SPECTRO SPECTROSCOUT User manual

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SPECTROSCOUT
Portable X-ray fluorescence
spectrometer
Original operating instructions

SPECTROSCOUT — 07.09.2015 — 3
Table of Contents
1Description of instrument ....................................................................................5
1.1Description .......................................................................................................................... 5
1.2Function .............................................................................................................................. 5
1.3Overview ............................................................................................................................. 6
1.3.1Configuration ......................................................................................................... 6
1.3.2Instrument.............................................................................................................. 7
1.4Lithium battery .................................................................................................................... 8
2Safety................................................................................................................10
2.1Symbols used ................................................................................................................... 10
2.2User information................................................................................................................ 11
2.3Intended use ..................................................................................................................... 12
2.4Prohibited operating conditions ........................................................................................ 12
2.5Residual risks.................................................................................................................... 12
2.6Radiation protection advice .............................................................................................. 13
3Technical data...................................................................................................14
4Transportation/Setting-up .................................................................................15
4.1Set-up ............................................................................................................................... 15
4.2Use.................................................................................................................................... 15
4.3Transport........................................................................................................................... 16
4.4Gas supply (optional)........................................................................................................ 17
4.5Vacuum (option)................................................................................................................ 17
4.6Sample spinner (optional)................................................................................................. 18
4.7Notebook (optional)........................................................................................................... 18
5Initial start-up ....................................................................................................19
5.1Preparing the instrument for use ...................................................................................... 19
6Operation ..........................................................................................................20
6.1Overview of controls ......................................................................................................... 20
6.2Switching on the instrument.............................................................................................. 21
6.3Switching offthe instrument............................................................................................... 22
6.4Displays ............................................................................................................................ 23
6.4.1Instrument............................................................................................................ 23
6.4.2Screen ................................................................................................................. 24
6.4.3Notebook (optional) ............................................................................................. 24
6.5Measuring procedure........................................................................................................ 25
7Maintenance by the operator ............................................................................27
7.1Operator maintenance plan .............................................................................................. 27
7.2Standardizing the measuring device (ICALization)........................................................... 28

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7.3Replace the protective film................................................................................................ 29
7.3.1Precious metals instrument variant ..................................................................... 29
7.3.2Environmental screening / Geochemical exploration instrument variant ............ 29
7.4Install the sample spinner/vacuum sub-assembly ............................................................ 30
8Troubleshooting................................................................................................ 31
9Spare parts and consumables.......................................................................... 34
10De-commissioning............................................................................................ 34

Description of instrument
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1 Description of instrument
1.1 Description
Designation: SPECTROSCOUT
Model: XEP04
Type: 76004851
1.2 Function
X-rays excite the atoms of the sample to emit radiation. This radiation is measured
by a semiconductor detector.
The unit is delivered including an installed analysis method. Data are already
stored in the unit's memory. The measured values are compared with these data.
After the measurement is complete, the results relating to an unknown sample are
displayed on the screen.
The sample material can be solid, liquid or a powder.

Description of instrument
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1.3 Overview
1.3.1 Configuration
The SPECTROSCOUT is available in two different versions—one for the use
outdoors and the second for the application in a laboratory and production
(at-line).
Depending on the area of application, the instrument is equipped with the following
calibration options:
Precious metals
Environmental screening
Geochemical exploration
Depending on the application, the following options are available:
Sample spinner
Helium flush or vacuum connection
Video camera
Notebook
Battery

Description of instrument
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1.3.2 Instrument
Instrument in transport
condition
(not applicable to
SPECTROSCOUT at-line)
Instrument in measurement-
taking position
(sample chamber lid and
ePC closed)
Instrument in measurement-
taking position
(sample chamber lid and
ePC opened)
Front side
Rear side
Fig. 1
No. Component No. Component
1 Sample chamber lid a ON button
2 Handle b Power supply connection
3 X-ray radiation indicator c Vacuum pump connection
4 Shutter open/closed (indicator) d Gas input /vacuum connection
point
5-1 ePC closed
5-2 ePC opened
6 Measurement chamber plate
12345-1465-23
b
acd b acd b acd

Description of instrument
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1.4 Lithium battery
The lithium battery in the SPECTROSCOUT at-line is optional.
Caution! Lithium batteries
Lithium batteries contain acid.
Lithium batteries may explode if exposed to fire or excessive heat.
Never use damaged lithium batteries.
Never expose lithium batteries to fire or heat.
Lithium batteries must be transported and packaged in compliance with
transport regulations and country-specific provisions. These include, e.g.,
ADR/RID, IATA, DOT, IMDG, etc.
Lithium batteries must be protected to prevent a short circuit.
No risks are associated with lithium batteries, if they are handled and used
properly. Always heed the warnings on lithium batteries and comply with the
instructions in the operating manuals of the instruments.
It is prohibited to transport lithium batteries if one of the following conditions
applies. This includes, for example, lithium batteries that are being returned to
the manufacturer for reasons of safety.
Lithium batteries identified by the manufacturer as being defective for
safety reasons.
Lithium batteries that have been damaged.
Lithium batteries that have the potential of producing a dangerous
evolution of heat.
Lithium batteries that have the potential of producing a dangerous
evolution of fire or short circuit.
Disposing lithium batteries (IATA)
Lithium batteries must be disposed of in compliance with local and country-
specific regulations.
The emergency telephone number indicated on the shipping document is
solely intended for transportation and lithium batteries authorized by
SPECTRO Analytical Instruments GmbH.
Emergency number:
[phone] (International)
011441865407333 (USA)
Emergency contact: 441865407333 SPECTRO 29003-NCEC

Description of instrument
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Please observe the relevant national and regional regulations.
A fully charged lithium battery can last up to approximately 5 hours
(continuous operation). The exact battery life depends on the sample
throughput per time unit and the selected measurement parameters.
If a lithium battery is empty, it must be recharged after one week of storage at
the latest.
If lithium batteries are to be stored over an extended period, they should be
charged to 50%-70% of their capacity. The optimum storage temperature is
15° to 20°C (59° to 68°F); under these conditions, the stored lithium battery
should be recharged at the latest after 3 months.
If the storage temperature exceeds 20 °C (68 °F), the battery will self-
discharge more quickly. In this case, it needs to be recharged at shorter
intervals. (40°C (104°F) ~ 2 months, 60°C (140°F) ~ 1 month).
The lithium batteries include an electronic safety system that checks the state
of charge of the individual cells. As a result, it continuously withdraws energy
from the lithium batteries. Consequently, there is a risk of deep discharge if a
used lithium battery is stored that does not have the minimum charge.
If one of the cells in the lithium batteries is already deep-discharged, the
integrated electronic system prevents the recharge of the lithium batteries for
reasons of safety.
Note
Fully charge the lithium battery of the SPECTROSCOUT prior to using it for
the first time.
The lithium battery can only be charged at a temperature ranging from 0°C to
45°C (32°F to 113°F). A protective circuit within the instrument prevents the
battery from charging, unless the temperature is within this range.

Safety
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2 Safety
Every user of the instrument must have understood these operating instructions.
This applies in particular to the safety regulations.
2.1 Symbols used
The following symbols are used in these abbreviated operating instructions and on
the instrument.
If required, additional important information is available in connection with these
symbols.
Danger! Risk of electrical shock!
Caution! Risk of injury!
Caution! Danger of poisoning!
Caution! Ionizing radiation!
Caution! Risk of crushing injuries!
Notice!
Warns of activities or conditions that may adversely affect the
safety or function of the instrument.
Note
Displays information that is important for the correct and safe use
of the instrument