Julabo SC 2500a User manual

19514551-V7.doc 18.07.2017
Operating Manual
SemiChill Recirculating Coolers
Eco-Series
SC 2500a
air cooled
SC 2500w
water cooled
E
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-
A
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OFF
ON
SC 2500
°C
10
30
60 130
180
220
ESC
°C
Flow
Cond.
1.951.4551-V7 07/17
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2
Congratulations!
You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the operation and
possible applications of our circulators. For optimal utilization of all functions, we recommend that you
thoroughly study this manual prior to beginning operation.
The JULABO Quality Management System
Temperature control devices for research and industry are developed,
produced, and distributed according to the requirements of ISO 9001 and
ISO 14001. Certificate Registration No. 01 100044846
Unpacking and inspecting
Unpack the circulator and accessories and inspect them for possible transport damage. Damage
should be reported to the responsible carrier, railway, or postal authority, and a damage report should
be requested. These instructions must be followed fully for us to guarantee our full support of your
claim for protecting against loss from concealed damage. The form required for filing such a claim will
be provided by the carrier.
Printed in Germany Changes without prior notification reserved
Important: keep original operating manual for future use
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Recirculating Cooler
3
TABLE OF CONTENTS
Operating manual................................................................................................................ 5
1. Intended use.................................................................................................................5
1.1. Description...............................................................................................................5
2. Operator responsibility – Safety instructions................................................................. 5
2.1. Disposal................................................................................................................... 7
2.2. EC Declaration of Conformity................................................................................... 8
2.3. Warranty conditions ................................................................................................. 9
2.4. Technical specifications ......................................................................................... 10
2.5. Cooling water connection....................................................................................... 14
Operating instructions .......................................................................................................15
3. Operating controls and functional elements................................................................ 15
4. Safety notes for the user............................................................................................. 17
4.1. Explanation of safety notes.................................................................................... 17
4.2. Explanation of other notes...................................................................................... 17
4.3. Safety instructions.................................................................................................. 18
5. Preparations............................................................................................................... 20
5.1. Installation.............................................................................................................. 20
5.2. Connecting the external system............................................................................. 21
5.2.1.Tubing ............................................................................................................... 22
5.2.2.Bath fluids.......................................................................................................... 22
5.3. Filling ..................................................................................................................... 23
5.4. Draining ................................................................................................................. 24
6. Operating procedures................................................................................................. 25
6.1. Power connection................................................................................................... 25
6.2. Switching on / Start - Stop...................................................................................... 25
6.3. AUTOSTART ON / OFF......................................................................................... 26
7. Setting the temperatures .................................................................................. 27
8. Safety installations, warning functions............................................................... 27
8.1. Excess temperature protection............................................................................... 27
8.2. Early warning system, low level protection............................................................. 28
8.3. High and low temperature warning functions.......................................................... 29
8.4. Limitation of the operating temperature range........................................................ 30
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8.5. Change-over of the warning function to shutdown function .....................................31
9. Menu functions...................................................................................................32
9.1. Setting the pump pressure......................................................................................33
9.2. ATC Absolute Temperature Calibration, 3-point calibration.....................................33
9.3. Remote control: activate – deactivate......................................................................36
9.4. Interface - Baud rate, Handshake, Parity.................................................................36
9.5. Control parameters – Xp, Tv, Tn.............................................................................37
9.6. Reset ......................................................................................................................39
10. Troubleshooting guide / Error messages .....................................................................39
11. Electrical connections..................................................................................................41
12. Remote control............................................................................................................42
12.1. Setup for remote control..........................................................................................42
12.2. Communication with a PC or a superordinated data system ...................................42
12.3. List of commands....................................................................................................43
12.4. Status messages ....................................................................................................45
12.5. Error messages.......................................................................................................45
13. JULABO Service – Online remote diagnosis................................................................46
14. Cleaning / repairing the unit.........................................................................................47
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Recirculating Cooler
5
Operating manual
1. Intended use
JULABO recirculating coolers have been designed to control the temperature of specific fluids in a
bath tank. The units feature pump connections for temperature control of external systems (loop
circuit).
JULABO recirculating coolers are not suitable for direct temperature control of foods,
semi-luxury foods and tobacco, or pharmaceutical and medical products. Direct
temperature control means unprotected contact of the object with the bath medium (bath
fluid).
1.1. Description
PID2
ATC
3
RS232
PUMP
SMART
;The recirculating coolers are operated via the splash-proof keypad. The
implemented microprocessor technology allows to set and to store different values
that can be indicated on the MULTI-DISPLAY (LED). Three menu keys facilitate
adjusting setpoints, warning and safety functions and menu functions.
;The PID temperature control adapts the heat supplied to the thermal requirements
of the bath.
;Absolute Temperature Calibration (ATC3) provides a high temperature stability in
the bath. With the 3-point calibration an offset is adjusted at three temperatures to
ensure an accurate temperature pattern at the selected spot in the bath over the
full temperature range.
;Electrical connections:
The serial interface RS232 allows modern process technology without additional
interface.
;The excess temperature protection conforming to IEC 61010-2-010 is a safety
installation independent from the control circuit. This protection can be indicated
and set on the MULTI-DISPLAY (LED).
;The early warning system for low level signals that bath fluid needs to be refilled
before the low level protection conforming to IEC 61010-2-010 causes a complete
shut-down of the main functional elements.
;The pump capacity (electronically adjustable via the motor speed) enables to adapt
to varying conditions for internal and external temperature applications.
2. Operator responsibility – Safety instructions
The products of JULABO ensure safe operation when installed, operated, and maintained according to
common safety regulations. This section explains the potential dangers that may arise when operating
the circulator and also specifies the most important safety precautions to preclude these dangers as far
as possible.
The operator is responsible for the qualification of the personnel operating the units.
¾The personnel operating the units should be regularly instructed about the dangers involved with
their job activities as well as measures to avert these dangers.
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Operator responsibility – Safety instructions
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¾Make sure all persons tasked with operating, installing, and maintaining the unit have read and
understand the safety information and operating instructions.
¾When using hazardous materials or materials that could become hazardous, the circulator may be
operated only by persons who are absolutely familiar with these materials and the circulator. These
persons must be fully aware of possible risks.
If you have any questions concerning the operation of your unit or the information in this manual,
please contact us!
Contact:
Safety instructions for the operator:
¾Avoid strikes to the housing, vibrations, damage to the operating-element panel (keypad, display),
and contamination.
¾Make sure the product is checked for proper condition regularly (depending on the conditions of
use). Regularly check (at least every 2 years) the proper condition of the mandatory, warning,
prohibition and safety labels.
¾Make sure that the mains power supply has low impedance to avoid any negative effects on the
instruments being operated on the same mains.
¾This unit is designed for operation in a controlled electromagnetic environment. This means that
transmitting devices (e.g., cellular phones) should not be used in the immediate vicinity.
¾Magnetic radiation may affect other devices with components sensitive to magnetic fields (e.g.,
monitors). We recommend maintaining a minimum distance of 1 m.
¾Permissible ambient temperature: max. 40 °C, min. 5 °C.
¾Permissible relative humidity: 50% (40 °C).
¾Do not store the unit in an aggressive atmosphere. Protect the unit from contamination.
¾Do not expose the unit to sunlight.
Appropriate operation
Only qualified personnel is authorized to configure, install, maintain, or repair the circulator.
Persons who operate the circulator must be trained in the particular tasks by qualified personnel. The
summarized user guidance (short manual) and the specification table with information on individual
parameters are sufficient for this.
Use
The bath can be filled with flammable materials. Fire hazard!
There might be chemical dangers depending on the bath medium used.
Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data
sheets).
Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well
ventilated areas.
Only use recommended materials (bath fluids). Only use non-acid and non corroding materials.
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Recirculating Cooler
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When using hazardous materials or materials that could become hazardous, the operator must affix
the enclosed safety labels (1 + 2) to the front of the unit so they are highly visible:
1
Danger area. Attention! Observe instructions.
(operating manual, safety data sheet)
2
or
Carefully read the user information prior to beginning operation.
Scope: EU
2
Carefully read the user information prior to beginning operation.
Scope: USA, NAFTA
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.
Hot surface warning.
(The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to the
circulator, particularly the corresponding safety instructions. Also observe the pin assignment of plugs
and technical specifications of the products.
2.1. Disposal
The recirculating cooler contains a back-up battery that supplies voltage to the memory chips when
the unit is switched off. Do not dispose of the battery with household waste!
Depending on battery regulations in your country, you may be obligated to return used or defective
batteries to collection sites.
The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or
synthetic oil. For disposal, follow the instructions in the material safety data sheets.
This unit contains the refrigerant R452A which at this time is not considered harmful to the ozone
layer. However, over the long operating period of the unit, disposal rules may change. Therefore, only
qualified personnel should handle the disposal.
Valid in EU countries
See the current official journal of the European Union – WEEE directive.
Directive of the European Parliament and of the Council on waste electrical and
electronic equipment (WEEE).
This directive requires electrical and electronic equipment marked with a crossed-
out trash can to be disposed of separately in an environmentally friendly manner.
Contact an authorized waste management company in your country.
Disposal with household waste (unsorted waste) or similar collections of municipal
waste is not permitted!
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Operator responsibility – Safety instructions
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2.2. EC Declaration of Conformity
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Recirculating Cooler
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2.3. Warranty conditions
JULABO GmbH warrants its products against defects in material or in workmanship, when used under
appropriate conditions and in accordance with appropriate operating instructions
for a period of ONE YEAR.
Extension of the warranty period – free of charge
With the ‘1PLUS warranty’ the user receives a free of charge extension to the warranty of up to 24
months, limited to a maximum of 10 000 working hours.
To apply for this extended warranty the user must register the unit on the JULABO web site
indicating the serial no. The extended warranty will apply from the date of JULABO GmbH’s original
invoice.
JULABO GmbH reserves the right to decide the validity of any warranty claim. In case of faults arising
either due to faulty materials or workmanship, parts will be repaired or replaced free of charge, or a
new replacement unit will be supplied.
Any other compensation claims are excluded from this guarantee.
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Operator responsibility – Safety instructions
10
2.4. Technical specifications
Eco- Series SC 2500a SC 2500w
Working temperature ranges:
Standard unit °C +5 ... +35 +5 ... +35
Option Low Temp °C -20 ... +35 -20 ... +35
Option Low /HighTemp I °C -20 ... +80 -20 ... +80
Temperature stability °C 0.1 0.1
Absolute Temperature Calibration ±3 ±3
Heater wattage (at 230 V) Option H1 kW 1.0 1.0
Cooling capacity °C
Medium ethanol kW +20 0 -10
2.5 1.5 0.9 +20 0 -10
2.5 1.5 0.9
Refrigerant R452A R452A
Pump capacity P3
see table 1 page 11
Flow rate P3 L/min at 0 bar 33 33
Pressure max. P3 bar at 0 liters 3.5 3.5
Overall dimensions (WxDxH) cm 49x62/105 49x62/105
Filling volume liters 21 ... 33 21 ... 33
Weight kg 123 123
Ambient temperature °C 5 ... 40 5 ... 40
Mains power connection V/ Hz 230 / 50 230 / 50
Current consumption without heater A 11 (230 V) 11 (230 V)
Current consumption 1kW heater A 15 (230 V) 15 (230 V)
Mains power connection V/ Hz 208-230 / 60 208-230 / 60
Current consumption without heater A 11 (230 V) 11 (230 V)
Current consumption 1kW heater A 15 (230 V) 15 (230 V)
All measurements have been carried out at: rated voltage and frequencyambient temperature: 20 °C
Technical changes without prior notification reserved.
* Pump P3- reduces cooling capacity by 0.3 kW
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Recirculating Cooler
11
Eco- Series
Temperature selection digital
via keypad indication on LED-Multi-Display
remote control via personal computer indication on monitor
Temperature indication °C LED-Multi-Display
Resolution °C 0.1
Electrical connection:
Computer interface RS232
Table 1
Pump capacity
Bath fluid: Water, Silicone -oil
XX.XX
PUMP
1
XX.XX
PUMP
2
Circulating pump: P3 P3
Flow rate max. Lpm at 0 bar 30 33
Pressure max. bar at 0 liter 1.8 3.5
Bath fluid: Galden®
eg. Fluorinert®3283
Pressure max. bar at 0 liter 3.5
Notice:
If Galden®or Fluorinert®is used the charge of the motor increases. Wrong
adjustment causes overheating and eventually destruction of the motor.
xWith the circulation pump P3 a maximum pump pressure stage >PUMP 1< may
be adjusted.
The pump type can be recognized in the order no. on the name plate.
95 xx xxx _ xx PX xx
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Operator responsibility – Safety instructions
12
Safety installations according to IEC 61010-2-010:
Excess temperature protection adjustable from 0 °C ... 320 °C
Low liquid level protection float switch
Classification according to DIN 12876-1 class III
Supplementary safety installations
Early warning system for low level float switch
High temperature warning function optical + audible (in intervals)
Low temperature warning function optical + audible (in intervals)
Supervision of working sensor plausibility control
Reciprocal sensor monitoring between
working and safety sensors difference >35 K
Alarm message optical + audible (permanent)
Warning message optical + audible (in intervals)
Environmental conditions according to IEC 61 010-1:
Use indoors only.
Altitude up to 2000 m - normal zero.
Ambient temperature: see Technical specifications
Humidity:
Max. relative humidity 80% for temperatures up to +31 °C,
linear decrease down to 50% relative humidity at a temperature of +40 °C
Max. mains voltage fluctuations of ±10% are permissible.
Protection class according to IEC 60 529 IP21
The unit corresponds to Class I
Overvoltage category II
Pollution degree 2
Caution:
The unit is not for use in explosive environment.
EMC requirements
The device is an ISM device of group 1 per CISPR 11 (uses HF for internal purposes) and is classified
in class A (industrial and commercial sector).
Notice:
Devices of class A are intended for the use in an industrial electromagnetic
environment.
When operating in other electromagnetic environments, their electromagnetic
compatibility may be impacted.
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Recirculating Cooler
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Information about the used refrigerants
The Regulation (EU) No. 517/2014 on fluorinated greenhouse gases applies to all systems which
contain fluorinated refrigerants and replaces (EC) 842/2006.
The aim of the Regulation is to protect the environment by reducing emissions of fluorinated
greenhouse gases.
Among other things it regulates the emission limits, use and recovery of these substances. It also
contains requirements for operators of systems which require / contain these substances to function.
Under Regulation 517/2014, the operator of a system of this nature has the following duties:
xThe operator must ensure that the equipment is checked at regular intervals for leaks.
xThese intervals depend on the CO2equivalent of the system. This is calculated from the
refrigerant fill volume and type of refrigerant. The CO2equivalent of your system is shown on
the model plate.
xThe operator undertakes to have maintenance, repair, service, recovery and recycling work
carried out by certified personnel who have been authorized by JULABO.
xAll such work must be documented. The operator must keep records and archive them for at
least five years. The records must be submitted to the relevant authority on request.
Refer to the text of the Regulation for further information.
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Operator responsibility – Safety instructions
14
2.5. Cooling water connection
Cooling water pressure (IN/OUT) max. 6 bar
Pressure difference (IN - OUT) 3.5 to 6 bar
Cooling water consumption (IN with 15 °C) 5 l/min
Cooling water temperature < 20 °C
Notice: Cooling water circuit
Risk of oil leaking from the refrigeration system (compressor) of the recirculating
cooler into the cooling water in case of a fault in the cooling water circuit!
Observe the laws and regulations of the water distribution company valid in the location where
the unit is operated.
Notice:
Danger of corrosion of heat exchanger due to unsuitable quality of cooling
water.
xDue to its high content of lime, hard water is not suitable for cooling and causes
scale in the heat exchanger.
xFerrous water or water containing ferrous particles will cause formation of rust
even in heat exchangers made of stainless steel.
xChlorinated water will cause pitting corrosion in heat exchangers made of
stainless steel.
xDue to their corrosive characteristics, distilled water and deionized water are
unsuitable and will cause corrosion of the bath.
xDue to its corrosive characteristics, sea water is not suitable.
xDue to its microbiological (bacterial) components, which settle in the heat
exchanger, untreated and unpurified river water and water from cooling towers is
unsuitable.
xAvoid particulate matter in cooling water.
xAvoid putrid water.
Recommended quality of cooling water:
pH 7.5 to 9.0
Sulfate [SO4 2- ] < 100 ppm
Hydrocarbonate [HCO 3-]/sulfate [SO4 2-] > 1 ppm
Hardness [Ca 2+, Mg 2+]/[HCO 3-] > 0.5 qdH
Alkalinity 60 ppm < [HCO 3-] < 300 ppm
Conductivity ȝ6FP
Chloride (Cl -) < 50 ppm
Phosphate (PO4 3-) < 2 ppm
Ammonia (NH3) < 0.5 ppm
Free chlorine < 0.5 ppm
Trivalent iron ions (Fe 3+) < 0.5 ppm
Manganese ions (Mn 2+) < 0.05 ppm
Carbon dioxide (CO2) < 10 ppm
Hydrogen sulfide (H2S) < 50 ppm
Content of oxygen < 0.1 ppm
Algae growth impermissible
Suspended solids impermissible
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Recirculating Cooler
15
Operating instructions
3. Operating controls and functional elements
Front view Rear view
ENERGENCYSTOP
N
O
T
-
A
U
S
OFF
ON
SC 2500
°C
10
30
60 130
180
220
ES
C
°C
Flo
Con
d
12
3
4
5
6
7
8
9
10
12
20
19
21
22
23
24
25
26
1 Mains power switch
2 Emergency stop switch
3
°
C
10
30
60 130
18
0
220
Adjustable excess temperature protection according to IEC 61010-2-010
4 Keypad
Start / stop key
Key for selecting the working temperature - Setpoint 1, 2, 3
Key for selecting the warning and safety values
MENU button - for selecting the menu functions
Cursor keys (left or right)
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Operating controls and functional elements
16
Edit keys (increase or decrease)
Enter key 1) Store value / parameter
2) Next lower menu level
Escape key 1. Cancel entries
2. Return to a higher menu level
5 MULTI-DISPLAY (LED) temperature indication, menu indication
5.1 Control indicator –Heating
5.2 Control indicator – Cooling
5.3 Control indicator – Alarm
6 Filling level indication
7
Manometer (feed pressure)
8 Handle
9 Filling opening
10 Venting grid, removable
(only air cooled recirculating cooler)
12
RS232
Interface RS232: remote control via personal computer
19
2 Connectors for solenoid valve. 230 V / max. 0.1 A
No control voltage in the -OFF- condition
20
2 Safety cutouts: Mains fuses 16 A
0
1
Motor protection circuit breaker for compressor motor
21 Mains power cable with plug
22
23
Pump connectors: 3/4” NPT male
OUT / Feed IN / Return
24 Overflow connector, M10x1 female
Order-No. 8 970 460 Barbed fitting for tubing 8 mm inner dia.
LClosable when using e.g. 3M Fluorinert ®as temperature liquid.
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Recirculating Cooler
17
25
Discharge nozzle with cap nut, Connection: ½ " male
Recommendation:
Before filling please install a drain cock at the discharge nozzle.
(not included in delivery)
Order-No. 8 920 100 Drain cock, stainless steel
26
Only for water cooled models: Cooling water OUTLET and INLET
4. Safety notes for the user
4.1. Explanation of safety notes
In addition to the safety warnings listed above, warnings are posted throughout the
manual. These warnings are designated by an exclamation mark inside an equilateral
triangle. “Warning of a dangerous situation (Attention! Please follow the
documentation).”
The danger is classified using a signal word.
Read and follow these important instructions.
Warning:
Describes a possibly highly dangerous situation. If these instructions are not followed,
serious injury and danger to life could result.
Caution:
Describes a possibly dangerous situation. If this is not avoided, slight or minor injuries
could result. A warning of possible property damage may also be contained in the text.
Notice:
Describes a possibly harmful situation. If this is not avoided, the product or anything in
its surroundings can be damaged.
4.2. Explanation of other notes
Note!
Draws attention to something special.
Important!
Indicates usage tips and other useful information.
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Safety notes for the user
18
4.3. Safety instructions
Follow the safety instructions to avoid personal injury and property damage. Also, the valid
safety instructions for workplaces must be followed.
xOnly connect the unit to a power socket with an earthing contact (PE – protective
earth)!
xThe power supply plug serves as a safe disconnecting device from the line and
must always be easily accessible.
xPlace the unit on an even surface on a base made of nonflammable material.
xDo not stay in the area below the unit.
xMake sure you read and understand all instructions and safety precautions listed
in this manual before installing or operating your unit.
xSet the excess temperature safety installation at least below the flash point of the
bath fluid.
xNever operate the unit without bath fluid in the bath.
xPay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the fluid.
xPrevent water from entering the hot bath oil.
xDo not drain the bath fluid while it is hot!
Check the temperature of the bath fluid prior to draining (e.g., by switching the
unit on for a short moment).
xUse suitable connecting tubing.
xAvoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
xMake sure that the tubing is securely attached.
xRegularly check the tubing for material defects (e.g., for cracks).
xNever operate damaged or leaking units.
xAlways turn off the unit and disconnect the mains cable from the power source
before performing any service or maintenance procedures, or before moving the
unit.
xAlways turn off the unit and disconnect the mains cable from the power source
before cleaning the unit.
xAlways empty the bath before moving the unit.
xTransport the unit with care.
xSudden jolts or drops may cause damage in the interior of the unit.
xObserve all warning labels.
xNever remove warning labels.
xNever operate units with damaged mains power cables.
xRepairs are to be carried out only by qualified service personnel.
xSome parts of the bath tank and the pump connections may become extremely
hot during continuous operation. Therefore, exercise particular caution when
touching these parts.
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Recirculating Cooler
19
Caution:
The unit may be used, for example, to control the temperature of fluids in a reactor.
We do not know what substances are contained in these vessels.
Many substances are:
xinflammable, easily ignited, or explosive
xhazardous to health
xenvironmentally hazardous
i.e.: dangerous
The user alone is responsible for the handling of these substances!
The following questions should help to recognize possible dangers and to reduce the
risks to a minimum.
xAre all tubes and electrical cables connected and layed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
xDo dangerous vapors or gases develop during heating?
Must the work be done in a fume hood?
xWhat to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and
determine the method of decontamination.

Notice:
Check the safety installations at least twice a year!
xExcess temperature protection according to IEC 61010-2-010
With a screwdriver, turn back the adjustable excess temperature protection until
the shutdown point (actual temperature).
xLow level protection according to IEC 61010-2-010
To check the function of the float, it can be manually lowered with a screwdriver,
for example.
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Preparations
20
5. Preparations
5.1. Installation
xPlace the unit in an upright position.
For better stability, apply the holding brakes on the front casters.
xThe place of installation should be large enough and provide
sufficient air ventilation to ensure the room does not warm up
excessively because of the heat the instrument rejects to the
environment. (Max. permissible ambient temperature: 35 °C).
For a fault (leakage) in the refrigeration system, the standard EN
378 prescribes a certain room space to be available for each kg of
refrigerant.
The refrigerant quantity is specified on the type plate.
> For 0.423 kg of refrigerant R452A, 1 m3 of space is required.
xKeep at least 20 cm of open space on the front and rear venting
grids.
xDo not set up the unit in the immediate vicinity of heat sources
and do not expose to sun light
xBefore operating the unit after transport, wait about one hour after
installation. This will allow any oil that has accumulated laterally
during transport to flow back down, thus ensuring that the
compressor can develop its maximum capacity.
Recommendation:
Before filling please install a drain cock at the discharge nozzle. (25)
Connection: ½ " male (not included in delivery)
Order-No. 8 920 100 Drain cock, stainless steel
Cooling water connection (26)
Only for water cooled models:
Ensure circulation of cooling water by connecting the tubing to cooling
water inlet and outlet on the rear of the recirculating cooler.
Cooling water connectors G3/4” male
Cooling water temperature <20 °C
Cooling water see page 14
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