Hanna Instruments HI 38018 User manual

Instruction Manual
HI 38018
Free Chlorine
Low and Medium
Range
Test Kit with
Checker Disc
Dear Customer,
Thank you for choosing a Hanna Product.
Please read the instruction sheet carefully before using the
test kit. It will provide you with the necessary information for
correct use of the kit. If you need additional information, do
not hesitate to e-mail us at [email protected].
Remove the chemical test kit from the packing material and
examine it carefully to make sure that no damage has
occurred during shipping. If there is any noticeable damage,
notify your Dealer or the nearest Hanna office immediately.
Each kit is supplied with:
•HI 93701-0 Free Chlorine Reagent, powder packet
(200 pcs);
• Demineralizer Bottle with filter cap for about 12 liters
of deionized water (depending on the hardness level
of water to be treated);
• 1 checker disc (containing a mirror, a mirror holder
and the disc);
• 2 glass vials with caps;
• 1 plastic pipette (3 mL).
Note: Any damaged or defective item must be returned in its
original packing materials.
ISTR38018R2 02/07
Chlorine is the most commonly used water disinfectant in
applications that vary from treatment of drinking water and
wastewater, pool and spa sanitization, to food processing
and sterilization. Chlorine present in water binds with bacteria,
leaving only a part of the original quantity (free chlorine) to
continue its disinfecting action. If the free chlorine level is
improper with respect to pH, water will have an unpleasant
taste and odor and the disinfecting potential of the chlorine
will be diminished.
Free chlorine reacts with ammonium ions and organic
compounds to form chlorine compounds resulting in
diminished disinfecting capabilities compared with free
chlorine. Chlorine compounds together with chloramines form
combined chlorine. Combined chlorine and free chlorine
together result in total chlorine.
While free chlorine has a much higher disinfectant potential,
combined chlorine has a much higher stability and has a
lesser volatility.
Note: mg/L is equivalent to ppm (parts per million).
The reaction between chlorine and the DPD reagent causes a
pink tint in the sample which is proportional to the chlorine
concentration.
READ THE ENTIRE INSTRUCTIONS BEFORE USING THE KIT
• To measure free chlorine in the 0-0.7 mg/L range,
verify that the mirror, its holder and the disc are pre-
installed in the checker disc. If not, install them as shown
in the figure.
• Use the pipette to fill
each glass vial with 10
mL of sample (up to
the mark).
• Insert one of the vials into the left hand opening of the
checker disc. This is the blank.
•Remove the cap and fill
the Demineralizer Bottle
with tap water.
• Replace the cap and
shake gently for at
least 2 minutes. The
demineralized water is
now ready.
• Flip open the top of the Demineralizer Bottle cap. By
gently squeezing the bottle, add demineralized water to
the other vial up to the 20 mL mark. Replace the cap
and shake to mix.
10 mL
• Remove the cap and add 1 packet of HI 93701-0 Free
Chlorine Reagent. Replace the cap and mix. This is the
reacted sample.
• Remove the cap and insert the reacted sample into the
right hand opening of the checker disc.
• Hold the checker disc so that a light source illuminates
the samples from the top.
• Keep the checker disc at a distance of 30-40 cm (12-
16") from the eyes to match the color. Rotate the disc
while looking at the color test windows and stop when
you find the color match. Read the value in the result
window and divide it by 5 to obtain mg/L (or ppm) of
Chlorine.
Range 0 to 0.7 mg/L (ppm) as Chlorine (LR)
0 to 3.5 mg/L (ppm) as Chlorine (MR)
Smallest Increment LR: 0.02 mg/L
MR: 0.1 mg/L
Analysis Method Colorimetric
Sample Size 10 mL (LR), 5 mL (MR)
Number of Tests 200
Case Dimensions 235x175x115 mm (9.2x6.9x4.5")
Shipping Weight 647 g (22.8 oz.)
www.hannainst.com
Specifications
Significance and use
Chemical Reaction
Instructions

• To measure free chlorine in the 0-3.5 mg/L range,
remove the disc, mirror and its holder, if pre-installed.
Then install just the disc as shown here.
• Use the pipette to fill each glass
vial with 5 mL of sample (up to
the mark) and insert one of them
into the left hand opening of the
checker disc. This is the blank.
• Add to the other vial demineralized water up to the 10
mL mark and shake to mix.
• Add 1 packet of HI 93701-0 Free Chlorine Reagent.
Replace the cap and mix. This is the reacted sample.
• Remove the cap and insert the reacted sample into the
right hand opening of the checker disc.
5 mL
The chemicals contained in this kit may be hazardous if
improperly handled. Read the relevant Safety Data Sheet
before performing this test.
Adaptation of the EPA recommended DPD method 330.5.
References
Safety Data Sheets
• Hold the checker disc so that a light source illuminates
the samples from the back of the windows.
• Keep the checker disc at a distance of 30-40 cm (12-
16") from the eyes to match the color. Rotate the disc
while looking at the color test windows and stop when
you find the color match. Read the value in the result
window directly in mg/L (or ppm) of Chlorine.
For best results:
Perform the reading three times and take the average
value (divide by 3 the sum of the three numbers).
Intensely colored samples will make the color matching
difficult and they should be adequately treated before
performing the test. Suspended matter in large amounts
should be removed by prior filtration.
Caution:
Ultraviolet radiation may cause fading of colors. When
not in use, keep the disc protected from light, in a
cool and dry place.
Interferences:
Bromine, iodine, fluorine, ozone, oxidized manganese
and chromium.
Accessories
HI 93701-01 Free Chlorine reagents for 100 tests
HI 93701-03 Free Chlorine reagents for 300 tests
HI 740231 20 ml glass cylinders with caps (2 pcs)
DEMI-10 Demineralizer Bottle