Knick Protos 34009(X) Parts list manual

Protos® 3400(X)
Additional Functions
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Latest Product Information:
www.knick.de

Knick
Elektronische Messgeräte GmbH & Co. KG
P.O. Box 37 04 15
D-14134 Berlin
Phone: +49 (0)30 - 801 91 - 0
Fax: +49 (0)30 - 801 91 - 200
Internet: http://www.knick.de
[e-mail]
©2010 Subject to change without notice
Trademarks
The following registered trademarks are used in this manual without further marking:
CalCheck®
Calimatic®
Protos®
Sensocheck®
Sensoface®
ServiceScope®
VariPower®
are registered trademarks of Knick GmbH & Co. KG, Germany
Memosens®
is a registered trademark of
Endress+Hauser Conducta GmbH & Co. KG, Germany
Knick Elektronische Messgeräte GmbH & Co. KG, Germany
SMARTMEDIA®
is a registered trademark of Toshiba Corp., Japan

3
Additional Functions
for the Protos 3400(X) modular measuring system
Provided by: TAN
Information on TAN release and SmartMedia cards
Additional functions
Provided by: TAN and SmartMedia card
How to order an additional function ................................................................................... 5
Activating an additional function (Option release) ........................................................ 6
SmartMedia card .......................................................................................................................32
SW 3400-001 KI recorder ......................................................................................................... 7
SW 3400-002 Specifiable buffer set (pH) ........................................................................13
SW 3400-004 ServiceScope ..................................................................................................14
SW 3400-005 Tolerance band recorder (pH) ..................................................................15
SW 3400-006 Current characteristic definable ..............................................................17
SW 3400-008 TC ultrapure water (COND) .......................................................................19
SW 3400-009 Concentration determination ..................................................................20
SW 3400-011 Dissolved oxygen measurement in carbonated beverages .........26
SW 3400-102 5 loadable parameter sets .........................................................................37
SW 3400-103 Measurement recorder ...............................................................................39
SW 3400-104 Extended logbook ........................................................................................42
SW 3400-106 Software update ...........................................................................................43
SW 3400-012 ISFET for PH 3400(X)-035 ISM module ..................................................28
SW 3400-107 AuditTrail (FDA 21 CFR Part 11) ...............................................................47
SW 3400-014 2nd channel for FIU 3400-141, FIU 3400X-140 ..................................30
SW 3400-015 OXY measurement for Memosens modules .......................................31
SW 3400-016 OXY trace measurement for Memosens modules............................31

4Protos 3400(X)

5
Device description
Enter this
serial number
when ordering
an additional function.
Device description
Return
22.7 °C
0.003mS/cm
Protos operating panel
Module FRONT 3400-011
Hardware: 2, Software: 9.0
Serial number: 3730737
BASE
Module FRONT
Additional functions expand the device capabilities.
The additional functions are device-specific. When ordering an additional
function, you therefore have to specify the serial number of your FRONT
module in addition to the respective order number.
(The FRONT module contains the Protos system control).
The manufacturer then supplies a TAN (transaction number) to release the
additional function.
Serial number of FRONT module
How to Order an Additional Function
Device-specific TAN (transaction number)
Menu Display Serial number FRONT module
Menu selection
Open diagnostics.
From the measuring mode:
Press menu key to select menu.
Select diagnostics using arrow keys,
confirm by pressing enter.
Menu selection
Return to meas
0.002mS/cm
23.7 °C
Select: [enter]
Lingua
Diagnostics
Return
23.7 °C
Set favorite
0.003mS/cm
Logbook
Message list
Device description
Module FRONT
Module CONDI 3400-051
Module BASE
Diagnostics
Select “Device description” using arrow
keys, confirm by pressing enter.

6Protos 3400(X)
Menu Display Activate additional function
Activating an Additional Function
Select menu: Parameter setting/System control/Release of options
Note: The TAN for releasing an additional function is only valid for the
device with the corresponding serial number (see previous page).
Release of options
Select the additional function to be
released.
Set option to “active”. Enter the TAN
at the prompt. (Note: The TAN is only
valid for the device with the corre-
sponding serial number, see previous
page.) The option is available after
the TAN has been entered.
Release of options (Administrator)
Return
25.6 °C
0.003mS/cm
001 KI recorder
004 ServiceScope
002 Buffer sets
006 Current characteristic
005 Cal tolerance band
Active
Inactive
Inactive
Inactive
Inactive
Menu selection
Open parameter setting.
From the measuring mode:
Press menu key to select menu.
Select parameter setting using arrow
keys, press enter to confirm.
Menu selection
Return to meas
Select: [enter]
Lingua
Parameter setting (Administrator)
System control
Return
25.6°C
Module BASE
Module OXY 3400-062
16.9%Air
Module PH 3400-032
Module CONDI 3400-051
Module FRONT
Parameter setting
Return
Viewing Level
Administrator Level (All Data) adm
(Operation Data) opl
(All Data) view
Operator Level
Parameter setting
Select Administrator level using arrow
keys, press enter to confirm.
Enter passcode and confirm
(Passcode as delivered: 1989).
Select system control using arrow
keys, press enter to confirm.
Then select Release of options using
arrow keys, press enter to confirm.
SW 3400-xxx
25.6 °C
0.003mS/cm
25.6 °C
0.003mS/cm

7
SW 3400-001: KI Recorder
Select menu: Parameter setting/Module FRONT/KI recorder
Additional function SW 3400-001
t
Variable
Measured signal
Message
Fig.: KI recorder, continuous process
t
Variable
Measured signal
Fig.: KI recorder, Batch process (Self-learning function)
Start End
The KI recorder follows the course of the process and releases a messages in
the event of a deviation. It is called from the measuring mode: meas
Continuous processes
The measured signal is surrounded by a dynamically tracked,
process- controlled tolerance band. Slight fluctuations are tolerated.
If the measured value leaves the tolerance range, a message is released (Fig.).
The recording interval can be set from 10 s to 60 h.
Batch processes
The KI recorder provides an automatic self-learning function. This allows
checking whether regularly recurring processes keep the preset tolerances.
Deviations from the normal course of process (plus preset tolerances) generate
a message (Fig.). Maximum process duration can be set from 1 to 60 h.
Tolerance band around the measured
signal generated by a low-pass filter
Preset tolerance band around the
measured signal

8Protos 3400(X)
SW 3400-001: KI Recorder
Menu Display Configuring the KI recorder
KI recorder
Called directly from the
measuring mode:
Press meas key.
For function description,
press “Info” softkey
“Info” softkey
Explains icons and capabilities of the
KI recorder
Configuring the KI recorder
• Parameter setting of FRONT module
• Select KI recorder
• Select the variables to be displayed
as well as the start and end values
• Set the recording interval
(10 s ... 60 h) (per pixel)
• Monitoring
(Off/Failure/Maintenance request)
Controlling the KI recorder
Example:
Select softkey usage: “KI recorder”:
• Select parameter setting, then:
• System control
• Function control matrix
• Softkey : “KI rec. Start/Stop”
Close
Recording data
Wait - HOLD
Failure value channel 2
Failure value channel 1
Info on KI recorder
Keys:
[enter]
[meas]
[menu]
Cursor to current
To meas. display
Call up menu
Cursor 1 line
Cursor 1/2 page
Info
°C
°C29.48.56
07/09/10 11:23
°C
22 °C
pH
pH,
pH5 pH
KI recorder
932
25.6°C
Input OK2
7.00pH
Return Connect
Function control matrix (Administrator)
Left softkey
Right softkey
Profibus DO 2
ParSet KI rec. Fav Unical
– –
–
–
–
–
KI recorder (Administrator)
Return
25.6°C
7.00 pH
Batch process
Channel 1
Channel 2
Recording interval 10s
Failure
Monitoring
Off
KI recorder
Continuous process

9
Menu Display KI recorder: Batch process
Configuring the KI recorder
• Parameter setting of FRONT module
• Select KI recorder
• Select the variables to be displayed
as well as the start, end values,
and deviation (%)
• Set process duration
(200 samples are recorded)
• Select “New record “Yes”
• Monitoring
(Off/Failure/Maintenance request)
Accessing the KI recorder
From the measuring mode:
Press meas key.
KI recorder (Administrator)
Return
25.6 °C
7.00 pH
Continuous process
Channel 1
Channel 2
New record Yes
Failure
Monitoring
Off
KI recorder
Batch process
Max. process duration No
Record KI stop
5
9
50 100 150 200
15
25
050 100 150 200
pH
°C
I
I
Parameters adjustable for batch operation
Variable
End
Start
Max. process
duration
Channel 1
Channel 2
The gray envelope represents the
deviation [%]
When the parameters are edited once more, the reference curve is
automatically re-adjusted to start, end and deviation.
When variable or process duration are changed, the curve will be deleted!
SW 3400-001: KI Recorder

10 Protos 3400(X)
SW 3400-001: KI Recorder
Display KI recorder: Batch process
Recording a reference curve
Start “Record” with left softkey.
Reference value and envelope are displayed
during the recording process. At the end of
recording or after “KI stop” the KI recorder
switches to control mode.
KI pause KI stop
5
9
50 100 150 200
20
27
050 100 150 200
pH
°C
I
I
KI start KI stop
5
9
50 100 150 200
20
27
050 100 150 200
pH
°C
I
I
In control mode only the envelope is visible.
Batch control
After a synchronous start the recorder monitors
whether the currently measured values remain
within the envelope.
Every deviation can trigger a message.
KI pause: Stops the recorder.
KI stop: Terminates control.
Pressing “Continue” restarts a stopped recorder.
Note: In HOLD mode (e.g. during calibration)
neither recording nor checking of a batch are
interrupted. The last measured value continues
to be used.
KI pause KI stop
5
9
50 100 150 200
20
27
050 100 150 200
pH
°C
I
I
Cursor

11
SW 3400-001: KI Recorder
• Saving / loading reference curves
Up to 5 batch reference curves can be stored on and retrieved
from a SmartMedia card:
Parameter setting / System control / KI batch recording
The reference curve, envelope, time response and KI settings are
saved.
• Archiving of completed batch processes
Complete batch results can be archived on the SmartMedia card.
All reference values and current batch data are stored in the
archive.
Display KI recorder: Batch process
Evaluation
Within the “KI recorder” function you can evalu-
ate a reference curve directly on the device.
To do so, use the arrow keys (up/down).
The reference curves and the most important
parameters are displayed one after the other.
KI pause KI stop
5
9
50 100 150 200
Evaluation channel 1:
pH
I
Control via OK2 input
5
9
50 100 150 200
20
27
050 100 150 200
pH
°C
I
I
External control
A Start/Stop function can be remote-controlled
via the OK2 input (BASE module) or via the
COMPA 3400(X)-081 PROFIBUS module
(To set the control element, call:
Parameter setting / System control /
Function control matrix).
The softkeys will then be deactivated.
The K1, K2, and K3 contacts of the BASE
module can be assigned to the “KI rec active”
signal.
Contact K3
Return
25.6 °C
7.00 pH
Limit value
Contact type
NAMUR maintenance
Usage
KI rec. active
Rinse contact
NAMUR HOLD
End
Start
Deviation
Process duration
9.00 pH
5.00 pH
10 %
10 h
Max
Min
Max. deviation
Messages
8.35 pH
5.80 pH
7 %
0x

12 Protos 3400(X)

13
SW 3400-002: Specifiable Buffer Set
Select menu: Parameter setting/System control/Buffer table
Individual buffer set (with 3 buffer solutions) for pH measurement
Buffer table
You can enter an individual buffer set (with 3 buffer solutions). To do so, you
enter the nominal buffer values for the correct temperature (range 0 ... 95 °C /
5°C steps). Then this buffer set is available in addition to the permanently set
standard buffer solutions in the “Calimatic buffer” menu (select “Table”).
Menu Display Buffer table: Entering values
To enter a buffer set
• Open parameter setting
• System control
• Select “Buffer table”
• Select buffer to be entered
• Enter nominal buffer value and all
other values for the correct temper-
ature (right/left arrow keys to select
position, up/down arrow keys to
edit number, confirm by pressing
enter.)
The special buffer set is selected as follows:
Parameter setting/Module PH/Cal preset values/Calimatic buffer/Table.
Return
25.6 °C
7.20 pH
Point of measurement
Logbook
Concentration table
Release of options
Calculation Blocks
Buffer table
System control (Administrator)
Return
25.6 °C
7.10 pH
Buffer 2
Buffer 3
Buffer 1
Buffer table (Administrator)
Return
25.6 °C
7.10 pH
Nominal buffer value
pH value at 10 °C
pH value at 15 °C
pH value at 05 °C
pH value at 20 °C
pH value at 00 °C
Buffer 1 (Administrator)
+04.00 pH
+04.00 pH
+04.00 pH
+04.00 pH
+04.00 pH
+04.00 pH

14 Protos 3400(X)
Menu Display ServiceScope
SW 3400-004: ServiceScope (pH)
Select menu: Diagnostics/Module PH/ServiceScope
ServiceScope
(Diagnostics/Module PH 3400-xxx)
Displays the noise levels over the
time. Allows distinction of individual
disturbances, periodic and broadband
disturbances, which is helpful for
troubleshooting. An error message is
generated if the noise level exceeds
the failure limit.
ServiceScope
20.2 °C
Return
Fail
Noise
level
7.00 pH
t
ServiceScope
ServiceScope monitors the pH input signal and checks whether it remains in
the control range. An error message is generated if the input signal exceeds the
failure limit.

15
Menu Display Tolerance band recorder
Cal record
SW 3400-005: Tolerance Adjustment (pH)
Select menu: Diagnostics/Module PH/Tolerance band recorder
Tolerance band recorder
(Diagnostics/Module PH 3400-xxx)
Records the tolerance ranges for zero
and slope over the time. New calibra-
tion values are only accepted if the
tolerance limits have been exceeded.
Display can be graphical or as a listing.
T-band recorder
Return
Zero
22.3 °C
7.00 pH
Slope 61.750.78.006.00
Tolerance band recorder
(For adjusting the tolerance band, see next page.)
During manual calibration this function checks the zero and slope values and
automatically performs an adjustment when the tolerance band is exceeded.
The parameters are stored in the tolerance band recorder (Diagnostics menu).
If the zero and slope values determined during calibration remain within their
tolerance bands, the new data are not saved.
Drift due to aging or calibration scatter can be identified at a glance, thus
allowing to draw conclusions as to electrode life and the required calibration
interval.
In the Calibration record you see whether the data have been saved or
whether the old data can still be tolerated.
Cal record
Return
22.3 °C
7.00 pH
Last calibration
Old el data
05/02/2010 11:24
Cal tolerance band
Cal mode
7.00 pH
Calimatic
Zero point
Slope
0 mV
58.0 mV/pH
Isothermal potential
Cal record
(Diagnostics/Module PH 3400-xxx)
In the Cal record you can see whether
the data have been saved (New el
data) or whether the old calibration
data can still be tolerated (Old el data).

16 Protos 3400(X)
SW 3400-005: Tolerance Adjustment (pH)
Adjustment of tolerance band. Select menu:
Parameter setting/Module PH/Cal preset values/Cal tolerance band
Menu Display Parameter setting
Menu selection
From the measuring mode:
Press menu key to select menu.
Select parameter setting using arrow
keys, press enter to confirm.
Passcode as delivered: 1989
Parameter setting
Select “PH” module,
press enter to confirm.
pH module
Select "Cal preset values" using arrow
keys. Press enter to confirm.
Then select "Cal tolerance band".
Menu selection
Return to meas
17.1 °C
Select: [enter]
Lingua
7.00 pH
Parameter setting (Administrator)
17.1°C
Return
Module CONDI 3400-051
Module FRONT 3400-011
Module BASE 3400-021
7.00pH
System control
Module PID 3400-121
Module PH 3400-032
Module PH 3400-032 (Administrator)
17.1 °C
TC process medium
Sensor data
Cal preset values
7.00pH
ORP/rH value
Delta function
Input filter
Block
Return
Cal tolerance band (Administrator)
17.1 °C
Tolerance Zero
Tolerance band check
7.00pH
Tolerance Slope
Calibration data taken over when
tolerance band is exceeded
Block
Return
+02.00 pH
On
002.0 mV/pH
Off
Cal tolerance band
Enter tolerance ranges for zero and
slope
(enter numbers using arrow keys,
confirm by pressing enter.)

17
SW 3400-006: Current Characteristic Definable
Select menu: Parameter setting/Module BASE (OUT)/Output current/
Characteristic
Menu Display Specifying a current characteristic
Table characteristic
Assign output current to measured
value in 1-mA steps.
Select menu: Parameter setting/
Module BASE (OUT)/Output current
First select process variable!
Then select curve: Table
25.6 °C
7.03 pH
Variable
Start
End
Output
Output filter
Curve
Output current I1 (Administrator)
Trilinear
Function
Linear
Table
0000 s
pH
Abort OK
+ 00.00 pH
+ 00.00 pH
+ 0000 pH
+ 0000 pH
+ 0000 pH
+ 0000 pH
OK
25.6 °C
7.03 pH
Variable
Output
Behavior during messages
Curve
Output filter
Output current I1 (Administrator)
Table
Table
0000 s
pH
Abort OK
4 ... 20 mA
The “Table” menu is displayed.
The entered values must be
continuously rising or falling.
On the following page, you find a list-
ing to write down your adjustments.
Value at 01 mA:
Value at 03 mA:
Value at 04 mA:
Value at 02 mA:
Value at 05 mA:
Value at 00 mA:
Table (Administrator)
Abort
25.6 °C
7.03 pH

18 Protos 3400(X)
Current Curve Adjustments – Original for Copy
Parameter setting/Module BASE (OUT)/Output current/
Characteristic "Table", own adjustments
Value at measured variable
00 mA ............... _________
01 mA ............... _________
02 mA ............... _________
03 mA ............... _________
04 mA ............... _________
05 mA ............... _________
06 mA ............... _________
07 mA ............... _________
08 mA ............... _________
09 mA ............... _________
10 mA ............... _________
11 mA ............... _________
12 mA ............... _________
13 mA ............... _________
14 mA ............... _________
15 mA ............... _________
16 mA ............... _________
17 mA ............... _________
18 mA ............... _________
19 mA ............... _________
20 mA ............... _________

19
SW 3400-008: TC Ultrapure Water (COND)
Select menu: Parameter setting/Module COND/TC process medium/
Ultrapure water
Menu Display TC process medium
TC process medium (Administrator)
22.3 °C
0.20mS/cm
Return
EN 27888 Natural waters (0 ... 35°C)
Ultrapure water: traces of impurity
TC correction
Reference temp
Impurity
Ultrapure wa NaCl
Ultrapure water with traces of
impurity
• Parameter setting
• Module COND
• TC process medium
• TC correction: Ultrapure water
Select type of impurity:
• NaOH
Alkaline ultrapure water
• NaCl
Neutral ultrapure water,
for conductivity measurement in
water processing behind gravel bed
filter
• HCl
Acidic ultrapure water,
for conductivity measurement
behind cation filter
• NH3
Ammoniacal ultrapure water
HCl
NaOH
NH3
OK

20 Protos 3400(X)
SW 3400-009: Concentration Determination
Select menu: Parameter setting/System control/Module COND/Concentration
Default settings and selection range
Concentration determination
The substance concentration in percent by weight (% by wt) is determined
for H2SO4, HNO3, HCl, NaOH, NaCl from the measured conductivity and
temperature values.
Conditions for concentration determination
Below you find tables with the concentration ranges of the preset substances.
These tables show the conductivity of the substances versus substance
concentration and process temperature.
The following conditions must be met for a reliable concentration
determination:
• For calculation of concentration, the medium to be measured must be
a purely binary mixture (e.g. water-hydrochloric acid). Presence of other
dissolved substances (e.g. salts) leads to incorrect concentration values.
• In the region of small slopes (e.g. at the range limits) small conductivity
changes can correspond to great concentration changes.
This may lead to an unsteady display of the concentration value.
• As the concentration value is calculated from the measured conductivity and
temperature values, accurate temperature measurement is very important.
Therefore, you should make sure that sensor and process medium are in
thermal equilibrium.
Messages
You can define limits for warning and failure messages for the concentration
value:
Select menu: Parameter setting/System control/Module COND/Messages