pressure difference, which
was occurred when power switch is turned off
by mistake. However, since backflow
progresses little by little if decompression
is continued for a long time, please release
the decompression. Also, store-bought backflow
prevention valve is available.
In case of trouble, release the decompression
and turn off power switch immediately, and
refer to “Troubleshooting”.
Stop using the product if it does not
work properly.
CAUTION

(1) Remove cover for bath from main body.
Fit the lamp part of cooling coil into
the edge of bath and set up cooling coil
in the bath.
(3)Remove cooling coil cap from the cover for bath.
3-4 How to operate options(cooling coil CCU and CCS)
9
Cooling coil
Metal part
Bath
(2) Fit the main body into bath
バス
※To get a rough guide, the point where cooling coil
should be attached is about 4cm from the center of
exterior part of coil to the edge of the bath.
Approx.4cm
Cover for bath
Remove it
Cooling coil cap
※When using model CCU,
cut off approx. 1mm of
two clicks.
Then, cooling coil can
be fit in smoothly.
※Cooling coil cap can be attached once again.
Main body
Bath

(5)Please proceed the pipe fitting as below.
※Two types of cooling coil are available, which are
type CCU that is made of copper, and type CCS that is
made of SUS304.
Cooling water
circulating device Evaporator
Cooling coil
Cover for bath
10
Cooling coil
Cover for bath
Slot
Roll it
Curve of
cooling
coil
Completed
(4) Setting up cover for bath
Fit the slot of the cover into the pipe of
cooling coil.
※ When using the cover for bath without
cutting about 1mm of clicks (model CCU),
turn the cover along the curve of cooling
coil, then fit the cover into bath.
(Cooling coil can be attached once again
after use).

Troubleshooting
4For the trouble that is not mentioned in this manual,
please consult your local dealer or closest customer
service center.
T r o u b l e Cause of trouble S o l u t I o n
Solvent is dissolved into water.
Remove the clogged dirt.
Corrosion or wear of metal aspirator Replace metal aspirator.
Poor air volume
displacement
Stop the operation
immediately and contact your
local dealer or closest
customer service center.
Dirt clogged in the pump casing.
Abnormal noise occurs
when motor works.
Stop the operation immediately
and contact your local dealer or
closest customer service center.
Poor vacuum degree.
Metal aspirator is clogged.
Pump part is cracked.
Water leaks from casing packing.
Remove the dirt in the casing.
Motor does not work
even though power switch
is turned on.
Mains connector is unplugged.
Or it is not plugged tightly.
Power is not supplied.
Fuse blows.
Replace fuse. If it still does
not work out, stop the operation
immediately and call your local
dealer or closest customer service
center.
Turn on the breaker of the
distribution board.
Turn off the power switch and
plug the mains connector into
outlet.
Oil seal and bearing are worn.
Motor is damaged.
Water temperature in the bath is high.
Replace the water of
aspirator bath or do not let
solvent mix into the water.
Use the unit with performing
Overflow or put the cooling coil
into the bath and connect to
cooling water circulating device
to cool down the water temperature.
F cheese of pump part is damaged
because of organic solvent.
Metal aspirator is clogged with
foreign substance.
11
Lower the ambient temperature
or lower the water temperature
of the bath.
Thermal protector works.
Backflow prevention valve is clogged
Backflow prevention valve is
clogged.
Remove the dirt.

12
(1)When cleaning and caring the product,
turn off the power switch and unplug
the mains connector.
(2)For cleaning, use soft cloth after screwing
water tightly. Use mild detergent the remove
greasy dirt and wipe it off
after using the detergent.
Use appropriate product for cleaning
and caring the unit in proper way.
When cleaning and caring the product, do
not pour water directly on the exterior
and internal part of the unit, and also
do not use cleanser, thinner, petrol,
lamp oil, acid and related products.
These products may cause electric shock
or damage the unit.
CAUTION
※Checking up piping and etc.
Before and after use, check up
the piping system for leaks, slackness
or whether the hose is deteriorated.
Since the progress of deterioration
or obsolescence of the product differ
depending on the use condition, please
check the machine regularly.
Maintenance・checkup
5
Cleaning and caring the product.
Do not take down the product.
A part of interior portion of the unit is
under electric pressure and subject to have
high temperature. Therefore, breaking down
the unit may cause electric shock or injure
yourself.
WARNING
※Dispose packing materials by separating each type of material.
Please follow the instruction as below when disposing the product or parts.
Disposal of the product
6
Major components and the method of disposing
Contact waster
disposer.
Component Specification How to dispose
A-1000S
Weight External measurement
6.7kg 255(W)×361(D)×406 (H) mm
Main body

1.When the machine does not work properly,
check and see whether it has breakdown with
referring to pages of “Troubleshooting.”
2.If you are sure that it has a breakdown,
contact your local dealer or closest customer
service center, which is mentioned on the manual.
3. Repair work during guarantee period is
available based on service warranty.
After-sale service
7
13
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