FLUXANA VITRIOX ELECTRIC Parts list manual

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FXBA‐0072‐17    1/42
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VITRIOX®ELECTRIC
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Usermanualandtechnicaldescription
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Manufacturer:
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FLUXANA®GmbH&Co.KG
Borschelstr.3
D‐47551Bedburg‐Hau
Tel.+49(0)2821/48011‐10
Fax.+49(0)2821/48011‐99
E‐mail:[email protected]
Homepage:http://www.fluxana.com
Serviceandsupport:
FLUXANA®GmbH&Co.KG
Borschelstr.3
D‐47551Bedburg‐Hau
Tel.+49(0)2821/48011‐10
Fax.+49(0)2821/48011‐99
E‐mail:[email protected]
Homepage:http://www.fluxana.com

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FXBA‐0072‐17    2/42
TableofContents
1.Overview
1.1 ProductDescription
1.2 Overviewofthesystem
1.3 Technicaldata
1.4 Models
1.5 ProtectiveHousing
1.6 Hoodwithfan
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2.WarrantyandLiability
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3.Safety
3.1 IntendedUse
3.2 Requirementsofthesystemoperator
3.3 Requirementsoftheoperatingpersonal
3.4 Protectiveclothing
3.5 Basicmeasuresfornormaloperation
3.6 Behaviorincaseofemergency
3.7 Basicmeasuresforupkeepandmaintenance
3.8 Safetysymbols
3.9 Generaldangersofthesystem
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4.Transport,SetupandInstallation
4.1 Delivery
4.2 Unpacking
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5.OperatingElements
5.1 Frontplate
5.2 Tiltedview
5.3 Generaltechnicaldescription
5.4 Mainscreen(touchscreen)
5.5 Sequenceforafusionprocess(withoutextracoolingstation)
5.6 Sequenceforafusionprocess
5.6.1 User
5.6.2 Autosampler
5.6.3 Errorlist
5.6.4 Createnew/changeapplication
5.6.5 Selecting,changingandsavinganapplication
5.6.6 Copyinganapplication
5.6.7 Time,nightshut‐off
5.6.8 Showingthetemperature
5.6.9 SavingandloadingapplicationsonaUSBdevice
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6.WorkingwiththeVITRIOX®ELECTRIC
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7.Warrantyconditionsforsamplepreparationmachines
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8.ECDeclarationofConformity

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FXBA‐0072‐17    3/42
1.Overview
1.1ProductDescription
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TheVITRIOX®ELECTRICisafusioninstrumentforsamplepreparation for X‐ray
fluorescence analysis. Thefusionchamberisheated by systematically arranged
heatingelementsthatareisolatedfromthefusionchamber.Inthisway,itispossible
toachieveidealheatingofthefusionchamber.Temperaturedetermination is
conductedwithaspecialthermoelement.Thefusionchambercanbeheatedtoupto
1250°C.
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Withthecoldtocoldoperation,eachindividualsampleexperiencesthesameenergy.
Rotationmixingenablesthemachinetoachieveideallymixedhomogeneoussamples.
Themachineisdeliveredwithaprotectivehousing(personnelandprocessprotection)
andamirrorontheceilingoftheovenforobservationoftheovenchamber.
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Additionalcharacteristicsoftheproductinclude:
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 Microprocessorcontrolforthestorageofupto10differentapplicationprograms
 Heatgenerationbyheatingelements
 Ovenwiththermallyinsulatingmaterials(Inside:fusiontemperature;Outside:
lukewarm)
 Temperaturedistributionthroughall‐roundheatingoftheovenchamber
 Exhaustventintheceiling
 TypeBorSthermoelements(dependingonmodel)
 Switchingsystemwithphase‐anglefiringthyristors
 Liftwithflooropening
 Mixingbyhighspeedrotation(upto250rpm,bidirectional)
 CrucibleholderandovenfloormadefromfusionresistantFLUXinert®ceramic(no
attackfromlithiumtetraborate;easilycleanedwithdilutedHCl)
 Autosamplerforautomaticprocessingofupto6samples
 Modularsystemenablesupgradetoupto6positions
 Optional:additionalstationforcontinuousoperation(loadingandunloadingof
samplesduringthefusionispossible)
 Optional:Useofcruciblelidsfortheanalysisofvolatileelements,likeF,ClorS
 Optional:OvenceilingmadefromFLUXinert®ceramic
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FXBA‐0072‐17    4/42
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1.1 Overviewofthesystem
Frontsideoftheoven:
1. Fusionchamber
2. Display(Touchscreen)
3. EmergencyStopbutton
4. Powerswitch
5. USB‐Connection
6. Bottomholder(Reservoir)
7. Bottominsolation
8. Rotationunit
9. Setupstation
10. Extracoolingstation
11. Mirror
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Rearsideoftheoven:
1. Powersupply
2. Airsupply
3. LAN‐Connection
4. Autosampler
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FXBA‐0072‐17    5/42
1.3TechnicalData
TechnicalData1Station2Stations
4Stations/
2StationswithCOO
6Stations/
4StationswithCOO
Voltage:
230V/208V
50‐60Hz
230V/208V
50‐60Hz
230V/208V
50‐60Hz
230V/208V
50‐60Hz
Power:3000W 3000W 3000W 3000W
Powersupply:
1~AC/16A
2~AC/16A
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IEC60309
Powerplug**
1~AC/16A
2~AC/16A
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IEC60309
Powerplug**
1~AC/16A
2~AC/16A
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IEC60309
Powerplug**
1~AC/16A
2~AC/16A
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IEC60309
Powerplug**
Temperatures:Upto1,250°C Upto1,250°C Upto1,250°C Upto1,250°C
Permissibleair
pressure6bar 6bar 6bar 6bar
Air
consumption:max.1.5m³/hr max.1.5m³/hr max.1.7m³/hr max.1.9m³/hr
Length:860mm 1115mm 1315mm 1515mm
Depth:750mm 750mm 750mm 750mm
Height:
900mm(without
mirror)
1055mm(withmirror)
900mm(without
mirror)
1055mm(withmirror)
900mm(without
mirror)
1055mm(withmirror)
900mm(without
mirror)
1055mm(withmirror)
Weight:~120kg ~120kg ~135kg ~150kg
**IEC60309powerplug:
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