Micromeritics Saturn II 5205 DigiSizer User manual

Saturn II 5205 DigiSizer
Installation Instructions and Checklist
520-42875-02
July 2009

Windows is a registered trademark of Microsoft Corporation.
Copyright Micromeritics Instrument Corporation, 2009. All rights reserved.

Jul 09 i
Table of Contents
Introduction............................................................................................................................................ 1
Conventions............................................................................................................................................ 1
Symbols.......................................................................................................................................... 1
Commands...................................................................................................................................... 2
Part 1: Installation Instructions ............................................................................................................. 3
Preparing for Installation........................................................................................................................ 3
Equipment Description........................................................................................................................... 4
Analyzer......................................................................................................................................... 4
Liquid Sample Handler .................................................................................................................. 5
AquaPrep........................................................................................................................................ 6
MasterTech 052.............................................................................................................................. 6
Completing the Installation Checklist.................................................................................................... 7
Documenting Installation....................................................................................................................... 7
Inspecting the Equipment....................................................................................................................... 8
Setting up the DigiSizer System ............................................................................................................ 9
Installing the DigiSizer................................................................................................................... 9
Space Requirements .............................................................................................................. 9
Placing the DigiSizer on a Work Surface .............................................................................. 9
Selecting the Voltage Setting and Installing the Fuses ......................................................... 10
Selecting the Computer Line Voltage............................................................................................ 12
Connecting Cables ................................................................................................................. 12
Installing the Liquid Sample Handling Unit.................................................................................. 14
Installing the Sample Cell.............................................................................................................. 18
Installing the Liquid Sample Handler Tubing................................................................................ 19
Connecting the Ultrasonic Controller Unit .................................................................................... 22
Installing the AquaPrep.................................................................................................................. 23
Selecting the Input Power ......................................................................................................24
Installing the AquaPrep Tubing ............................................................................................ 27
Connecting the Power Cord .................................................................................................. 28
Installing the MasterTech (Optional)............................................................................................. 29
Removing Packing Material From the Unit .......................................................................... 29

Table of Contents Sazturn DigiSizer II 5205
ii Jul 09
Selecting the Voltage ............................................................................................................. 29
Turning on the MasterTech (If Used) .................................................................................... 33
Installing the Ultrasonic Probe .............................................................................................. 34
Installing the Beaker Tray .....................................................................................................35
Installing Sample Transfer Tubing ........................................................................................ 36
Liquid Sample Handler Installation ............................................................................................... 39
Standard Liquid Sample Handler .......................................................................................... 39
Low-Volume Liquid Sample Handler ................................................................................... 41
Connecting Cables ................................................................................................................. 43
Installing the Analysis Program............................................................................................................. 44
Entering Ethernet Settings.............................................................................................................. 44
Configuring the Firewall Setting.................................................................................................... 44
Installing the Software.................................................................................................................... 44
Saturn DigiSizer 5205 confirm Systems ........................................................................................ 50
Preparing the Network ........................................................................................................... 50
Determining File Locations ................................................................................................... 50
Installing the confirm Analysis Program ............................................................................... 51
Entering Windows User Accounts ........................................................................................ 56
Adding Users to Windows User Groups ............................................................................... 57
Recording User Information .................................................................................................. 58
User Information Worksheet ................................................................................................. 58
Setting Up User Profiles in the Administrator Utility ........................................................... 61
Verifying Operation ............................................................................................................................... 66
Entering Service Test Mode........................................................................................................... 66
Exiting Service Test Mode............................................................................................................. 66
Saturn DigiSizer............................................................................................................................. 67
Performing a Leak-Check Procedure .................................................................................... 67
Moving the Rotation Arm to the Specified Angle ................................................................. 69
Fire the Laser ......................................................................................................................... 70
Checking the Temperature .................................................................................................... 70
Liquid Sample Handling Unit ........................................................................................................ 71
Recording Application Version ............................................................................................. 71
Checking Temperature of Fluid ............................................................................................. 72

Saturn DigiSizer II 5205 Table of Contents
Jul 09 iii
Checking the Pumps and Valve ............................................................................................. 73
Ultrasonic Probe............................................................................................................................. 74
AquaPrep........................................................................................................................................ 75
Performing a Leak Test .........................................................................................................75
Checking the Flow Rate ........................................................................................................ 75
Performing a Bubble Test ...................................................................................................... 76
Verifying MasterTech Operation................................................................................................... 77
Preparing the Analysis Liquid........................................................................................................ 80
Rinsing the Sample Cell................................................................................................................. 81
Performing a Background Measurement........................................................................................ 81
Creating a Sample Information File............................................................................................... 82
Standard Systems .................................................................................................................. 82
Confirm Systems ................................................................................................................... 86
Performing a Reference Material Test........................................................................................... 87
Part 2: Installation Checklist ................................................................................................................. 88
Checklist Description............................................................................................................................. 88
Preparing for Installation........................................................................................................................ 89
Setting Up the DigiSizer System............................................................................................................ 89
Installing the MasterTech (if used)........................................................................................................ 90
Installing the Analysis Program (Standard Software Only)................................................................... 90
Installing the Analysis Program (Confirm Software Only) ................................................................... 91
Verifying DigiSizer System Components.............................................................................................. 92
Verifying the MasterTech (if used)........................................................................................................ 93
Preparing the System for Operational Tests........................................................................................... 93
Performing Reference Material Test...................................................................................................... 94
Exceptions.............................................................................................................................................. 96
Signatures............................................................................................................................................... 97
Installer........................................................................................................................................... 97
Customer Representative................................................................................................................ 97
Final Documentation.............................................................................................................................. 98
Appendix A: Attaching Multiple Analyzers to One Computer
Appendix B: Saturn DigiSizer Configuration Management
Appendix C: Selecting the Voltage and Installing Fuses with Other Input Power Configuration

Table of Contents Sazturn DigiSizer II 5205
iv Jul 09

Saturn DigiSizer II 5205 Introduction
Jul 09 1
Introduction
This document describes how to install and verify operation of the Saturn DigiSizer II 5205.
The Saturn DigiSizer 5205 software is available as either a Standard analysis system or a
confirm analysis system. This document contains instructions for a typical Saturn DigiSizer
5205 standard or confirm installation. Follow the instructions applicable for the type of system
the customer purchased.
An installation checklist is included following the instructions. Complete each item in the
checklist and return the checklist to Micromeritics.
In addition to the steps described in this checklist, the Micromeritics Installation Qualification
Package for the Saturn DigiSizer 5205 and the Micromeritics Operational Qualification
Package for the Saturn DigiSizer 5205 may be completed during installation.
Conventions
Symbols
This document uses the symbols shown below to identify notes of importance, cautions, and
warnings.
Notes contain important information pertinent to the subject matter.
Warnings contain information that helps you prevent actions that may cause personal
injury.
Cautions contain information that helps you prevent actions that may damage the
analyzer.

Conventions Saturn DigiSizer II 5205
2 Jul 09
Commands
Menu commands are represented as shown in the following example:
Select Unit1 > Rinse > DigiSizer.
Which means, select Unit1, then Rinse, then DigiSizer from the main menu.
Command buttons in dialog boxes are shown in bold type. For example: Click OK to close the
dialog box.

Saturn DigiSizer II 5205 PreparingforInstallation
Jul 09 3
Part 1: Installation Instructions
Preparing for Installation
Before you begin installation of the Saturn DigiSizer 5205, perform these steps:
• Thoroughly review the Preinstallation Checklist, which has been returned from the cus-
tomer.
The Preinstallation Checklist and Instructions have been written to ensure that the
customer site is ready for this installation. In addition, the customer has been notified that
the installation will proceed smoothly if all of the items on the checklist are completed
properly.
• The Preinstallation Checklist helps you perform the steps described in the Installation
Instructions. If there are ANY discrepancies on the Preinstallation Checklist, contact the
customer and explain how the installation will be affected.
For a successful installation, you will need the following:
Item Purpose Location
Installation
Instructions To provide step-by-step instructions for each procedure.
Make sure you follow the procedures
in the order in which they are
presented to ensure a successful
installation.
If the user has not purchased an
option, for example, a MasterTech,
skip the instructions for that
component and proceed to the next
step.
In this document.
Installation Checklist To list the procedures required for the
installation process and verify
completion of each procedure.
In this document.
Standard Service
Tool Kit, safety
glasses, and
protective gloves
To provide the tools required for a
proper, safe installation. Provided by the Service Representative.

Equipment Description Saturn DigiSizer II 5205
4 Jul 09
Equipment Description
The Saturn DigiSizer 5205 System consists of up to two particle size analyzers, each with a
liquid sample handler, an AquaPrep, and one multifunction personal computer. Up to two
MasterTech 052 Autosamplers can be installed, allowing automatic analysis of up to 18
samples each.
Analyzer
The Saturn DigiSizer uses a laser in conjunction
with a CCD (charge-coupled device) containing
over three million detector elements to measure
particle size. These detectors are placed so that
they can measure the intensity of light scattered
by the particles at various angles. Light is
scattered by particles in a pattern dependent on
their size, shape, refractive index, and wave
length of incident light. Based on the Mie
theory, the particle size distribution is calculated
from the angle distribution of the scattered light
intensity collected by the detectors.
Saturn DigiSizer 5205 Analysis System
Liquid Sample
Handler
Analyzer
AquaPrep
AquaPrep

Saturn DigiSizer II 5205 EquipmentDescription
Jul 09 5
Both organic and inorganic particles can be analyzed and measured over a range of 0.06 to
2100 micrometers. The Saturn DigiSizer includes a complete system for circulating the
dispersing liquid/sample mixture through the cell and reservoir, as well as to an external waste
container.
Liquid Sample Handler
The Saturn DigiSizer requires the use of a liquid sample
handler to transfer the sample to the analyzer for analysis.
The sample handler also allows for connection of an
ultrasonic probe to assist in sample dispersion.
The sample handler enables automatic sample handling. All
the user has to do is define analysis conditions (in the
sample file), add the sample to the reservoir (containing the
dispersing liquid), and start the analysis. The sample will be
automatically monitored and diluted when necessary; and
the system rinsed after each analysis (when specified in the
sample file).
The Liquid Sample Handler is available in two configurations:
•Standard unit: includes a reservoir that holds 500 to 600 mL of dispersed sample. This
model is best suited for samples containing coarse particles or for those of high density.
•Low-Volume unit: includes a reservoir that holds 100 to 120 mL of dispersed sample.
This model is best suited for analyses where the sample quantity or dispersion liquid is
limited, or where the dispersion liquid may be hazardous or difficult to dispose of.
You also can attach a MasterTech 052 which allows you to analyze up to 18 samples
sequentially without further intervention. The MasterTech automatically transfers each sample
to the liquid sample handler for analysis.

Equipment Description Saturn DigiSizer II 5205
6 Jul 09
AquaPrep
Tap water varies greatly in its dissolved air
content and the presence of debris. This water
must be deionized and well filtered before using
with the AquaPrep.
Filtering the water through (at least) a 1-micron
filter will greatly extend the life of the
hydrophobic capsule by means of which air is
removed.
The AquaPrep recirculates water through a
hydrophobic capsule consisting of capillaries.
The result is a diffusion of dissolved air from the
water through the capillary walls and into the
ambient air.
The AquaPrep has water inlet and outlet connectors on its front panel. The switch for turning it
on and off is located on the rear panel just left of the power cord entrance.
The air removed from the water is exhausted through a small tube also at the front of the
instrument. Placing a small beaker of water around the tube so that its vent is submerged
reveals by its bubbling the rate of air removal. This guides in assessing when sufficient air has
been extracted from the water. Not all dissolved air has to be removed for satisfactory use with
the DigiSizer.
MasterTech 052
The MasterTech 052 is an optional automatic sampling device that operates in conjunction
with the Saturn DigiSizer. The MasterTech allows you to queue as many as 18 predispersed
samples to run consecutively and unattended. It allows samples to be redispersed either by
stirring only or by stirring and disruption with an ultrasonic probe.

Saturn DigiSizer II 5205 Completing the Installation Checklist
Jul 09 7
During operation, the beaker tray is loaded with beakers containing predispersed sample.
When the Saturn DigiSizer is ready for a sample, the tray rotates until in the correct position
for transfer. The sample is stirred for a user-specified length of time just before transfer to the
Saturn DigiSizer for analysis. The ultrasonic probe can also be activated for a user-specified
length of time to assist in redispersion if needed.
After redispersion, the sample is transferred to the reservoir of the analyzer. Then a small
amount of analysis fluid is back-flushed to the MasterTech to rinse the stirrer, probe, and
tubing. After rinsing is complete, the MasterTech prepares itself for the next sample.
Completing the Installation Checklist
Section 2 of this document contains the Installation Checklist. For each operational
verification procedure, fill in the values obtained in the test. When you complete the checklist,
fill in the customer information, sign and date, and return the checklist to Micromeritics
Service Center as described below.
Documenting Installation
In order to provide consistent instrument service, Micromeritics retains records of installation,
operational verification, and calibration data in its Service Support Center in Norcross,
Georgia, USA. After completing the installation process, representatives of Micromeritics
who install instruments are required to send the documents listed below to Micromeritics for
inclusion in the customer's instrument history file.
For sample information files and calibration data, you may either save the files on CD and
mail the CD to Micromeritics or send them as an email attachment.
The mailing address is:
Micromeritics Service Support Center
4356 Communications Drive
Norcross, GA 30093
USA
The email address is:
[email protected]

Inspecting the Equipment Saturn DigiSizer II 5205
8 Jul 09
The documents to be sent to the Micromeritics Service Support Center are:
• Saturn DigiSizer 5205 Installation Checklist, completed and signed
• Reference Material Analysis Sample File
• Laser Diagnostics Report
• Laser Stability Test Report
• Calibration files if instrument calibration data are changed during installation.*
*Generally, it is not necessary to change calibration data during installation. If however, you
need to change calibration data, the calibration files must be saved and sent to Micromeritics
for retention in the instrument history file.
Inspecting the Equipment
Before you begin installing the Saturn DigiSizer 5205, check the packing list to ensure that all
components and accessories are available.
If the analyzer has not been unpacked, the customer must unpack the analyzer and
place it on an appropriate work surface before you can proceed with the installation.
If the customer needs to declare equipment as damaged or lost, the customer must
save the shipping cartons. The claims investigator must examine the cartons in order
to complete the inspection report.
The Saturn DigiSizer analyzer weighs 45 kg (99 lbs) and requires the use of two
people to lift it from its shipping carton. One person should not attempt to lift the
analyzer. With one person on each side of the analyzer, lift it upright from its shipping
carton.

Saturn DigiSizer II 5205 Setting up the DigiSizer System
Jul 09 9
Setting up the DigiSizer System
Installing the DigiSizer
Space Requirements
The Saturn DigiSizer System requires the work space shown below.
Placing the DigiSizer on a Work Surface
Ensure that the DigiSizer is placed on the work surface with the back panel facing the front of
the table in order to access the fuse block.
You must have access to the front, side, and rear panels for installation of the
instrument.

Setting up the DigiSizer System Saturn DigiSizer II 5205
10 Jul 09
Selecting the Voltage Setting and Installing the Fuses
The Saturn DigiSizer leaves the factory set for 120 VAC and with the line fuses removed. The
correct setting of the universal power entrance must be checked and the appropriate fuses
installed before the analyzer can be operated.
The Saturn DigiSizer is designed to operate with 100, 120 or 220, 240 VAC from 47 to 63 Hz.
Voltage selection and fusing are made at the power connector located on the rear panel of the
analyzer. Appropriate fuses are included in the accessories kit:
• Two 5x20mm, SLO-BLO, 1.6A (100 - 120 VAC)
• Two 5x20mm, SLO-BLO, 1.25A (220 - 240 VAC)
1. Make sure the power cord is not connected.
2. Check the voltage setting at the power connector on the rear panel of the instrument.
• If the voltage is correct:
a. Open the cover by prying the left side of the cover with a pointed object, such as a
small flat-blade screwdriver.
b. Remove the fuse block.
c. Proceed to Step 6.
• If the voltage is incorrect, open the cover and remove the fuse block as described above,
then proceed to Step 3.
3. Using a pointed object, pry the voltage selector card loose and remove it from the power
connector housing.

Saturn DigiSizer II 5205 Setting up the DigiSizer System
Jul 09 11
4. Orient the voltage selector card so that the desired voltage is shown on the side of the card
facing you.
5. Slide the voltage selector card into the power connector housing and press until it fits
securely.
6. Insert the appropriate fuses into the fuse block. Refer to the chart below for the appropriate
fuse rating.
Power Source Fuse
100 - 120 VAC Two 5x20mm, SLO-BLO, 1.6A
220 - 240 VAC Two 5x20mm, SLO-BLO, 1.25A
7. Slide the fuse block into the housing and press until it fits securely.
Voltage
setting
The fuses used in the instrument must be identical in type and rating to that specified.
Use of other fuses could result in electrical shock and/or damage to the instrument.

Setting up the DigiSizer System Saturn DigiSizer II 5205
12 Jul 09
Selecting the Computer Line Voltage
The line voltage of the computer must be set to match the input power source (from the wall
outlet). The computer operates with either 100-120 VAC or 200-240 VAC at 50 or 60 Hz.
Refer to the instruction manual supplied with your computer for instructions on selecting
power input.
Connecting Cables
Ethernet Cable
The Ethernet cable has RJ45 connectors (similar to a phone jack). Either a straight-through
patch cable or a crossover cable can be used. Install the cable as follows:
1. Insert one end of the Ethernet crossover cable into the connector labeled Ethernet on the
rear panel of the analyzer.
2. Insert the other end of the cable into the RJ45 connector on the ethernet card (exposed on
the rear panel of the computer).
Do not connect the computer power cord to a power source until the proper voltage
selection is made. Doing so could result in electrical shock and/or damage to the
computer.

Saturn DigiSizer II 5205 Setting up the DigiSizer System
Jul 09 13
Power Cord
Connect the power cord to the connector on the rear panel of the DigiSizer and to an
appropriate power source.
Computer Cables
Follow the instructions provided below to connect the monitor, keyboard, printer, and mouse.
1. Plug the keyboard cable, the monitor cable, and the mouse cable into their respective
connectors on the rear panel of the computer.
2. Plug one end of the printer cable into the connector on the rear panel of the printer. Plug
the other end of the printer cable into the appropriate connector on the rear panel of the
computer.
3. Plug all power cords into an appropriate power source.
Refer to the instruction manuals supplied with the computer, video monitor, and
printer for voltage requirements for these units.

Setting up the DigiSizer System Saturn DigiSizer II 5205
14 Jul 09
Installing the Liquid Sample Handling Unit
A liquid sample handler is required to transfer the sample to the analyzer for analysis. The
sample is transferred through the use of tubing. This tubing is installed on the left side of the
sample handler and inserted through two ports on the right side of the analyzer. Precut tubing
is provided for this purpose; if you are installing the:
• Standard unit, the tubing is 1.27-cm (1/2-in.) diameter (2 pieces)
• Low-volume unit, the tubing is 0.79-cm (5/16-in.) diameter (1 piece)
Perform the following steps to install the liquid sample handler.
1. Remove the two plugs from the ports on the side of the sample handler
If you are installing the Low-volume unit, the tubing on the upper port is installed; remove
the plug from the end of the tubing.
2. Install the tubing onto the connectors provided on the left side of the liquid sample
handler. One piece of tubing is approximately 2 inches longer than the other; install this
piece on the upper connector and the shorter one on the lower connector.
3. Install the tubing onto the connectors provided on the left side of the liquid sample
handler. One piece of tubing is approximately 2 inches longer than the other; install this
piece on the upper connector and the shorter one on the lower connector.
Longer piece on upper port.
This piece of tubing is
already installed if you have
the Low-volume unit.
Shorter piece on lower port.