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Radleys Carousel 6 Plus User manual

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Instructions
Cooled Carousel 6 Plus™
Reaction Station
Your Local Distributor
February 2023 | Issue 5
Radleys, Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom.
Tel: +44-1799-513320 Fax: +44-1799-513283
Email: [email protected]m Web: www.radleys.com
These instructions should be read in conjunction
with the Carousel 6 Plus and Stirring Hotplate Instructions.
Page 1
Cooled Carousel 6 Plus Reaction Station
Index
Page 1 Index
Page 2 1. Introduction
Page 3 2. Warranty
3. Safety Information
4. Important WARNINGS
Page 4 5. Product Component Guide
Page 5 6. Products & Accessories
Page 6 6. Products & Accessories - Continued
Page 7 6. Products & Accessories - Continued
Page 8 6. Products & Accessories - Continued
Page 9 7. Glassware
Page 10 7. Glassware - Continued
Page 11 8. Quick Start Guide
Page 12 9. Set-Up & Operation
Page 13 9. Set-Up & Operation - Continued
Page 14 9. Set-Up & Operation - Continued
Page 15 9. Set-Up & Operation - Continued
Page 16 9. Set-Up & Operation - Continued
Page 17 9. Set-Up & Operation - Continued
Page 18 10. Safe handling of cooling fluids
11. Cooling Mixture Appendix
Page 19 12. Radleys/Genevac Compatibility Chart
Page 20 WARRANTY - EMAIL BACK
Page 2
Cooled Carousel 6 Plus Reaction Station
1. Introduction
Thank you for purchasing your Cooled Carousel 6 Plus Reaction Station.
Please read this Instruction Manual thoroughly before operating your unit.
The Cooled Carousel 6 allows chemists to perform stirred, sub-ambient reactions in a range of
round bottom flasks from 5ml to 250ml with the option of an inert, moisture free atmosphere.
Features...
• Simultaneously performs up to six cooled and stirred reactions to -78˚C.
• Powerful, even stirring - reservoir fits on to a Carousel stirring hotplate.
• Robust HDPE cooling reservoir is compatible with a wide range of cooling mixtures, including
dry-ice/acetone for manually controlled cooling from ambient down to -78˚C.
• Insulated foam core maintains low temperatures for long periods, whilst protecting the stirrer
from freezing.
• Insulation also reduces condensation and ice formation on outer surfaces of reservoir.
• HDPE lid keeps your reaction cooler for longer, minimises ice formation on your flasks (maintaining visibility of the contents) and prevents
spitting from the cooling mixture.
• Round design makes all reaction flasks visible and allows easy addition of reagents and solvents, with no need to lean into the fumehood.
Whats NEW...
• Easy-on PTFE caps feature a ‘quick-thread’ for a gas tight seal to flasks.
• Easy to clean contoured surface.
• Exclusive wide neck flasks with quick coupling for improved sealing and ease of use.
Page 3
• Please read these instructions completely before using your Cooled Carousel 6 Plus Reaction Station.
• The Cooled Carousel is NOT suitable for heated reactions.
• Operate only in a fumehood with protective safety sash.
• The Carousel Reaction Flasks are not designed for pressurised reactions. DO NOT PRESSURISE ABOVE 1psi.
• Reactor Head - Chemical Resistance - the aluminium Carousel reactor head is resistant to the majority of solvents and splash resistant
to dilute acids and alkalis at room temperature. Extended exposure to acids or alkalis will attack the surface of the Carousel. The stronger
the concentration and the longer the exposure time the more chance and intensity of any attack. It is important to clean off any residual
chemical spills immediately after they occur.
• Cooling Reservoir - Chemical Resistance - The cooling reservoir is manufactured from a HDPE polymer which is compatible with the
freezing mixtures listed in Section 11. Cooling Mixture Appendix on page 18 of this manual.
• Ensure that the heating control on the stirring hotplate is switched off and that the hotplate is cool before using the Cooled Carousel.
• Cooling solvents such as acetone are extremely flammable. Always follow appropriate safety instructions and chemical handling
procedures.
Page 3
Warning
Applies when there is a possibility
of personal injury.
Important Note
Alerts the user to important facts.
!
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important Note
The Cooled Carousel should only be operated by trained and competent personnel. As with all chemistries, a full risk
assessment should be performed prior to starting an experiment, and care should be taken to monitor your reactions at all
stages. The Carousel should not be left unattended unless in a supervised area.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
3. Safety Information
4. Important WARNINGS
The Cooled Carousel 6 Plus Reaction Station includes one year full parts and labour warranty from date of original purchase.
Warranty will only be valid if a completed Warranty Fax Back is returned within 1 month of date of purchase (see last page). In the event of
product failure please contact your local distributor.
Please do not return any goods without prior agreement.
2. Warranty
Cooled Carousel 6 Plus Reaction Station
The following symbols are intended to assist the user in the safe and efficient operation of the Cooled Carousel 6 Plus Reaction Station.
Page 4
Cooled Carousel 6 Plus Reaction Station
Easy-On PTFE Caps & Septa
Reactor Head
HDPE Reservoir
Central Gas Inlet
Stirring Hotplate
HDPE Stand
Easy-On Cap
Reflux Tube
Rodaviss
Connecting Set
Flask
Easy-On Cap
Flask with integrated
Reflux Tube
Easy-On Cap
Wide Neck Reflux Tube
Wide Neck Coupling
Wide Neck Flask
Stirring Bars
HDPE Lid
5. Product Component Guide
Hole for
temperature probe
Connector Pins
Page 5
Cooled Carousel 6 Plus Reaction Station
6. Products & Accessories
Heated System - Basic
System 34
RR99943 Carousel 6 Plus System
1 x RR99916 Carousel 6 Plus Reaction Station
1 x RR91070 Easy-On PTFE Cap, pk 6
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
1 x RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
1 x RR99043 B24/29 Rodaviss Sealing Cap, pk 10
1 x RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
1 x RR99061 Reaction Flask Support Ring, pk 6
1 x RR99064 Elliptical Stirring Bar 25mm RE, pk 10
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
Heated System - Additions
System 35
RR99944 Carousel 6 Plus System
1 x RR99916 Carousel 6 Plus Reaction Station
1 x RR91070 Easy-On PTFE Cap, pk 6
1 x RR91202 Carousel Tech Stirring Hotplate 230v UK Plug
1 x RR91210 Carousel Temperature Controller
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
1 x RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
1 x RR99043 B24/29 Rodaviss Sealing Cap, pk 10
1 x RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
1 x RR99061 Reaction Flask Support Ring, pk 6
1 x RR99064 Elliptical Stirring Bar 25mm RE, pk 10
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
1 x RR99077 B24/29 250ml Reaction Flasks with Sidearm + Septa Port, pk 6
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99079 B24/29 Solid Additions Funnel, pk 3
1 x RR99082 PTFE/Silicone Septa 29mm for B24/29, pk 50
Heated System - Basic + Hotplate
System 33
RR99942 Carousel 6 Plus System
1 x RR99916 Carousel 6 Plus Reaction Station
1 x RR91070 Easy-On PTFE Cap, pk 6
1 x RR91202 Carousel Tech Stirring Hotplate 230v UK Plug
1 x RR91210 Carousel Temperature Controller
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
1 x RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
1 x RR99043 B24/29 Rodaviss Sealing Cap, pk 10
1 x RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
1 x RR99061 Reaction Flask Support Ring, pk 6
1 x RR99064 Elliptical Stirring Bar 25mm RE, pk 10
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
180˚C
180˚C
180˚C
Page 6
Carousel 6 Plus Reaction Station
6. Products & Accessories
Cooled System - Comprehensive
System 39
RR99950 Cooled Carousel 6 Plus System
1 x RR99947 Cooled Carousel 6 Plus (Reservoir, Head, Stand + Cover)
1 x RR98024 Protective Cold Temperature Gloves
1 x RR91070 Easy-On PTFE Cap, pk 6
1 x RR91202 Carousel Tech Stirring Hotplate 230v UK Plug
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
1 x RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
1 x RR99043 B24/29 Rodaviss Sealing Cap, pk 10
1 x RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
1 x RR99054 100ml Reaction Flask, pk 6
1 x RR99061 Reaction Flask Support Ring, pk 6
1 x RR99064 Elliptical Stirring Bar 25mm RE, pk 10
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
1 x RR99077 B24/29 250ml Reaction Flasks with Sidearm + Septa Port, pk 6
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99079 B24/29 Solid Additions Funnel
1 x RR99905 Digital Thermometer (-250˚C to +400˚C) + 200mm Probe
1 x RR99908 Dry Ice Scoop
1 x RR99909 Cold Temp. Apron 1060mm long Waterproof
1 x RR99910 Protective Face Shield
-78˚C
Cooled System - Upgrade
System 38
RR99949 Cooled Carousel 6 Plus System
1 x RR99947 Cooled Carousel 6 Plus (Reservoir, Head, Stand + Cover)
1 x RR98024 Protective Cold Temperature Gloves
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
1 x RR99905 Digital Thermometer (-250˚C to +400˚C) + 200mm Probe
1 x RR99908 Dry Ice Scoop
1 x RR99909 Cold Temp. Apron 1060mm long Waterproof
1 x RR99910 Protective Face Shield
Heated System - Comprehensive
System 36
RR99945 Carousel 6 Plus System
1 x RR99916 Carousel 6 Plus Reaction Station
1 x RR91070 Easy-On PTFE Cap, pk 6
1 x RR91202 Carousel Tech Stirring Hotplate 230v UK Plug
1 x RR91210 Carousel Temperature Controller
1 x RR98076 Silicone Septa for PTFE Caps, pk 100
1 x RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
1 x RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
1 x RR99043 B24/29 Rodaviss Sealing Cap, pk 10
1 x RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
1 x RR99054 100ml Reaction Flask, pk 6
1 x RR99920 250ml Azeotropic Reaction Flask, pk 3
1 x RR99920 250ml Azeotropic Reaction Flask, pk 3
1 x RR99058 Aluminium Insert for 100ml Reaction Flask, pk 6
1 x RR99061 Reaction Flask Support Ring, pk 6
1 x RR99064 Elliptical Stirring Bar 25mm RE, pk 10
1 x RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
1 x RR99077 B24/29 250ml Reaction Flasks with Sidearm + Septa Port, pk 6
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99078 B24/29 Liquid Additions Dropping Funnel with Pressure Equalising Arm, pk 3
1 x RR99079 B24/29 Solid Additions Funnel, pk 3
1 x RR99082 PTFE/Silicone Septa 29mm for B24/29, pk 50
This system does not include reaction flasks, stirring hotplate etc and
is intended for those users who already have a heated Carousel 6 Plus.
-78˚C
180˚C
Page 7
Cooled Carousel 6 Plus Reaction Station
6. Products & Accessories - Continued
Carousel 6 Plus Reaction Station
Carousel 6 Plus
RR99916 Carousel 6 Plus Reaction Station
Carousel 6 Plus Systems
RR99942 Carousel 6 Plus System 33 - Heated System - Basic + Hotplate
RR99943 Carousel 6 Plus System 34 - Heated System - Basic
RR99944 Carousel 6 Plus System 35 - Heated System - Additions
RR99945 Carousel 6 Plus System 36 - Heated System - Comprehensive
Glassware
Standard Flasks & Reflux Tubes
RR99151 5ml Reaction Flask with B14/23 Neck, pk 6
RR99148 10ml Reaction Flask with B14/23 Neck, pk 6
RR99923 B14/23 Reflux Tube + Connecting Set, pk 6
RR99145 25ml Reaction Flask, pk 6
RR99070 50ml Reaction Flask, pk 6
RR99054 100ml Reaction Flask, pk 6
RR99052 170ml Reaction Flask, pk 6
RR99041 250ml Reaction Flask, pk 6
RR99917 250ml Reaction Flask + Reflux Tube + Connecting Set, pk 6
RR99918 B24/29 Reflux Tube + Connecting Set, pk 6
RR99919 250ml Long Neck Reaction Flask, pk 6
Standard Flasks with Sidearms
RR99071 50ml Reaction Flask with B14/23 Sidearm + Septa Port, pk 6
RR99074 100ml Reaction Flask with B14/23 Sidearm + Septa Port, pk 6
RR99077 250ml Reaction Flask with B24/29 Sidearm + Septa Port, pk 6
RR99047 250ml Reaction Flask with B14/23 Sidearm + Septa Port, pk 6
RR99087 250ml Reaction Flask with 2x B14/23 Sidearms + Septa Port, pk 6
RR99088 250ml Reaction Flask with 2x B24/29 Sidearms + Septa Port, pk 6
RR99089 250ml Reaction Flask with 1x B14/23 + 1x B24/29 Sidearm + Septa Port, pk 6
Wide Neck Flasks with Coupling
RR99924 Wide Neck Reflux Tube + Coupling
RR99925 Coupling for Wide Neck Flasks
RR99940 PTFE Wide Neck Support Collar
RR99941 Nitrile O-Ring for PTFE Wide Neck Support Collar
RR99926 50ml Wide Neck Flask
RR99928 100ml Wide Neck Flask
RR99933 250ml Wide Neck Flask
Wide Neck Flasks with Sidearms
RR99927 50ml Wide Neck Flask with B14/23 Sidearm + Septa Port
RR99929 100ml Wide Neck Flask with B14/23 Sidearm + Septa Port
RR99930 100ml Wide Neck Flask with 2x B14/23 Sidearms + Septa Port
RR99934 250ml Wide Neck Flask with B24/29 Sidearm + Septa Port
RR99935 250ml Wide Neck Flask with 2x B24/29 Sidearms + Septa Port
Wide Neck Flasks with Baffles & Sidearms
RR99931 100ml Baffled Wide Neck Flask with B14/23 Sidearm + Septa Port
RR99932 100ml Baffled Wide Neck Flask with 2x B14/23 Sidearms + Septa Port
RR99936 250ml Baffled Wide Neck Flask with B24/29 Sidearm + Septa Port
RR99937 250ml Baffled Wide Neck Flask with 2x B24/29 Sidearms + Septa Port
Azeotropic Glassware
RR99922 100ml Azeotropic Reaction Flask, pk 3
RR99920 250ml Azeotropic Reaction Flask, pk 3
RR99939 100ml Tornado Azeotropic Reaction Flask, pk 3
RR99938 250ml Tornado Azeotropic Reaction Flask, pk 3
Liquid & Solid Addition Funnels
RR99049 B14/23 Solid Additions Funnel, pk 3
RR99079 B24/29 Solid Additions Funnel, pk 3
RR99048 B14/23 Liquid Additions Dropping Funnel + Pressure Equalising Arm, pk 3
RR99078 B24/29 Liquid Additions Dropping Funnel + Pressure Equalising Arm, pk 3
Evaporation Adapters, Splash Heads & Evaporation Flasks
RR99045 Rotary Evaporator Adapters Rodaviss B29 Socket to B24 Cone, pk 2
RR99046 Rotary Evaporator Adapters Ordinary B29 Socket to B24 Cone, pk 2
RR99055 Rotary Evaporator Adapters USA 24/40 Socket to B24 Cone, pk 2
RR99083 Splash Head Rodaviss B29 Socket to B24 Cone
RR99084 Splash Head Ordinary B29 Socket to B24 Cone
RR99085 Splash Head USA 24/40 Socket to B24 Cone
RR99053 250ml EZ-2/HT Evaporation Flask (Compatible with Genevac Evaporators), pk 4
Flasks ar NOT suppli d with r flux tub s or PTFE caps, th s must b purchas d s parat ly.
Carousel 6 Plus Accessories
Aluminium Inserts
RR99142 Aluminium Insert for 5ml Reaction Flask, pk 6
RR99141 Aluminium Insert for 10ml Reaction Flask, pk 6
RR99140 Aluminium Insert for 25ml Reaction Flask, pk 6
RR99060 Aluminium Insert for 50ml Reaction Flask, pk 6
RR99058 Aluminium Insert for 100ml Reaction Flask, pk 6
RR99057 Aluminium Insert for 170ml Reaction Flask, pk 6
PTFE Magnetic Stirring Bars
RR98075 Cross Shape Stirring Bar 10mm, pk 40
RR98091 Cross Shape Stirring Bar 16.5mm RE, pk 20
RR98096 Elliptical Stirring Bar 10mm RE, pk 40
RR98097 Elliptical Stirring Bar 15mm RE, pk 20
RR99064 Elliptical Stirring Bar 25mm RE, pk 10
RR98070 Octagonal Stirring Bar 13mm, pk 20
RR98071 Pivot Ring Stirring Bar 12 x 6mm, pk 40
RR98095 PTFE Magnetic Stirring Bar Evaluation Kit, pk 30
RR98094 PTFE Magnetic Stirring Bar Retriever 350mm
RR98114 Magnetic Stirring Bar Restrainer
PTFE Caps & Accessories
RR91070 Easy-On PTFE Cap, pk 6
RR91072 Easy-On PTFE Storage Cap, pk 6
RR98076 Silicone Septa for PTFE Caps, pk 100
RR98176 Viton Septa for PTFE Caps, pk 100
RR98060 O-Rings for Caps - Nitrile 24mm, pk 100
RR98160 O-Rings for Caps - Viton 24mm, pk 100
Replacement O-Rings & Quick Release Couplings
RR91060 Nitrile O-Rings 4mm Gas Outlet - Bottom, pk 50
RR91061 Nitrile O-Rings 3mm Gas Outlet - Top, pk 50
RR91062 Viton O-Rings 4mm Gas Outlet - Bottom, pk 50
RR91063 Viton O-Rings 3mm Gas Outlet - Top, pk 50
RR91065 Qui ck Release Male Body Coupling No Shut-off, pk 2
RR91066 Quick Release Barbed Coupling No Shut-off
RR99062 Quick Release Barbed Coupling + Shut-off, pk 2
RR99063 90˚ Elbow Quick Release Barbed Coupling + Shut-off, pk 2
RR99065 Quick Release Male Body Coupling + Shut-off, pk 2
Rodaviss Caps & Connecting Sets
RR99051 B14/23 Rodaviss Sealing Cap, pk 10
RR99043 B24/29 Rodaviss Sealing Cap, pk 10
RR99955 B14/23 Rodaviss Connecting Set, pk 10
RR99044 B24/29 Rodaviss Connecting Set, pk 10
RR99080 PTFE/Silicone Septa 20mm - B14/23, pk 50
RR99081 PTFE/Silicone Septa 24.5mm - B19/26, pk 50
RR99082 PTFE/Silicone Septa 29mm - B24/29, pk 50
RR99068 B14/23 Rodaviss Connecting Cap, pk 10
RR99090 B24/29 Rodaviss Connecting Cap, pk 10
Other Accessories
RR98906 Black Lab Marker, pk 10
RR99061 Reaction Flask Support Ring, pk 6
RR99067 Tubing for Inert Gas or Reflux Cooling 2 metres
Page 8
Cooled Carousel 6 Plus Reaction Station
6. Products & Accessories - Continued
Storm & Breeze Heating/Cooling Work Stations
Storm & Breeze Work Stations
RR96200 Storm Work Station + Carousel 6 PTFE Insulating Plates
(M24 hose connections)
RR96210 Breeze Work Station + Integral Stand
(M16 hose connections)
RR96220 PTFE Insulating Plates for Carousel 6 Plus
Insulated Hoses
HB6084 Insulated Hose - 100cm long, with M16 thread
HB6085 Insulated Hose - 150cm long, with M16 thread
HB6136 Insulated Hose - 200cm long, with M16 thread
HB6255 Insulated Hose - 300cm long, with M16 thread
HB6784 Insulated Hose - 100cm long, with M24 thread
HB6785 Insulated Hose - 150cm long, with M24 thread
HB6786 Insulated Hose - 200cm long, with M24 thread
HB6787 Insulated Hose - 300cm long, with M24 thread
M16 Hose Adapters & Valves
HB6945 M16 Female to M24 Male Adapter
HB6431 M16 Female to M30 Male Adapter
HB6195 M16 90 Degree Adapter
HB6091 M16 Ball Valve
RR96316 M16 Thread Protection Cap, pk 10
M24 Hose Adapters & Valves
HB6724 M24 Female to M16 Male Adapter
HB6723 M24 Female to M30 Male Adapter
HB9256 M24 90 Degree Adapter
HB9236 M24 Ball Valve
RR96336 M24 Thread Protection Cap, pk 10
M30 Hose Adapters & Valves
HB6454 M30 Female to M16 Male Adapter
HB9268 M30 Female to M24 Male Adapter
HB6461 M30 90 Degree Adapter
HB6451 M30 Ball Valve
RR96348 M30 Thread Protection Cap, pk 10
Thermofluids
HB6164 Silicone Oil -40˚C to +165˚C - 10 litres
HB6162 Silicone Oil -20˚C to +235˚C - 10 litres
HB6479 DWTherm -90˚C to +200˚C - 10 litres
Cooled Carousel 6 Plus Reaction Station
Cooled Carousel 6 Plus
RR99947 Cooled Carousel 6 Plus (Reservoir, Head, Stand + Cover)
Cooled Carousel 6 Plus Systems
RR99949 Cooled Carousel 6 Plus System 38 - Cooled System - Upgrade
RR99950 Cooled Carousel 6 Plus System 39 - Cooled System - Comprehensive
Cooled Carousel 6 Plus Components
RR99501 Cooled Carousel 6 Plus Cooling Reservoir
RR99948 Cooled Carousel 6 Plus Head
RR99503 Cooled Carousel 6 Plus Stand
RR99515 Cooled Carousel 6 Plus Cover (with gas connectors)
Cooled Carousel 6 Plus Accessories
RR99905 Digital Thermometer (-250˚C to +400˚C) + 200mm Probe
RR99906 Digital Thermometer (-250˚C to +400˚C)
RR99907 200mm Temperature Probe
RR99908 Dry Ice Scoop
RR99909 Cold Temperature Apron 1060mm long, Waterproof
RR99910 Protective Face Shield
RR98024 Protective Cold Temperature Gloves
RR71505 Cooling Protection Kit
1 x RR99909 Cold Temperature Apron 1060mm long, Waterproof
1 x RR99910 Protective Face Shield
1 x RR98024 Protective Cold Temperature Gloves
Tornado Plus Overhead Stirring System
Tornado Plus
RR99951 Tornado Plus Overhead Stirring System
RR99230 Universal Support Stand
RR99237 Carousel Temperature Controller with extended 345mm Probe
RR71127 Temp Sensor Support Rod (13mm x 500mm)
RR71120 Support Rod Hotplate Adapter (extension plate)
PTFE Stirring Paddles
RR99240 Centrifugal PTFE Stirrer Paddle, pk 6
RR99241 Centrifugal PTFE Stirrer Paddle, pk 1
RR99244 Anchor PTFE Stirrer Paddle for 100ml Flasks, pk 6
RR99245 Anchor PTFE Stirrer Paddle for 100ml Flasks, pk 1
RR99248 Anchor PTFE Stirrer Paddle for 250ml Flasks, pk 6
RR99249 Anchor PTFE Stirrer Paddle for 250ml Flasks, pk 1
RR99251 Propellor PTFE Stirrer Paddle, pk 6
RR99252 Propellor PTFE Stirrer Paddle, pk 1
RS Overhead Stirrers
Please note that other overhead stirrer options are available on request, please contact Radleys
for further information.
RR91302 RS27 Standard Overhead Stirrer 230v UK Plug
RR91302/EURO RS27 Standard Overhead Stirrer 230v Euro Plug
RR91306 RS37 Digital Plus Overhead Stirrer 230v UK Plug
RR91306/EURO RS37 Digital Plus Overhead Stirrer 230v Euro Plug
RR91308 RS50 Control Overhead Stirrer 230v UK Plug
RR91308/EURO RS50 Control Overhead Stirrer 230v Euro Plug
RR91428 Remote Control for RS50 Control
RR91430 RS232 Interface Cable Stirrer-PC
Spare Parts
RR99952 Quick-Thread Stirrer Guide Assembly
RR99953 Replacement Tubing for RR99952 110mm (Stirrer Guide to gas manifold)
Pl as contact Radl ys for d tails of r plac m nt parts for th Stirr r Guid and Tornado Syst m.
Stirring Hotplates
Tech Stirring Hotplates
RR91202 Carousel Tech Stirring Hotplate 230v UK Plug
RR91202/EURO Carousel Tech Stirring Hotplate 230v Euro Plug
RR91202/JAP Carousel Tech Stirring Hotplate 110v Japanese Plug
RR91202/SWISS Carousel Tech Stirring Hotplate 240v Swiss Plug
RR91202/USA Carousel Tech Stirring Hotplate 115v US Plug
Advanced Stirring Hotplates
RR91204 Carousel Advanced Stirring Hotplate 230v UK Plug
RR91204/EURO Carousel Advanced Stirring Hotplate 230v Euro Plug
RR91204/JAP Carousel Advanced Stirring Hotplate 100V Japanese Plug
RR91204/SWISS Carousel Advanced Stirring Hotplate 230v Swiss Plug
RR91204/USA Carousel Advanced Stirring Hotplate 115V US Plug
Oth r Stirring Hotplat mod ls ar availabl on r qu st...
Temperature Controllers & Sensors
RR91210 Carousel Temperature Controller
Includ s RR71125 T mp S nsor Support Rod and RR71120 Support Rod Hotplat Adapt r
RR91226 Pt1000 S/S Sensor for Carousel Advanced Stirring Hotplate
RR91227 Pt1000 Glass Coated Sensor for Carousel Advanced Stirring Hotplate
RR91228 Temperature Sensor Holder
RR91229 Temp Sensor Support Rod (13mm x 425mm)
RR71127 Temp Sensor Support Rod (13mm x 500mm)
RR71125 Temp Sensor Support Rod (13mm x 340mm)
RR71120 Support Rod Hotplate Adapter (extension plate)
RR91234 RS232 Interface Cable - 15 Pin to 9 Pin
Page 9
7. Glassware
Cooled Carousel 6 Plus Reaction Station
7.1 Standard Flasks...
• Constructed of heavy duty, borosilicate glass.
• Choice of sizes: 5ml, 10ml, 25ml, 50ml, 100ml, 170ml and 250ml.
• Precision engineered round bottom design ensures an excellent fit with the Carousel’s wells, maximising heat transfer.
• Flasks feature a B24/B29 Rodaviss joint for connection to the detachable Reflux Tube.
• The 5ml and 10ml flasks feature a B14/23 Rodaviss joint.
• Reflux Tubes feature a quick-thread, which when combined with PTFE Easy-On Cap, give a gas tight seal up to 1psi.
• Optional single piece 250ml Long Neck design.
• Compatible with magnetic stirring bars and the centrifugal stirrer paddles (Tornado).
• Flasks are NOT supplied with reflux tubes or PTFE caps, which must be ordered separately.
7.2 Standard Flasks with Sidearms...
• Sidearm flasks have all the features of the standard flasks with the addition of either one or two sidearms.
• Flasks are available with B14/23 and B24/29 sidearm options and include Rodaviss caps and sealing septa.
• Sidearms are compatible with Dropping Funnels and Solid Addition Funnels.
7.3 Azeotropic Flasks (Dean & Stark)...
• Unique single piece flasks fit directly into the Carousel 6 Plus, allowing chemists to perform up to six Azeotropic processes in parallel.
• Choice of sizes: 100ml and 250ml.
• Special Tornado version with wider neck is designed to accept centrifugal stirring paddle.
• Flasks feature a replaceable PTFE stopcock for removal of the aqueous phase.
• Feature B14/23 or B24/29 sidearms.
• Sidearms are compatible with Dropping Funnels and Solid Addition Funnels.
RR99145
25ml Flask
RR99151
5ml Flask
RR99148
10ml Flask
RR99070
50ml Flask
RR99054
100ml Flask
RR99052
170ml Flask
RR99041
250ml Flask
RR99918
B24/29 Reflux Tube
+ Connecting Set
RR99923
B14/23 Reflux Tube
+ Connecting Set
RR99917
250ml Flask
+ Reflux Tube
+ Connecting Set
RR99919
250ml Long
Neck Flask
RR99071
50ml Flask with
B14/23 Sidearm
RR99087
250ml Flask with
2 x B14/23 Sidearm
RR99088
250ml Flask with
2 x B24/29 Sidearm
RR99077
250ml Flask with
B24/29 Sidearm
RR99047
250ml Flask with
B14/23 Sidearm
RR99074
100ml Flask with
B14/23 Sidearm
RR99089
250ml Flask with
1 x B14/23 Sidearm
1 x B24/29 Sidearm
RR99922
100ml Azeotropic
Flask
RR99938
250ml Tornado
Azeotropic Flask
RR99920
250ml Azeotropic
Flask
RR99939
100ml Tornado
Azeotropic Flask