Bruker Anton Paar User manual

Innovation with Integrity XRD
Anton Paar
Temperature Chambers
for D8 ADVANCE / D8 DISCOVER
User Manual
Original Instructions (English)

The reproduction, transmission or use of this document or its contents is not permitted without express written
authority. Offenders will be liable for damages. All rights reserved.
We have checked the contents of this manual for agreement with the hardware and software described. Since
deviations cannot be precluded entirely, we cannot guarantee full agreement. However, the data in this manual are
reviewed regularly and any necessary corrections are included in subsequent editions. Suggestions for improvement
are welcome.
All configurations and specifications are subject to change without notice.
Order no. DOC-M88-EXX268 V1. Dec 20, 2016.
© 2016 Bruker AXS GmbH, Karlsruhe, Germany.
All trademarks and registered trademarks are the sole property of their respective owners.
Printed in the Federal Republic of Germany.
Bruker AXS GmbH
Östliche Rheinbrückenstr. 49
76187 Karlsruhe, Germany
Tel. [phone]
Fax [phone]
[e-mail]
www.bruker.com

Contents
DOC-M88-EXX268_V1_12.2016 3
Contents
List of Figures............................................................................................................................... 7
1 Safety Guidelines ....................................................................................................................... 13
1.1 About this Manual ........................................................................................................13
1.2 Qualified Personnel......................................................................................................14
1.3 Correct and Intended Usage........................................................................................15
1.4 Disclaimer and Liability ................................................................................................15
1.5 General Safety Precautions.........................................................................................15
1.6 Signage........................................................................................................................18
2 General Remarks ........................................................................................................................ 19
2.1 Heating Principles........................................................................................................19
2.2 Temperature Measurement and Calibration ................................................................20
2.2.1 Temperature Measurement .........................................................................................20
2.2.2 Temperature Calibration ..............................................................................................21
2.2.2.1 Temperature Calibration by Thermal Expansion of MgO (Periclase) ..........................21
2.2.2.1.1 Detailed Procedure for Temperature Determination....................................................22
2.2.2.1.2 Shortened Procedure for Temperature Determination.................................................23
2.2.2.2 Temperature Calibration by Phase Transitions............................................................24
3 Vacuum Equipment .................................................................................................................... 27
3.1 Installation of the Edwards High Vacuum Stage with TIC............................................27
3.1.1 Mounting of the Edwards High Vacuum Stage ............................................................27
3.1.2 Operation of the Edwards High Vacuum Stage ...........................................................31
3.2 Installation of the Edwards Backing-Pump ..................................................................32
4 Adjustment of a Chamber on the D8 ........................................................................................ 35
4.1 Adjustment Procedures................................................................................................35
4.1.1 Adjustment Procedure with Alignment Slit...................................................................36
4.1.2 Alternative Procedure Without Alignment Slit ..............................................................40
4.1.3 Using Automated Height Correction ............................................................................44

Contents
4 DOC-M88-EXX268_V1_12.2016
5 Mounting the Temperature Controller into the D8 Enclosure ................................................ 47
6 Installation and Operation of the HTK-Series, TTK 600, XRK 900, and HPC 900 Chambers
...................................................................................................................................................... 49
6.1 Introduction ..................................................................................................................49
6.2 Mounting the Chamber to the Goniometer...................................................................50
6.3 Temperature Controllers for Anton Paar Chambers ....................................................53
6.3.1 Connecting the TCU Controller....................................................................................54
6.4 Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER............................56
6.5 Operation .....................................................................................................................56
6.6 Alignment.....................................................................................................................57
7 Installation and Operation of the CHC plus Humidity Chamber ............................................ 59
7.1 Introduction ..................................................................................................................59
7.2 Mounting the Chamber to the Goniometer...................................................................59
7.3 Temperature Controllers and Water Circuit for CHC plus............................................60
7.3.1 Connecting the CCU Controller ...................................................................................65
7.3.2 Connecting the MHG for CHC plus..............................................................................65
7.4 Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER............................69
7.5 Operation .....................................................................................................................69
7.6 Alignment.....................................................................................................................72
8 Installation and Operation of the DCS 350 and DHS 1100 Chambers ................................... 73
8.1 Introduction ..................................................................................................................73
8.2 Mounting the Chamber to the Goniometer...................................................................73
8.3 Temperature Controllers DC S350 and DHS 1100......................................................75
8.4 Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER............................76
8.5 Operation .....................................................................................................................77
8.5.1 Activating the Chamber in DA VINCI ...........................................................................77
8.5.2 Operating the Chamber ...............................................................................................79
8.6 Alignment.....................................................................................................................81
8.6.1 Aligning the Chamber for Automated Height Correction..............................................81

Contents
DOC-M88-EXX268_V1_12.2016 5
8.6.2 Optimizing Theta, Two Theta and Psi..........................................................................87
8.6.2.1 Optimizing Theta..........................................................................................................87
8.6.2.2 Optimizing Two Theta..................................................................................................88
8.6.2.3 Optimizing Psi:.............................................................................................................89
8.6.3 Creating a Temperature Dependent Measurement Using the WIZARD......................90
9 Installation and Operation of the BTS 150 and BTS 500 Chambers ...................................... 95
9.1 Introduction ..................................................................................................................95
9.2 Mounting the Chamber to the Goniometer...................................................................95
9.3 USB Connection of the BTS 150/500 to the CPU1 Board ...........................................97
9.4 Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER............................98
9.5 Operation and Alignment .............................................................................................98
10 Appendix / Service Details......................................................................................................... 99
10.1 Vacuum Equipment......................................................................................................99
10.1.1 Programming of the Edwards High Vacuum Stage .....................................................99
10.2 Configuring a Chamber in DIFFRAC.MEASUREMENT CENTER.............................100
10.2.1 HTK-series, TTK 600, XRK 900, and HPC 900 Chambers........................................100
10.2.2 CHC plus....................................................................................................................107
10.2.2.1 CHC plus with TCU 110 and HE-4 Water Bath..........................................................107
10.2.2.2 CHC plus with CCU100 and Corio Water Bath..........................................................117
10.2.3 DCS 350 and DHS 1100............................................................................................126
10.2.4 BTS 150 and BTS 500...............................................................................................131
10.3 References.................................................................................................................132
Index .......................................................................................................................................... 133