
6 Calibration with gas
A calibration can only be performed together with a Statox 502 or 503 Control Module (linecalibration).
After an ex-works linecalibration, the mated devices are labeled pairwise.
A calibration is required
after installation (other than ex-works line calibration)
after replacement of the control module
after changing the program
after sensor replacement
in time intervals as required by local regulations.
Before calibrating, allow 30 min warm up time.
Calibration to liquid substances in the field is labor intensive and prone to error. Use Isobutene as
reference gas and apply the response factors (noted on the type plate) provided by Compur Monitors.
The tools required for calibration are: span gas in appropriate concentration, a regulator and a gas
adapter.
The interface will accept set points between 10 and 100 % of the end of scale value.
To achieve best accuracy Compur Monitors recommends to calibrate at the desired alarm threshold
value. Calculate the most suitable span gas concentration with this formula:
Procedure:
Hold the magnetic pin on to the contact area to start the calibration routine. The green LED will start
flashing. If there is no further activity, the sensor head will automatically return to the measuring mode
after 30 minutes.
Enter the menu “CALIB. ROUTINE” on the Control Module. Adjust zero.
Connect the gas tube to one of the fittings of the gas adapter. If you want to avoid gas emissions, you
may connect an active carbon filter to the outlet. (Art.no. 806 488) Do not bend or twist the tube to
avoid overpressure in the gas adapter.
As soon as the Control Module displays „APPLY SPAN GAS“, connect the gas adapter to the sensor
and open the valve. Press „Enter“. The recommend flow is 20 l/h (300 ml/min).
As soon as „CALIB. FINISHED“ is displayed, press „Enter“ again.
Now enter the product of span gas concentration multiplied by the response factor.
In case the sensor signal is too low, you will get the message „GAS CONC ERROR“or “CALIBR.
FAILED” on the Control Module. Proceed as described in the next chapter.
Remove the gas adapter and switch the gas off.
Leave the calibration menu on the Control Module.
Touch the contact area on the PID with the magnetic pin to enter the measuring mode. The LED
should be green then.
Alarm threshold
c Isobutene =
Response factor
Example: Measuring range 0 - 1000 ppm methyl methacrylate, Response factor = 1,6
minimal Isobutene concentration: 100 ppm / 1,6 = 62,5 ppm Isobutene
maximum Isobutene concentration : 1000 ppm / 1,6 = 625 ppm Isobutene
Example: Calibration to methyl methacrylate with 100 ppm Isobutene.
You have to enter 100 ppm * 1,6 = 160 (The response factor of methyl methacrylate is 1,6)