Ecotech Acoem Serinus 10 User manual

Serinus® 10

Ozone Analyser

User Manual

Version: 3.2

ACOEM Ecotech

1492 Ferntree Gully Road Knoxfield VIC 3180

Melbourne Australia +61 3 9730 7800 [email protected] ecotech.com

Manual subject to change without notice. Images used are for illustrative purposes only. Ecotech & Serinus are trademarks or registered trademarks

Serinus® 10 User Manual 3.2

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Introduction 
Page 3 
 
Table of Contents 
Manufacturer’s Statement ....................................................................................................................................12 
Safety Information.................................................................................................................................................13 
Warranty................................................................................................................................................................15 
Service and Repairs................................................................................................................................................16 
Product Compliance and Approvals.......................................................................................................................17 
Manual Revision History........................................................................................................................................18 
Introduction........................................................................................................................... 21 
1 Description................................................................................................................................................21 
2 Specifications ............................................................................................................................................21 
2.1 Measurement ............................................................................................................................21 
2.2 Precision/Accuracy ....................................................................................................................21 
2.3 Calibration .................................................................................................................................21 
2.4 Power ......................................................................................................................................22 
2.5 Operating Conditions.................................................................................................................22 
2.6 Communications........................................................................................................................22 
2.7 Physical Dimensions...................................................................................................................23 
2.8 Certifications..............................................................................................................................23 
3 Nomenclature ...........................................................................................................................................24 
4 Background/Theory...................................................................................................................................25 
4.1 Measurement Theory ................................................................................................................25 
4.2 Kalman Filter Theory..................................................................................................................25 
5 Instrument Description .............................................................................................................................26 
5.1 Calibration Valve Manifold ........................................................................................................26 
5.2 Sample Filter Holder ..................................................................................................................27 
5.3 Ozone Scrubber .........................................................................................................................27 
5.4 Optical Bench.............................................................................................................................28 
5.5 Main Controller PCA ..................................................................................................................30 
5.6 Pneumatic Tubing......................................................................................................................30 
5.7 Rear Panel..................................................................................................................................30 
5.8 Communications........................................................................................................................32 
Installation/Decommission.................................................................................................... 35 
1 Initial Check...............................................................................................................................................35 
2 Installation Notes ......................................................................................................................................38 
3 Instrument Set-Up.....................................................................................................................................39 
3.1 Power connections ....................................................................................................................39 
3.2 Pneumatic Connections.............................................................................................................40 
3.3 Communications Connections ...................................................................................................43 
3.4 Instrument Set-Up .....................................................................................................................43 
4 U.S. EPA Equivalent Set-Up .......................................................................................................................44 
5 EN Type Approval Set-Up ..........................................................................................................................45 
6 Transporting/Storage ................................................................................................................................45 
Operation............................................................................................................................... 49 
1 Warm-Up...................................................................................................................................................49 
2 Measurement............................................................................................................................................49 

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3 General Operation Information................................................................................................................ 50 
3.1 Keypad & Display....................................................................................................................... 50 
3.2 Home Screen............................................................................................................................. 52 
4 Menus & Screens...................................................................................................................................... 54 
4.1 Quick Menu............................................................................................................................... 55 
4.2 Main Menu................................................................................................................................ 56 
4.3 Analyser State Menu................................................................................................................. 57 
4.4 Status Menu.............................................................................................................................. 58 
4.5 Temperature Menu................................................................................................................... 59 
4.6 Pressure & Flow Menu.............................................................................................................. 60 
4.7 Voltage Menu............................................................................................................................ 61 
4.8 General Settings Menu.............................................................................................................. 62 
4.9 Measurement Settings Menu.................................................................................................... 63 
4.10 Calibration Menu ...................................................................................................................... 64 
4.11 Pressure Calibration Menu........................................................................................................ 66 
4.12 Ozone Calibration Menu (Option)............................................................................................. 67 
4.13 Flow Calibration Menu (Option)................................................................................................ 68 
4.14 Service Menu............................................................................................................................. 69 
4.15 Diagnostics Menu...................................................................................................................... 70 
4.16 Digital Pots Menu...................................................................................................................... 70 
4.17 Internal Pump Menu (Option)................................................................................................... 72 
4.18 Valve Menu ............................................................................................................................... 73 
4.19 Tests Menu................................................................................................................................ 74 
4.20 Digital Input Test Menu............................................................................................................. 75 
4.21 Digital Output Test Menu.......................................................................................................... 75 
4.22 Calculation Factors Menu.......................................................................................................... 76 
4.23 Communications Menu............................................................................................................. 77 
4.24 Data Logging Menu ................................................................................................................... 78 
4.25 Serial Communication Menu..................................................................................................... 78 
4.26 Analog Input Menu ................................................................................................................... 79 
4.27 Analog Output Menu................................................................................................................. 80 
4.28 Digital Input Menu .................................................................................................................... 82 
4.29 Digital Output Menu ................................................................................................................. 83 
4.30 Network Menu (Option)............................................................................................................ 84 
4.31 Bluetooth Menu........................................................................................................................ 85 
4.32 Trend Display Menu .................................................................................................................. 86 
4.33 Chart ...................................................................................................................................... 87 
4.34 Advanced Menu ........................................................................................................................ 89 
4.35 Hardware Menu ........................................................................................................................ 90 
4.36 Parameter Display Menu........................................................................................................... 91 
Communications.................................................................................................................... 93 
1 RS232 Communication.............................................................................................................................. 93 
2 USB Communication................................................................................................................................. 94 
3 TCP/IP Network Communication (Optional)............................................................................................. 95 
3.1 Reading Network Port Setup..................................................................................................... 96 
3.2 Setting Network Port Setup ...................................................................................................... 96 
3.3 Port Forwarding on Remote Modem/Router Setup.................................................................. 97 
3.4 Airodis Setup to Communicate with Serinus............................................................................. 98 
4 Analog and Digital Communication .......................................................................................................... 99 
4.1 Analog Outputs ......................................................................................................................... 99 
4.2 Analog Inputs .......................................................................................................................... 100 

 
 
Introduction 
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4.3 Digital Status Inputs.................................................................................................................100 
4.4 Digital Status Outputs..............................................................................................................100 
5 Logging Data............................................................................................................................................101 
5.1 Configure Instrument Internal Logging....................................................................................101 
6 Using Airodis Software to Download Data ..............................................................................................102 
6.1 Connecting the Instrument to PC ............................................................................................102 
6.2 Installing Airodis ......................................................................................................................105 
6.3 Configuring Airodis ..................................................................................................................105 
7 Serinus Remote App/Bluetooth ..............................................................................................................110 
7.1 Installation...............................................................................................................................111 
7.2 Connecting to the Instrument .................................................................................................111 
7.3 Instrument Control ..................................................................................................................112 
7.4 Real-Time Plot..........................................................................................................................114 
7.5 Download.................................................................................................................................115 
7.6 Get Parameters........................................................................................................................115 
7.7 Preferences..............................................................................................................................116 
Calibration ........................................................................................................................... 119 
1 Overview .................................................................................................................................................119 
2 Using Transfer Standards - Overview ......................................................................................................120 
2.1 Principle...................................................................................................................................121 
2.2 Set-Up ....................................................................................................................................122 
3 Pressure Calibration ................................................................................................................................123 
3.1 Full Pressure Calibration (Two Point Calibration) ....................................................................123 
3.2 Pressure Calibration (Ambient Only) .......................................................................................125 
3.3 Pressure Calibration (Internal Pump Option Only) ..................................................................126 
4 Zero Calibration.......................................................................................................................................127 
4.1 Calibration Port........................................................................................................................128 
4.2 Sample Port .............................................................................................................................128 
4.3 IZS (Option)..............................................................................................................................129 
5 Span Calibration ......................................................................................................................................130 
5.1 Calibration Port........................................................................................................................130 
5.2 Sample Port .............................................................................................................................130 
6 Precision Check .......................................................................................................................................131 
6.1 Zero Precision Check................................................................................................................131 
6.2 Span Precision Check ...............................................................................................................132 
7 Multipoint Precision Check .....................................................................................................................133 
8 Flow Calibration (Internal Pump Option Only) ........................................................................................134 
9 High Pressure Zero Valve (Option) ..........................................................................................................135 
9.1 Single Pressurised Calibration (Option) ...................................................................................136 
Service ................................................................................................................................. 139 
1 Additional Safety Requirements for Service Personnel...........................................................................139 
2 Maintenance Tools..................................................................................................................................139 
3 Maintenance Schedule............................................................................................................................140 
4 Maintenance Procedures ........................................................................................................................142 
4.1 Particulate Filter Replacement ................................................................................................142 
4.2 Clean Chassis Fan Filter............................................................................................................144 
4.3 Leak Check ...............................................................................................................................145 
4.4 Ozone Scrubber Check.............................................................................................................150 

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4.5 Clean Pneumatics.................................................................................................................... 152 
4.6 Clean Optical Cell .................................................................................................................... 152 
4.7 UV Lamp Check ....................................................................................................................... 156 
4.8 Orifice/Sintered Filter Replacement ....................................................................................... 157
4.9 Pressure Sensor Check ............................................................................................................ 159 
5 Bootloader.............................................................................................................................................. 160 
5.1 Display Help Screen................................................................................................................. 161 
5.2 Communications Port Test...................................................................................................... 161 
5.3 Updating Firmware ................................................................................................................. 161 
5.4 Erase All Settings..................................................................................................................... 161 
5.5 Start Analyser.......................................................................................................................... 161 
Troubleshooting................................................................................................................... 163 
1 Flow Fault ............................................................................................................................................... 166 
2 Noisy/Unstable Readings........................................................................................................................ 167 
3 Lamp Temperature Failure ..................................................................................................................... 168 
4 USB Memory Stick Failure....................................................................................................................... 169 
5 Ecotech Service Support Files ................................................................................................................. 170 
Optional Extras.....................................................................................................................173 
1 Dual Sample Filter (PN: E020100)........................................................................................................... 173 
2 Network Port (PN: E020101)................................................................................................................... 173 
2.1 Hardware Setup ...................................................................................................................... 174 
3 Rack Mount Kit (PN: E020116)................................................................................................................ 174 
4 Internal Pump (PN: E020105) ................................................................................................................. 178 
4.1 Hardware Setup ...................................................................................................................... 178 
4.2 Internal Pump Additional Components................................................................................... 178 
4.3 Internal Pump Removed Components .................................................................................... 179 
4.4 Pressure Calibration Internal Pump Option ............................................................................ 179 
4.5 Flow Calibration ...................................................................................................................... 179 
4.6 Internal Pump Leak Check....................................................................................................... 179 
4.7 Pump Control .......................................................................................................................... 179 
5 High Pressurised Zero Valve (PN: E020109)............................................................................................ 180 
6 Internal Zero & Span (IZS) (PN: E020130) ............................................................................................... 180 
6.1 Hardware Setup ...................................................................................................................... 180 
6.2 IZS Additional Components..................................................................................................... 180 
6.3 IZS Removed Components ...................................................................................................... 181 
6.4 Serinus 10 Schematic with IZS Option..................................................................................... 182 
6.5 Ozone Generator Characterisation ......................................................................................... 182 
Parts List and Schematics..................................................................................................... 183 
1 Serinus Accessories Kit............................................................................................................................ 183 
2 Maintenance Kit...................................................................................................................................... 183 
3 Consumables .......................................................................................................................................... 184 
4 Instrument Parts List............................................................................................................................... 185 
5 Plumbing Schematic –(PN: D020004) .................................................................................................... 188 
6 Plumbing Schematic –(PN: D020050) .................................................................................................... 189 
7 Plumbing Schematic –(PN: D020051) .................................................................................................... 190 
8 Block Wiring Schematic –(PN: D020101) ............................................................................................... 191 

 
 
Introduction 
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9.9 Block Wiring Schematic –(PN: D020121)................................................................................................192 
9.10 Optical Bench/Photometer Assembly –(PN: H013100)..........................................................................193 
9.11 Calibration Manifold Assembly –(PN: H010013-02)...............................................................................194 
9.12 Valve Assembly –(PN: H010042) ............................................................................................................195 
9.13 Charcoal Scrubber Assembly –(PN: H010038)........................................................................................196 
9.14 Calibration Manifold Assembly (IZS) –(PN: H010056) ............................................................................197 
9.15 Sample Filter Holder Assembly –(PN: H010160) ....................................................................................198 
9.16 Ozone Generator Assembly –(PN: H013150) .........................................................................................199 
 
List of Figures 
Figure 1 –Major Components of Serinus 10............................................................................... 26 
Figure 2 –Calibration Valve Manifold......................................................................................... 26 
Figure 3 –Sample Filter Holder................................................................................................... 27 
Figure 4 –Ozone Scrubber.......................................................................................................... 27 
Figure 5 –Optical Bench Major Parts.......................................................................................... 28 
Figure 6 –Orifice and Sintered Filter .......................................................................................... 28 
Figure 7 –Lamp Driver PCA Type Jumper Setting (REV D).......................................................... 29 
Figure 8 –Ecotech Tubing ........................................................................................................... 30 
Figure 9 –Rear Panel................................................................................................................... 30 
Figure 10 –Power ON/OFF Switch.............................................................................................. 31 
Figure 11 –Communication Connections ................................................................................... 32 
Figure 12 –Items Received ......................................................................................................... 36 
Figure 13 –Opening the Instrument –1..................................................................................... 37 
Figure 14 –Opening the Instrument –2..................................................................................... 37 
Figure 15 –Opening the Instrument –3..................................................................................... 37 
Figure 16 –Opening the Instrument –4..................................................................................... 38 
Figure 17 –Instrument Rear Panel.............................................................................................. 39 
Figure 18 –Connect Power Cord................................................................................................. 40 
Figure 19 –Turn ON Power Switch ............................................................................................. 40 
Figure 20 –Dust Plugs................................................................................................................. 41 
Figure 21 –Remove Nut.............................................................................................................. 41 
Figure 22 –Insert Tube ............................................................................................................... 41 
Figure 23 –Tighten Nut............................................................................................................... 42 
Figure 24 –Installation of USB Memory Stick............................................................................. 43 
Figure 25 –Switching the Battery ON/OFF ................................................................................. 43 
Figure 26 –Dust Plugs................................................................................................................. 46 
Figure 27 –Packing Instruction................................................................................................... 47 
Figure 28 –Front Panel ............................................................................................................... 50 
Figure 29 –Home Screen ............................................................................................................ 52 
Figure 30 –Quick Menu Screen .................................................................................................. 55 
Figure 31 –Main Menu screen ................................................................................................... 56 
Figure 32 –Analyser State Menu Screen .................................................................................... 57 

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Figure 33 –Status Menu Screen.................................................................................................. 58 
Figure 34 –Temperature Menu Screen.......................................................................................59 
Figure 35 –Pressure & Flow Menu Screen..................................................................................60 
Figure 36 –Voltage Menu Screen ...............................................................................................61 
Figure 37 –General Settings Menu Screen................................................................................. 62 
Figure 38 –Measurement Settings Menu Screen.......................................................................63 
Figure 39 –Calibration Menu Screen .......................................................................................... 64 
Figure 40 –Pressure Calibration Menu Screen ...........................................................................66 
Figure 41 –Ozone Calibration Menu Screen...............................................................................67 
Figure 42 –Flow Calibration Menu Screen..................................................................................68 
Figure 43 –Service Menu Screen ................................................................................................69 
Figure 44 –Diagnostics Menu Screen .........................................................................................70 
Figure 45 –Digital Pots Menu .....................................................................................................70 
Figure 46 –Internal Pump Menu Screen..................................................................................... 72 
Figure 47 –Valve Menu Screen................................................................................................... 73 
Figure 48 –Tests Menu Screen ...................................................................................................74 
Figure 49 –Digital Input Test Menu Screen ................................................................................75 
Figure 50 –Digital Output Test Menu Screen ............................................................................. 75 
Figure 51 –Calculation Factors Menu Screen .............................................................................76 
Figure 52 –Communications Menu Screen.................................................................................77 
Figure 53 –Data Logging Menu Screen....................................................................................... 78 
Figure 54 –Serial Communication Menu Screen ........................................................................78 
Figure 55 –Analog Input Menu Screen.......................................................................................79 
Figure 56 –Analog Output Menu Screen.................................................................................... 80 
Figure 57 –Digital Input Menu Screen........................................................................................82 
Figure 58 –Digital Output Menu Screen.....................................................................................83 
Figure 59 –Network Menu Screen..............................................................................................84 
Figure 60 –Bluetooth Menu Screen............................................................................................85 
Figure 61 –Trend Display Menu Screen...................................................................................... 86 
Figure 62 –Chart Screen .............................................................................................................87 
Figure 63 –Advanced Menu.........................................................................................................89 
Figure 64 –Hardware Menu Screen............................................................................................90 
Figure 65 –Parameter Display Menu Screen .............................................................................. 91 
Figure 66 –Communication Ports...............................................................................................93 
Figure 67 –Multidrop RS232 Cable Example ..............................................................................94 
Figure 68 –Example of Typical Network Setups .........................................................................95 
Figure 69 –Example of Network Menu Setup.............................................................................97 
Figure 70 –Port Forwarding Example .........................................................................................97 
Figure 71 –LAN Network Set-Up (Airodis) ..................................................................................98 
Figure 72 –WAN Network Set-Up (Airodis) ................................................................................98 
Figure 73 –25 Pin Rear Panel PCA (Default Jumpers Highlighted) ...........................................100 
Figure 74 –Analog & Digital I/O Individual Pin Descriptions ....................................................101 
Figure 75 –Installing Driver Software (Device Manager).......................................................... 102 
Figure 76 –Update Driver Popup..............................................................................................103 

 
 
Introduction 
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Figure 77 –Update Driver Popup (Directory Location)............................................................. 103 
Figure 78 –Installing Driver Confirmation Prompt................................................................... 104 
Figure 79 –Successful Driver Installation ................................................................................. 104 
Figure 80 –Airodis Workspace Manager .................................................................................. 105 
Figure 81 –Adding a New Station............................................................................................. 106 
Figure 82 –New Station Connection......................................................................................... 106 
Figure 83 –Station Configuration (Channel List) ...................................................................... 107 
Figure 84 –Error Status Notification......................................................................................... 107 
Figure 85 –Downloading Data.................................................................................................. 108 
Figure 86 –Download Data Status............................................................................................ 108 
Figure 87 –Data Visibility.......................................................................................................... 109 
Figure 88 –Exporting Data........................................................................................................ 109 
Figure 89 –Data Download Complete ...................................................................................... 110 
Figure 90 –Downloading the App from Google Play Store ...................................................... 111 
Figure 91 –Bluetooth Pairing Request...................................................................................... 111 
Figure 92 –Showing or Hiding the NumPad ............................................................................. 112 
Figure 93 –Switching Instruments............................................................................................ 113 
Figure 94 –Real-Time Plot ........................................................................................................ 114 
Figure 95 –Plot of Downloaded Data ....................................................................................... 115 
Figure 96 –Directory Settings................................................................................................... 116 
Figure 97 –Logs Format............................................................................................................ 116 
Figure 98 –Colour Theme Settings ........................................................................................... 117 
Figure 99 –Example of a Calibration System............................................................................ 119 
Figure 100 –Ozone Transfer Standard Hierarchy..................................................................... 121 
Figure 101 –Typical uses of Transfer Standards to Calibrate Instruments. ............................. 122 
Figure 102 –Full Pressure Calibration Set-up (Vacuum)........................................................... 124 
Figure 103 –Full Pressure Calibration Set-up (Ambient).......................................................... 124 
Figure 104 –Ambient Pressure Calibration Set-up................................................................... 125 
Figure 105 –Pressure Calibration (Internal Pump Option Only) Set-up................................... 126 
Figure 106 –Pump Bypass Flow................................................................................................ 127 
Figure 107 –Zero Calibration Set-up - 1 ................................................................................... 128 
Figure 108 –Zero Calibration Set-up - 2 ................................................................................... 129 
Figure 109 –Excel Graph of Multipoint Calibration.................................................................. 134 
Figure 110 –Single High Pressure Calibration Option .............................................................. 136 
Figure 111 –Minifit Extraction Tool –(PN: T030001)............................................................... 139 
Figure 112 –Orifice Removal Tool –(PN: H010046)................................................................. 140 
Figure 113 –Leak Test Jig –(PN: H050069) .............................................................................. 140 
Figure 114 –Air Monitoring Test Equipment Kit (AMTEK) –Customisable.............................. 140 
Figure 115 –Remove Kynar Nut................................................................................................ 142 
Figure 116 –Remove Retaining Ring......................................................................................... 142 
Figure 117 –Remove Filter Sealing Cap.................................................................................... 143 
Figure 118 –Particulate Filter................................................................................................... 143 
Figure 119 –Avoid to Touch Particulate Filter Paper ............................................................... 144 
Figure 120 –Kynar Elbow Barb Fitting Direction ...................................................................... 144 

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Figure 121 –Remove Filter Casing and Filter............................................................................145 
Figure 122 –Leak Test Jig on Exhaust Port................................................................................145 
Figure 123 –Connect Vacuum Source....................................................................................... 146 
Figure 124 –Kynar Blocker Nut.................................................................................................146 
Figure 125 –Pressure Gauge on Leak Test Jig...........................................................................147 
Figure 126 –Pump Bypass Flow ................................................................................................148 
Figure 127 –Barometer to Sample Port....................................................................................149 
Figure 128 –Barometer to Calibration Port..............................................................................150 
Figure 129 –Connect Span Source............................................................................................151 
Figure 130 –Ozone Scrubber ....................................................................................................151 
Figure 131 –Remove the Kynar Nut..........................................................................................152 
Figure 132 –Loosening Tube Collet from Detector End ...........................................................153 
Figure 133 –Removing Two Screws..........................................................................................153 
Figure 134 –Removing Detector Block from Optical Cell .........................................................154 
Figure 135 –Remove Retaining Screw ...................................................................................... 154 
Figure 136 –Removing Measurement Cell (Glass).................................................................... 155 
Figure 137 –Location of UV Lamp Securing Grub Screw ..........................................................156 
Figure 138 –Remove Screw ......................................................................................................157 
Figure 139 –Remove Lamp Block..............................................................................................157 
Figure 140 –Remove Lamp Mounting Block.............................................................................158 
Figure 141 –Remove Kynar Elbow Fitting.................................................................................158 
Figure 142 –Remove Orifice and Sintered Filter.......................................................................159 
Figure 143 –Test Point Location ............................................................................................... 160 
Figure 144 –Flow Fault Diagnostic Procedure..........................................................................166 
Figure 145 –Noisy Zero or Unstable Span Diagnostic Procedure............................................. 167 
Figure 146 –Lamp Temperature Failure Diagnostic Procedure................................................168 
Figure 147 –USB Memory Stick Failure ....................................................................................169 
Figure 148 –USB Memory Stick File Structure.......................................................................... 171 
Figure 149 –Dual Filter Option Installed...................................................................................173 
Figure 150 –Separate Rack Slides.............................................................................................174 
Figure 151 –Assemble Inner Slide on Chassis...........................................................................175 
Figure 152 –Rack Mount Ears Fitted to Instrument .................................................................175 
Figure 153 –Attach Rack Mount Adaptors to Outer Slides ...................................................... 176 
Figure 154 –Test Fit Rack Slide Assembly into Rack .................................................................176 
Figure 155 –Attach Slides to Front of Rack............................................................................... 177 
Figure 156 –Slide Clips..............................................................................................................177 
Figure 157 –IZS Additional Components ..................................................................................181 
Figure 158 –IZS Schematic........................................................................................................182 
List of Tables 
Table 1 –Internationally Recognised Symbols............................................................................ 13 
Table 2 –Manual Revision History ..............................................................................................18 
Table 3 –List of Items Received................................................................................................... 35 