Knick Protos 3400 User manual

Latest Product Information: www.knick.de
Protos 3400(X)
Process Analysis System
Protos PHU 3400(X)-110 Communication Module
For Actuating Probe Controllers (Unical / Uniclean)
-Automatic pH Measurement-
The Art of Measuring.
Aktuelle Produktinformation: www.knick.de
Analysenmesssystem
Protos 3400(X)
Betriebsanleitung Messmodul Protos CONDI 3400 (X)-051
zur Leitfähigkeitsmessung mit induktiven Sensoren
Deutsch
The Art of Measuring.
Aktuelle Produktinformation: www.knick.de
Analysenmesssystem
Protos 3400(X)
Betriebsanleitung Messmodul Protos CONDI 3400 (X)-051
zur Leitfähigkeitsmessung mit induktiven Sensoren
Deutsch
User Manual
English

Trademarks
The following trademarks are used in this manual without further marking:
CalCheck®, Calimatic®, Protos®, Sensocheck®, Sensoface®, Unical®, VariPower®, Ceramat®, SensoGate®
are registered trademarks of Knick Elektronische Messgeräte GmbH & Co. KG, Germany
Memosens®
is a registered trademark of
Endress+Hauser Conducta GmbH & Co. KG, Germany
Knick Elektronische Messgeräte GmbH & Co. KG, Germany
SMARTMEDIA®
is a registered trademark of Toshiba Corp., Japan
©2017 Subject to change without notice
Return of products under warranty
Please contact our Service Team before returning a defective device. Ship the cleaned device to
the address you have been given. If the device has been in contact with process fluids, it must be
decontaminated/disinfected before shipment. In that case, please attach a corresponding certificate,
for the health and safety of our service personnel.
Disposal
Please observe the applicable local or national regulations concerning the disposal of
“waste electrical and electronic equipment”.
Knick
Elektronische Messgeräte GmbH & Co. KG
Beuckestr. 22
14163 Berlin, Germany
Phone: [phone] - 0
Fax: [phone] - 200
Web: www.knick.de
Email: [email protected]

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Table of Contents
Protos PHU 3400(X)-110 Module
Return of products under warranty .................................................................................... 2
Disposal ......................................................................................................................................... 2
Trademarks ................................................................................................................................... 2
Intended Use.................................................................................................... 9
Conformity with FDA 21 CFR Part 11.................................................................................. 9
Safety Information ........................................................................................ 10
Application in Hazardous Locations: PHU 3400X-110 Module ...............................10
Software Version ......................................................................................................................11
Modular Concept .....................................................................................................................13
Short Description .......................................................................................... 14
Short Description: FRONT Module ....................................................................................14
Short Description: Menu Structure....................................................................................15
Short Description: BASE Module........................................................................................17
Overview of the System Components .............................................................................18
PHU 3400(X)-110 Module......................................................................................................20
Terminal Plate PHU 3400(X)-110 Module.................................................... 21
Inserting the Module .................................................................................... 22
Wiring Example VP and SixPlug..........................................................................................23
Connecting the Probe Controller................................................................. 25
Menu Selection.............................................................................................. 26
Menu Structure.............................................................................................. 26
Passcode Entry............................................................................................... 27
Changing a passcode.....................................................................................................27
Configuring the Measurement Display ....................................................... 28
Start-Up.......................................................................................................... 30
Parameter Setting: Operating Levels .......................................................... 31
Administrator level .........................................................................................................31
Operator level ...................................................................................................................31
Viewing level.....................................................................................................................31
Parameter Setting: Locking a Function ...........................................................................32

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Table of Contents
Protos PHU 3400(X)-110 Module
Parameter Setting for PHU 3400(X)-110 ..................................................... 33
Activating Parameter Setting ..............................................................................................33
Settings of Sensor Data..........................................................................................................34
Sensoface ....................................................................................................................................36
SW 3400-005: Tolerance Adjustment................................................................................39
Activating the Cal Tolerance Band ............................................................................40
Documenting Parameter Setting.......................................................................................47
ProgaLog 3000 Software (Option) forConfiguration and Documentation .......49
Configuration using "ProgaLog 3000".....................................................................52
Logbook, Factory Setting......................................................................................................53
Configuring a Current Output.............................................................................................54
Current Outputs: Characteristics ........................................................................................55
Output Filter...............................................................................................................................57
NAMUR Signals: Current Outputs ......................................................................................58
NAMUR Signals: Relay Contacts..........................................................................................59
Relay Contacts: Protective Wiring ......................................................................................60
Relay Contacts, Usage ............................................................................................................61
Relay Contacts: Sensoface Messages................................................................................62
Rinse Contact.............................................................................................................................63
Limit Value, Hysteresis, Contact Type................................................................................64
Icons in the Measurement Display ....................................................................................64
OK1, OK2 Inputs: Specify Level ...........................................................................................65
Selecting Parameter Set (A, B) via OK2 Input ................................................................66
Signaling Active Parameter Set via Relay Contact.......................................................66
Unical 9000(X) Parameter Setting ............................................................... 67
Cal Preset Values Unical 9000 .....................................................................................68
Time Control......................................................................................................................68

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Parameter Setting: Program Flows ....................................................................................70
Cleaning (Continuous), Media Monitoring Off.....................................................70
Cal 2point (Continuous), Media Monitoring Off ..................................................71
Cal 1point (Continuous), Media Monitoring Off ..................................................72
Parking.................................................................................................................................74
Measurement (Short-Time), Media Monitoring Off............................................75
Cal 2point (Short-Time), Media Monitoring Off ...................................................76
Cal 1point (Short-Time), Media Monitoring Off ...................................................77
Service .................................................................................................................................78
Configuring the Program Flow...................................................................................79
Entering a Program Name............................................................................................79
Editing a Program Step .................................................................................................79
Configuring a Function .................................................................................................80
Activating Monitoring ...................................................................................................80
Parameter Setting: Installation............................................................................................81
Selecting the Measurement Procedure...................................................................82
External Control via DCS...............................................................................................82
Control via Process Control Cystem (DCS)......................................................................83
Control Programs and Meas. Procedures........................................................................84
Sensor Detection .............................................................................................................85
Probe....................................................................................................................................85
Configuring Media Monitoring...........................................................................................86
Media Adapter..................................................................................................................87
Additional Media (2).......................................................................................................87
Start-Up...............................................................................................................................87
System Forecast (Ceramat, SensoGate) ....................................................... 88
Reference / Probe Travel Profiles ...............................................................................89
Creation of a Probe Travel Profile and Presentation in Protos........................89
Setting the System Forecast Parameters.........................................................................90
System Forecast: Reference Profile ...........................................................................91
System Forecast: Tolerance Specifications.............................................................93
System Forecast: Diagnostic Messages ...................................................................95
System Forecast: RecordingonSmartMediaCard..............................................96
Table of Contents
Protos PHU 3400(X)-110 Module

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Uniclean 900(X) Parameter Setting ............................................................. 98
Measuring Module..........................................................................................................99
Time Control......................................................................................................................99
Parameter Setting: Program Flows ................................................................................. 101
Rinsing (Continuous)................................................................................................... 101
Cleaning (Continuous)................................................................................................ 102
Parking.............................................................................................................................. 104
Measuring (Short-Time) ............................................................................................. 105
Service .............................................................................................................................. 106
Editing a Program Step .............................................................................................. 107
Configuring a Function .............................................................................................. 107
Parameter Setting: Installation......................................................................................... 108
Selecting a Measurement Procedure.................................................................... 109
External Control via DCS............................................................................................ 109
Control via Process Control System (DCS) ................................................................... 110
Control Programs and Meas. Procedures..................................................................... 111
Sensor Detection .......................................................................................................... 112
Probe................................................................................................................................. 112
Media Adapter............................................................................................................... 113
Additional Media (2).................................................................................................... 113
Start-Up............................................................................................................................ 113
Calibration / Adjustment ............................................................................ 114
Calibration Methods ............................................................................................................ 116
One-Point Calibration................................................................................................. 116
Two-Point Calibration ................................................................................................. 116
Three-Point Calibration.............................................................................................. 116
Sensor Replacement (First Calibration)................................................................ 116
Temperature Compensation............................................................................................. 117
Automatic Calibration ......................................................................................................... 118
Manual Electrode Calibration........................................................................................... 120
HOLD Function During Calibration ................................................................................ 122
Table of Contents
Protos PHU 3400(X)-110 Module

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Selecting a Calibration Method....................................................................................... 123
Calimatic Automatic Buffer Recognition ............................................................. 124
Calibration with Manual Entry of Buffer Values ................................................ 126
Product Calibration ..................................................................................................... 128
Calibration by Entering Data from Premeasured Electrodes ....................... 130
ORP Calbration/Adjustment .................................................................................... 132
ISFET Zero Adjustment .............................................................................................. 134
Maintenance of PHU 3400(X)-110..............................................................136
Sensor Monitor....................................................................................................................... 136
Temp Probe Adjustment..................................................................................................... 136
Probe Maintenance via Protos 3400(X)..................................................... 137
Diagnostics Functions.................................................................................141
Point of Meas Description......................................................................................... 141
Logbook........................................................................................................................... 141
Device Description....................................................................................................... 142
Diagnostics of PHU 3400(X)-110 ..................................................................................... 143
Module Diagnostics.............................................................................................................. 143
Sensor Monitor.............................................................................................................. 143
Calibration Timer .......................................................................................................... 144
Tolerance Adjustment................................................................................................. 144
Cal Record ....................................................................................................................... 145
Sensor Network Diagram .......................................................................................... 145
Statistics........................................................................................................................... 145
Diagnostics of Unical 9000(X)........................................................................................... 146
Unical Status................................................................................................................... 146
Unical Network Diagram ........................................................................................... 146
Diagnostics of Uniclean 900(X) ........................................................................................ 147
Uniclean Status.............................................................................................................. 147
Diagnostic Messages of System Forecast..................................................................... 148
Setting Diagnostics Messages as Favorite ................................................ 149
Table of Contents
Protos PHU 3400(X)-110 Module

8
Message List ........................................................................................................................... 151
Messages......................................................................................................152
System Forecast Messages ................................................................................................ 161
Error Messages of Unical 9000(X).................................................................................... 162
Error Messages of Uniclean 900(X)................................................................................. 168
Specifications............................................................................................... 172
Appendix:.....................................................................................................176
Minimum Spans for Current Outputs............................................................................ 176
Buffer Table "Mettler-Toledo"............................................................................................ 177
Buffer Table "Knick CaliMat" .............................................................................................. 178
Buffer Table "DIN 19267" .................................................................................................... 179
Buffer Table "NIST Standard" (DIN 19266: 2000-01).................................................. 180
Buffer Table "Techn. Buffers to NIST".............................................................................. 181
Buffer Table "Hamilton"....................................................................................................... 182
Buffer Table "Kraft"................................................................................................................ 183
Buffer Table "Hamilton A"................................................................................................... 184
Buffer Table "Hamilton B"................................................................................................... 185
Buffer Table "HACH" ............................................................................................................. 186
Buffer Table "Ciba"................................................................................................................. 187
Buffer Table "Reagecon"...................................................................................................... 188
SW 3400-002: Specifiable Buffer Sets ............................................................................ 189
Overview of Parameter Setting..................................................................190
Index............................................................................................................. 196
Menu Selection............................................................................................210
Quick Access.................................................................................................211
Table of Contents
Protos PHU 3400(X)-110 Module

9
Intended Use
In their directive “Title 21 Code of Federal Regulations, 21 CFR Part 11,
Electronic Records; Electronic Signatures“ the US American health agency FDA
(Food and Drug Administration) regulates the production and processing of
electronic documents for pharmaceutical development and production. This
results in requirements for measuring devices used for corresponding applica-
tions. The following features ensure that the Protos 3400(X) modular process
analysis system meets the demands of FDA 21 CFR Part 11:
Electronic Signature
Access to the device functions is regulated and limited by individually adjust-
able codes – “Passcodes“. This prevents unauthorized modification of device
settings or manipulation of the measurement results. Appropriate use of these
passcodes makes them suitable as electronic signature.
Audit Trail Log
Every change of device settings can be automatically recorded and docu-
mented in the Audit Trail Log on the SmartMedia card. The recording can be
encrypted.
Conformity with FDA 21 CFR Part 11
The module is used for simultaneous pH, ORP, and temperature measurement
with glass electrodes. It allows connection of the Unical 9000(X) probe con-
troller for fully automated pH measurement, cleaning, and calibration or the
Uniclean 900(X) for fully automated pH measurement.
The PHU 3400X-110 module is intended for operation in locations subject to
explosion hazards which require equipment of Group II, device category 2(1),
gas/dust.

10
Safety Information
Application in Hazardous Locations
Caution!
Never try to open the module! If a repair should be required, return the module
to our factory.
If the specifications in the instruction manual are not sufficient for assessing
the safety of operation, please contact the manufacturer to make sure that your
intended application is possible and safe.
Application in Hazardous Locations: PHU 3400X-110 Module
The module is approved for operation in hazardous locations.
Observe all applicable local codes and standards for the installation of electrical
equipment in hazardous locations. For orientation, please refer to
IEC 60079-14, EU directives 2014/34/EU and 1999/92/EC (ATEX), NFPA 70 (NEC),
ANSI/ISA-RP12.06.01.
• When installing the device in a hazardous location, observe the specifica-
tions of the EC-Type-Examination Certificate and, if applicable, of the Control
Drawing (download: www.knick.de).
• Before commissioning you must prove that the device may be connected
with other equipment, such as a supply unit including cables and wires.
• In hazardous locations the device shall only be cleaned with a damp cloth to
prevent electrostatic charging.
• Devices and modules which have already been used shall be subjected to
a professional routine test before they may be operated in another zone or
another type of protection.
Be sure to observe during installation:
• Switch off power supply before replacing or inserting a module.
• Protect the signal inputs of the modules against electrostatic discharge.
• Before commissioning it must be proved that the device may be connected
with other equipment.
• Observe correct shielding: To avoid interferences, the cable shielding must
be completely covered by the ESD shielding cap.

11
Software Version
PHU 3400(X)-110 Module
Device Software Protos 3400(X)
The PHU 3400(X)-110 module is supported by software version 5.0
or higher.
Module Software PHU 3400(X)-110
Software version 3.x
Menu Display Device description
Device hardware and software
version
Provides information on all modules
installed: Module type and function,
serial number, hardware and software
version and device options.
Select the different modules (FRONT,
BASE, slots 1 - 3) using the arrow keys.
Device description
Return
22.7 °C
7.00 pH
Operating panel Protos
Module FRONT 3400-011
Hardware: 1.1, Software: A.2
Serial number: 08150815
BASE
Module FRONT
Query actual device/module software
When the analyzer is in measuring mode:
Press menu key, open Diagnostics menu: Device description
Options
Device description
Return
22.7 °C
7.00 pH
Input for pH, ORP and °C
Module PHU 3400-110
Hardware: 1, Software: 3.0
Serial number: 471101147
BASE
Module FRONT
Options
Query module software
Module PHU 3400-110,
hardware and software version,
serial number –
here installed in slot3.

12

13
Modular Concept
Basic unit, measuring modules, additional functions
Documentation
The basic unit is accompanied by a CD-ROM containing the complete
documentation.
Latest product information as well as user manuals for earlier software
releases are available at
www.knick.de.
The Protos 3400(X) is an expandable modular process analysis system.
The basic unit (FRONT and BASE modules) provides three slots which can be
equipped by the user with any combination of measuring or communication
modules. The software capabilities can be expanded by additional functions
(options). Additional functions must be ordered separately. They are supplied
with a device-specific TAN for function release.
3 module slots
for free combination of
measuring and communication
modules
Measuring modules
• pH / ORP / Temp
• O2/ Temp
• Noncontacting conductivity / Temp
• Contacting conductivity / Temp
• Memosens sensors
Additional functions
Activation via
device-specific TAN
SmartMedia card
Data recording
ProgaLog 3000
Windows® software for
parameter setting and
data evaluation
Protos 3400(X) Modular Process Analysis System
Communication modules
• OUT (additional switching and current
outputs)
• PID (analog and digital controller)
• Profibus PA
• Foundation Fieldbus
• FIU (radio, Memosens, Unical)
(software occupies 2 slots)
• Unical probe controller

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Short Description
Short Description: FRONT Module
Transflective LC graphic display
(240 x 160 pixels)
white backlighting, high resolution and
high contrast.
Red LED
signals failure (On) or
maintenance request/function check
(flashing) according to NE 44.
4 captive screws
for opening the analyzer
(Caution! Make sure that the gasket between FRONT and
BASE is properly seated and clean!)
Green LED
Voltage supply okay
5 self-sealing cable glands
M20 x 1.5
for entry of voltage supply and signal lines
2 softkeys
with context-sensitive functions.
User interface
with plaintext menus as recom-
mended by NAMUR.
Menu texts can be switched to:
German, English, French, Italian,
Swedish/Portuguese or Spanish.
Intuitively acquirable menu logic,
based on Windows standards.
Control panel
3 function keys
(menu, meas, enter)
and 4 arrow keys for menu selection
and data entry
Measurement display
Secondary displays
%Air
°C
24.0°C 25.8°C

15
Measure
Short Description: Menu Structure
Basic functions: Calibration, Maintenance, Parameter setting, Diagnostics
Calibration
Maintenance Parameter setting Diagnostics
Menu groups
1
2
3
1147 2958 1246
Operator level
1989
Administrator level
Passcode:
Selection of
further
menu items:
Module 1
Module 2
Module 3
BASE
Module 1
Module 2
Module 3
SYSTEM
FRONT
BASE
Module 1
Module 2
Module 3
Message list
Point of meas
description
Logbook
Device description
FRONT
BASE
Module 1
Module 2
Module 3
4
56
Legend:
1) Pressing the menu key accesses menu selection.
2) Pressing the meas key returns to measurement.
3) Menu groups are selected using the arrow keys
4) Press enter to confirm, enter passcode
5) Further menu items are displayed
6) Selected functions of the Diagnostics menu can be recalled
via softkey even when in measuring mode

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Short Description: FRONT Module
View into the open device (FRONT module)
Terminal plates
of “hidden” modules
Each module comes with an adhesive label
containing the contact assignments. This
label should be sticked to the inner side
of the front (as shown). Then, the terminal
assignments remain visible even if further
modules are inserted.
Slot for SmartMedia card
• Data recording
The SmartMedia card expands the
measurement recorder capacity to
> 50000 records.
• Exchange of parameter sets
5 parameter sets can be stored on the
SmartMedia card, 2 of them can be
loaded simultaneously to the analyzer
and be switched by remote control.
Parameter sets can be transmitted
from one analyzer to the other.
• Function expansions
are possible with additional software
modules, which are released using
transaction numbers (TAN).
• Software updates
The circumferential sealing
guarantees IP 65 protection and allows spray
cleaning / disinfection.
NOTICE! Keep clean!
Replacing the front module
Pull off power cord and ground wire.
To separate the FRONT module from
the BASE module, turn the retaining screws
of the pivot hinge by 90°.

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Short Description: BASE Module
View into the open device (BASE module, 3 function modules installed)
BASE module
2 current outputs (free assignment of pro-
cess variable) and 4 relay contacts,
2 digital inputs.
VariPower broad-range power supply unit,
20 ... 265 V AC/DC, suitable for all public
mains supplies in the world.
Power supply units, Ex version:
100 ... 230 V AC or
24 V AC/DC
Important notice concerning SmartMedia Card
The SmartMedia card may be inserted or replaced with the power supply
switched on. Before a memory card is removed, it must be “closed” in the main-
tenance menu. When closing the device, make sure that the sealing is properly
seated and clean.
Module equipment
Module identification: Plug & Play.
Up to 3 modules can be combined as
desired. Several input and communication
modules are available.
WARNING!
Do not touch the terminal compartment,
there may be dangerous contact voltages!
Note
Only one module can be
connected in addition to a
FIU 3400(X)-140/141 module.

18
Overview of the System Components
Fully Automated Process Analysis System
The fully automated process analysis system consists of the following
components
• Protos 3400(X) (modular process analysis system)
• Unical 9000(X) / Uniclean 900(X) (automatic control of retractable fittings)
• Ceramat WA 150(X) (retractable fitting with ceramic sealing to the process)
The system is operated from the Protos 3400(X). Four operating modes are
provided: calibration, parameter setting, maintenance, diagnostics.
The PHU 3400(X)-110 module consists of 2 functional groups:
• PHU 3400(X)-110 (measuring circuit)
• Unical 9000(X) / Uniclean 900(X) (probe control)
pH
25.6 °C09.03.07
Protos 3400(X) e.g. Unical 9000(X)
Service
switch
Max. 10 m
Max. 10 m
To probe (pH/temp) max. 20 m
Power supply
Compressed air Rinse water
Ceramat WA 150(X)
with pH sensor
Media adapter
with metering
pumps
(calibration buffers,
cleaning agent
Media connection
Max. 10 m

19
Overview of the System Components
Protos 3400(X) Basic Unit and Controller Module for Retractable Fittings
PHU 3400(X)-110 and Unical 9000(X) / Uniclean 900(X) Probe Controller
Module
slot SMARTMEDIA
Protos 3400(X)
OK 1 OK 2
Contacts
K1, K2, K3
Alarm
K4
I 2
mA
I 1
VariPower
0(4) ... 20 mA
pH
Temp
Module
slot
Module
slot
mA
0(4) ... 20 mA
Unical 9000 (X)
or
Uniclean 900(X)
Probe
RTD
Unical
pH, ORP
MΩ, kΩ
Interface
PHU 3400(X)-110
module
Temp
Protos 3400(X) basic unit.
The PHU 3400(X)-110 module is located in one of the 3 module slots available.
PHU 3400(X)-110 controller module for retractable fittings
and Unical 9000(X) / Uniclean 900(X) probe controller:

20
PHU 3400(X)-110 Module
Measuring Circuit and Probe Control Function Blocks
The Protos 3400(X) is an expandable modular process analysis system.
For latest product information, please refer to:
www.knick.de
For a direct access to the function descriptions related to the Unical 9000(X)/
Uniclean 900(X) probe controller, please refer to the overview on the back page
of this manual.
You can document your specific settings for the Unical 9000(X) / Uniclean
900(X) probe controller in the Excel spreadsheet from the CD-ROM
(supplied with Protos 3400(X) or as download at www.knick.de)
Measuring Circuit and Probe Control Function Blocks
Probe Controller
The PHU 3400(X)-110 module allows connection of the Unical 9000(X) probe
controller for fully automated pH measurement, cleaning, and calibration or
the Uniclean 900(X) probe controller for fully automated pH measurement.
Measuring Circuit
Even without the Unical 9000(X) / Uniclean 900(X), the PHU 3400(X)-110
module is a fully fledged pH measuring module for simultaneous pH, ORP and
temperature measurement with glass electrodes.
This instruction manual describes the whole functionality of the
PHU 3400(X)-110 module corresponding to the following menu groups:
• Calibration
• Maintenance
• Parameter setting
• Diagnostics