RKI Instruments 65-2340RK User manual

RKI Instruments, Inc.
www.rkiinstruments.com
65-2340RK
Toxic Gas Transmitter
Operator’s Manual
Part Number: 71-0143RK
Revision: G
Released: 6/12/20

2 • 65-2340RK Toxic Gas Transmitter
WARNING
Read and understand this instruction manual before operating detec-
tor. Improper use of the detector could result in bodily harm or death.
Periodic calibration and maintenance of the detector is essential for
proper operation and correct readings. Please calibrate and maintain
this detector regularly! Frequency of calibration depends upon the
type of use you have and the sensor types. Typical calibration frequen-
cies for most applications are between 3 and 6 months, but can be
required more often or less often based on your usage.

65-2340RK Toxic Gas Transmitter • 3
Product Warranty
RKI Instruments, Inc. warrants gas alarm equipment sold by us to be free from defects in
materials, workmanship, and performance for a period of one year from date of shipment from
RKI Instruments, Inc. Any parts found defective within that period will be repaired or
replaced, at our option, free of charge. This warranty does not apply to those items which by
their nature are subject to deterioration or consumption in normal service, and which must be
cleaned, repaired, or replaced on a routine basis. Examples of such items are:
Warranty is voided by abuse including mechanical damage, alteration, rough handling, or
repair procedures not in accordance with the operator’s manual. This warranty indicates the
full extent of our liability, and we are not responsible for removal or replacement costs, local
repair costs, transportation costs, or contingent expenses incurred without our prior approval.
THIS WARRANTY IS EXPRESSLY IN LIEU OF ANY AND ALL OTHER WARRANTIES AND
REPRESENTATIONS, EXPRESSED OR IMPLIED, AND ALL OTHER OBLIGATIONS OR
LIABILITIES ON THE PART OF RKI INSTRUMENTS, INC. INCLUDING BUT NOT
LIMITED TO, THE WARRANTY OF MERCHANTABILITY OR FITNESS FOR A
PARTICULAR PURPOSE. IN NO EVENT SHALL RKI INSTRUMENTS, INC. BE LIABLE
FOR INDIRECT, INCIDENTAL, OR CONSEQUENTIAL LOSS OR DAMAGE OF ANY KIND
CONNECTED WITH THE USE OF ITS PRODUCTS OR FAILURE OF ITS PRODUCTS TO
FUNCTION OR OPERATE PROPERLY.
This warranty covers instruments and parts sold to users by authorized distributors, dealers,
and representatives as appointed by RKI Instruments, Inc.
We do not assume indemnification for any accident or damage caused by the operation of this
gas monitor, and our warranty is limited to the replacement of parts or our complete goods.
a) Absorbent cartridges d) Batteries
b) Pump diaphragms and valves e) Filter elements
c) Fuses

4 • 65-2340RK Toxic Gas Transmitter
Table of Contents
Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Description. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Toxic Detector. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Amplifier. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Junction Box . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Mounting the Toxic Gas Transmitter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Wiring the Toxic Gas Transmitter. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Introducing Incoming Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Setting the Zero Signal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Preventive Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Replacing Components of the Toxic Gas Transmitter . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Calibration Frequency . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Preparing for Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Setting the Zero Reading. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Setting the Response Reading. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Returning to Normal Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Parts List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

65-2340RK Toxic Gas Transmitter • 5
Overview
This manual describes the 65-2340RK toxic gas transmitter. This manual also describes how
to install, start up, maintain, and calibrate the toxic gas transmitter when used with a gas
monitoring controller. A parts list at the end of this manual lists replacement parts and
accessories for the toxic gas transmitter.
The 65-2340RK toxic gas transmitter can be used for various target gases which are listed in
Table 1 below. For a particular target gas, the part number of the toxic transmitter will be of
the format 65-2340RK-XXX. For example, 65-2340RK-NH3 is for ammonia (NH3)
detection.
Specifications
Table 1 lists specifications for the toxic gas transmitter.
WARNING: When using the 65-2340RK, you must follow the instructions and warnings in
this manual to assure proper and safe operation of the 65-2340RK and to
minimize the risk of personal injury. Be sure to maintain and periodically
calibrate the 65-2340RK as described in this manual.
Table 1: Specifications
Target Gas 65-2340RK-ASH3: Arsine (AsH3)
65-2340RK-CL2: Chlorine (Cl2)
65-2340RK-CL-10: Chlorine (Cl2)
65-2340RK-HCN: Hydrogen Cyanide (HCN)
65-2340RK-NH3: Ammonia (NH3)
65-2340RK-SO2: Sulphur Dioxide (SO2)
65-2340RK-PH3: Phosphine (PH3)
Sampling Method Diffusion
Detection Range AsH3: 0 - 1.50 ppm
Cl2: 0 - 3.00 ppm
Cl2: 0 - 10.0 ppm
HCN: 0 - 15.0 ppm
NH3: 0 - 75.0 ppm
SO2: 0 - 6.00 ppm
PH3: 0 - 1.00 ppm
Accuracy ± 10% of reading or ± 5% of full scale (whichever is greater)
Signal Output 4 to 20 mA
Response Time •Cl
2and NH3: T90 in 90 seconds
• All others: T90 in 45 seconds
Operating Temperature &
Humidity • 14°F to 104°F (-10°C to 40°C)
• 20% to 90% Relative Humidity

6 • 65-2340RK Toxic Gas Transmitter
Description
This section describes the components of the toxic gas transmitter. The toxic gas transmitter is
a 4 - 20 mA type detector head. It consists of the toxic detector, amplifier, and junction box.
Figure 1: Toxic Transmitter Component Location
SPAN
SIG/PWR
ZERO
TOXIC OXY S
Amplifier
J-Box
Toxic Detector

65-2340RK Toxic Gas Transmitter • 7
Toxic Detector
The toxic detector consists of the detector housing body, detector housing cap, splashguard,
cap gasket, and the plug-in sensor.
Figure 2: Toxic Detector Component Location
Detector Housing Body
The detector housing body protects the electronic components within the housing. Use the
mounting threads at the top of the housing to screw the toxic detector into the 3/4 NPT hub on
the bottom of the junction box. Two wires extend from the top of the detector housing body.
Use these wires to connect the toxic detector to the amplifier. One of the wires is black and
one of the wires is color coded depending on the detector type. See Figure 5 on page 12 for the
color code assignments.
The housing body includes a 12 position connector at the bottom of the housing body. The
plug-in sensor mates to this connector. A pre-amplifier located between the connector and the
two interconnect wires conditions the sensor’s signal before the signal reaches the controller.
Each plug-in sensor type (Cl2 for example) requires a different pre-amplifier, so there is a
different detector housing body for each gas type.
Housing Cap, Cap Gasket, & Splashguard
The housing cap screws onto the detector housing. It retains the plug-in sensor and protects it
from damage. A removable splashguard is screwed onto the detector cap to protect the sensor
from impact damage, direct water spray, and splashing. Unscrew the detector cap to access the
sensor for maintenance or replacement. A cap gasket seals the interface between the housing
and cap.
Plug-In Sensor
The plug-in sensor is secured in the detector assembly by the housing cap. There is a different
sensor for each target gas. Through a series of chemical and electrical reactions, the sensor
Splash Guard
(removable)
Sensor
(different for each detector type)
Detector Housing
Cap
Cap Gasket
Detector Housing Body
(different for each detector type)

8 • 65-2340RK Toxic Gas Transmitter
produces an electrical output that corresponds to the detection range of the sensor.
Amplifier
The amplifier converts the electrical output from the detector to a 4 to 20 mA signal that
corresponds to the detection range and transmits the signal to a gas monitoring controller. A
foam gasket that orients the amplifier and keeps it from rotating is installed on the bottom of
the amplifier. The amplifier includes the detector terminal strip, controller terminal strip, zero
pot, span pot, and test points (see Figure 3).
Figure 3: Amplifier Component Location
Controller Terminal Strip
The controller terminal strip is a two position plug-in style terminal strip located at the top
edge of the amplifier. Use the controller terminal strip to wire the transmitter to a controller.
Detector Terminal Strip
The detector terminal strip is a four position plug-in style terminal strip located below the
controller terminal strip. Two of the positions are for use with an oxygen sensor and are not
used in the toxic gas transmitter. Use the two detector terminal strip positions that are labelled
“TOXIC” to connect the detector to the amplifier.
NOTE: The detector is factory-wired to the detector terminal strip. See “Wiring the Toxic Gas
Transmitter to a Controller” on page 11 for all wiring procedures related to the
transmitter.
Zero Pot
The zero pot is located in the upper left corner of the amplifier (see Figure 3). Use a small flat
blade screwdriver to turn the zero pot’s adjustment screw and adjust the amplifier’s zero (fresh
air) output during the start-up and calibration procedures. Turn the adjustment screw
clockwise to increase the zero output and counterclockwise to decrease the zero output.
Controller Terminal Strip
Detector Terminal Strip
Mounting Screw
SIG/PWR
SPAN
Span Pot
Factory Adjust Pot
Zero Pot
ZERO
Red + Test Point
Black - Test Point
S
TOXIC OXY

65-2340RK Toxic Gas Transmitter • 9
Span Pot
The span pot is located to the right of the zero pot (see Figure 3). Use a small flat blade
screwdriver to turn the span pot’s adjustment screw and adjust the amplifier’s gas response
output during the calibration procedure. Turn the adjustment screw clockwise to increase the
span output and counterclockwise to decrease the span output.
CAUTION:The amplifier includes an additional potentiometer. It is factory-set. Do not adjust
it.
Test Points
The test points are on the left side of the amplifier (see Figure 3). The test points produce a
100 mV to 500 mV output that corresponds to the transmitter’s 4 to 20 mA output. Use the test
points and a voltmeter to measure the amplifier’s output during the start-up and calibration
procedures. The black test point in the lower left corner is the negative (-) test point and the
red test point below the zero pot is the positive (+) test point.
Junction Box
Use the junction box to install the transmitter at a mounting site that is remote from the
controller. The junction box protects the amplifier and wiring connections made to the
amplifier. Use the top 3/4 NPT conduit hub to connect wiring from the amplifier to the
controller. Use the cover on the front of the junction box to access the interior of the junction
box. The detector and amplifier are factory installed in the junction box. Three spacers
installed on the back of the junction box control the distance of the junction box from a
mounting surface and ensure that there is enough room to install a calibration cup on the
detector during calibration.
Installation
This section describes procedures to mount the toxic gas transmitter in the monitoring
environment and wire the transmitter to a controller.
Mounting the Toxic Gas Transmitter
1. Select a mounting site that is representative of the monitoring environment. Consider the
following when you select the mounting site.
• Select a site where the transmitter is not likely to be bumped or disturbed. Make sure
there is sufficient room to perform start-up, maintenance, and calibration procedures.
• Select a site where the target gas is likely to be found first.

10 • 65-2340RK Toxic Gas Transmitter
Figure 4: Mounting the Toxic Gas Transmitter
2. At the monitoring site you select, hang or mount the junction box with the detector facing
down (see Figure 4).
3.65 Rubber
Spacer, 3X
3/4 NPT
Conduit Hub 0.38
.75
2.70
Junction
Box
9.60 Max
Toxic
Detector

65-2340RK Toxic Gas Transmitter • 11
Wiring the Toxic Gas Transmitter to a Controller
WARNING: Always verify that power to the controller is off before you make wiring
connections.
1. Turn off the controller.
2. Turn off power to the controller.
3. Remove the junction box cover.
4. The detector leads are factory wired. Verify that the detector leads are wired to the
amplifier’s detector terminal strip as shown in Figure 5.
5. To gain access to a plug-in terminal strip for wiring, pull it out of its socket by grasping the
terminal strip and pulling. The detector strip is keyed so that the controller and detector
terminal strips cannot be reversed inadvertently.
6. Guide a two-conductor, shielded cable or two wires in conduit through the top conduit hub
of the junction box.
7. Pull out the controller terminal strip, and connect the two wires to the terminal strip as
follows (see Figure 5).
• Connect the positive wire to the SIG/PWR “+” terminal.
• Connect the signal wire to the SIG/PWR “S” terminal.
CAUTION:If shielded cable is used, leave the cable shield’s drain wire disconnected and
insulated at the transmitter. You will connect the opposite end of the cable’s drain
wire to the controller’s chassis (earth) ground.
8. Reinstall the controller terminal strip into its socket.
9. Secure the junction box cover to the junction box.
10. Route the cable or wires leading from the toxic gas transmitter through one of the conduit
hubs at the controller housing.
CAUTION:Do not route power and transmitter wiring through the same controller conduit
hub. The power cable may disrupt the transmission of the transmitter signal to the
controller.
11. Connect the wires to the applicable detector/transmitter terminal strip at the controller as
shown in Figure 5.

12 • 65-2340RK Toxic Gas Transmitter
Figure 5: Wiring the Toxic Gas Transmitter to a Controller
12. If shielded cable is used, connect the cable’s drain wire to an available chassis (earth)
ground at the controller. RKI controllers typically have a ground stud that can be used to
ground the cable’s drain wire.
Gas TypeTable
Gas Type + Wire
0-10ppmCl2
0-3ppmCl2
S
SIG /P W RTO XIC OX Y ZERO
Controller Detector/Transmitter
Terminals, Typical Designations
Controller Housing
SPAN
Cable Shield
J-Box
+
S
Black
AsH3 brown
CL2 yellow
CL-10 yellow
HCN white
NH3 red
PH3 green
SO2 blue
(+) See Table
Toxic Detector

65-2340RK Toxic Gas Transmitter • 13
Start Up
This section describes procedures to start up the toxic gas transmitter and place the transmitter
into normal operation.
Introducing Incoming Power
1. Complete the installation procedures described earlier in this manual.
2. Verify that the power wiring to the controller is correct and secure. Refer to the controller
operator’s manual.
3. Turn on power to the controller.
4. Turn on the controller.
5. Verify that the controller is on and operating properly. Refer to the controller operator’s
manual.
CAUTION:Allow the transmitter to warm up for 5 minutes before you continue with the next
section, “Setting the Zero Signal”.
Setting the Zero Signal
CAUTION:If you suspect the presence of toxic gas in the monitoring environment, use the
calibration kit and the zero air calibration cylinder to introduce “fresh air” to the
detector and verify an accurate zero setting. See “Calibration” on page 18 for
instructions to apply zero air when setting the zero signal.
1. Verify that the transmitter is in a fresh air environment (environment known to be free of
toxic gas).
2. Unscrew and remove the junction box cover from the junction box.
3. Set a voltmeter to measure in the millivolt (mV) range.
4. Plug the voltmeter leads into the test points on the amplifier. Plug the positive lead into the
red + test point; plug the negative lead into the black - test point.
5. Verify a voltmeter reading of 100 mV (±2 mV).
6. If necessary, use a small flat-blade screwdriver to adjust the zero pot until the voltmeter
reading is 100 mV (±2 mV).
7. Remove the voltmeter leads from the test points.
8. Secure the junction box cover to the junction box.

14 • 65-2340RK Toxic Gas Transmitter
Maintenance
This section describes maintenance procedures. It includes preventive maintenance,
troubleshooting, and component replacement procedures.
Preventive Maintenance
This section describes a preventive maintenance schedule to ensure the optimum performance
of the toxic gas transmitter. It includes daily and quarterly procedures.
Daily
Verify a display reading of 0 ppm at the controller. Investigate significant changes in the
display reading.
Quarterly
Calibrate the toxic gas transmitter as described in “Calibration” on page 18 of this manual.
Troubleshooting
The troubleshooting guide describes symptoms, probable causes, and recommended action for
problems you may encounter with the toxic gas transmitter.
NOTE: This troubleshooting guide describes transmitter problems only. See the controller
operator’s manual for problems you may encounter with the controller.
Table 2: Troubleshooting the Toxic Gas Transmitter
Condition Symptom(s) Probable Causes Recommended Action
Fail
Condition
• Controller indicates
a fail condition.
• The transmitter wiring
is disconnected or
misconnected.
• The plug-in sensor is
not properly plugged
into the socket in the
detector housing body.
• The transmitter’s zero
reading is low enough
to cause a fail
condition.
• The transmitter is
malfunctioning.
1. Verify that the transmitter wiring is
correct and secure.
2. Confirm that the plug-in sensor is
installed properly.
3. Perform a zero (fresh air) adjustment.
A full calibration is recommended.
4. If the fail condition continues,
replace the plug-in sensor as
described later in this section.
5. If the fail condition continues,
contact RKI for further instruction.

65-2340RK Toxic Gas Transmitter • 15
Replacing Components of the Toxic Gas Transmitter
This section includes a procedure to replace the plug-in toxic sensor, a procedure to replace
the entire toxic detector assembly, and one to replace the amplifier. In most cases, it is not
necessary to replace the entire detector assembly.
Replacing The Plug-in Toxic Sensor
CAUTION:The plug-in sensor contains electrolyte which is a dilute acid. Do not disassemble
the sensor when replacing it with a new one. If sensor electrolyte comes in contact
with your skin, wash affected area thoroughly with soap and water.
1. Turn off the controller.
2. Turn off or unplug power to the controller.
3. Unscrew the detector housing cap with the splashguard from the detector housing body.
Make sure not to lose the cap gasket.
4. Unplug and remove the toxic sensor.
5. Remove the black plug from the top of the replacement sensor.
Slow or No
Response/
Difficult or
Unable to
Calibrate
• Unable to accurately
set the zero or
response reading
during calibration.
• Transmitter requires
frequent calibration.
Note: Under
“normal”
circumstances, the
transmitter requires
calibration once every
3 months.
Some applications
may require a more
frequent calibration
schedule.
• The calibration
cylinder is low, out-
dated, or defective.
• The incorrect
calibration cup or
regulator is being
used.
• The plug-in sensor
face is blocked with
dirt or some other
particulate
contamination.
• The calibration gas is
not an appropriate
concentration.
• The transmitter is
malfunctioning.
1. Verify that the calibration cylinder
contains an adequate supply of a
fresh test sample.
2. Confirm that you are using the
correct calibration cup and regulator
for your detector type. See Table 3 on
page 18 for a list of the required
calibration cups and regulators.
3. Check the plug-in sensor face and
remove any particulate contamination
if necessary.
4. Verify that the calibration gas
concentration is appropriate for the
transmitter. The concentration should
be in the detection range, preferably
about half of the detection range.
5. If the calibration/response difficulties
continue, replace the plug-in sensor
as described later in this section.
6. If the calibration/response difficulties
continue, contact RKI for further
instruction.
Table 2: Troubleshooting the Toxic Gas Transmitter (cont.)
Condition Symptom(s) Probable Causes Recommended Action

16 • 65-2340RK Toxic Gas Transmitter
6. Carefully plug the replacement sensor into the connector that is located in the detector
housing body.
WARNING: You must replace the plug-in sensor with the same type of sensor that is
installed. A detector cannot be converted from one type of detector to another
by using a different plug-in sensor. For example, if you are replacing a Cl2
sensor, you must replace it with a Cl2sensor.
7. Make sure the cap gasket is in place and screw the detector housing cap with the
splashguard back onto the detector housing body.
8. Turn on power to the controller.
9. Turn on the controller and place into normal operation.
CAUTION:Allow the replacement sensor to warm up for 5 minutes before you continue with
the next step.
10. Calibrate the detector as described in “Calibration” on page 18.
Replacing the Toxic Detector
NOTE: In most cases, it is only necessary to replace the plug-in sensor.
1. Turn off the controller.
2. Turn off or unplug power to the controller.
3. Remove the junction box cover.
4. Remove the detector terminal strip from its socket.
5. Disconnect the detector leads from the detector terminal strip. Note the position of the
color-coded leads as you remove them.
6. Unscrew the detector from the junction box conduit hub.
7. Guide the detector leads of the replacement detector through the bottom conduit hub of the
junction box, then screw the mounting threads of the detector into the conduit hub. If
necessary for environmental conditions, apply thread sealant or Teflon tape to the hub and/
or detector threads to seal them.
8. Connect the detector leads to the appropriate detector terminal strip terminals. Connect the
black wire to the terminal labelled TOXIC - and the color coded wire to the terminal
labelled TOXIC +. See Figure 5 on page 12 for the detector wiring connections to the
amplifier and the detector wire color coding.
9. Reinstall the junction box cover.
10. Turn on or plug in power to the controller.
11. Turn on the controller and place it into normal operation.

65-2340RK Toxic Gas Transmitter • 17
CAUTION: Allow the replacement detector to warm up for 5 minutes before you continue
with the next step.
12. Calibrate the replacement detector as described in “Calibration” on page 18.
Replacing the Amplifier
1. Turn off the controller.
2. Turn off or unplug power to the controller.
3. Remove the junction box cover.
4. Unplug the detector terminal strip and controller terminal strip from their sockets. You
may leave the wires connected to the terminal strips.
5. Unscrew and remove the screw with the flat and lock washers that secures the amplifier to
the junction box.
6. Remove the old amplifier.
7. Install the new amplifier into the junction box with the screw, lock washer, and flat washer
you removed in Step 5 above. A foam gasket that orients the amplifier and keeps it from
rotating is installed on the bottom of the amplifier. Make sure the amplifier is seated flat in
the junction box.
8. Install the detector and controller terminal strips into their sockets on the new amplifier as
shown in Figure 5 on page 12. If controller leads or detector leads were removed during
this procedure, refer to Figure 5 on page 12 for the detector and amplifier connections.
NOTE: When a transmitter is first powered up with a new amplifier, the initial output may be
either high or below zero depending on the setting of the zero pot. Be sure to make
arrangements so that this does not cause unwanted alarms.
9. Turn on power to the controller.
10. Turn on the controller and place it into normal operation.
11. Allow the transmitter to warm-up for 5 minutes.
12. Calibrate the transmitter as described in “Calibration” on page 18 of this manual.
Calibration Frequency
Although there is no particular calibration frequency that is correct for all applications, a
calibration frequency of every 3 months is adequate for most toxic gas transmitter
applications. Unless experience in a particular application dictates otherwise, RKI
Instruments, Inc. recommends a calibration frequency of every 3 months for the toxic gas
transmitter.
If an application is not very demanding, for example detection in a clean, temperature
controlled environment where toxic gas is not normally present, and calibration adjustments

18 • 65-2340RK Toxic Gas Transmitter
are minimal at calibration, then a calibration frequency of every 6 months is adequate.
If an application is very demanding, for example if the environment is not well controlled or if
toxic gas is often present, then more frequent calibration than every 3 months may be
necessary.
Calibration
This section describes how to calibrate the toxic gas transmitter. It includes procedures to
prepare for calibration, set the zero (fresh air) reading, set the span (response) reading, and
return to normal operation. It describes calibration using a calibration kit that includes a
calibration cup, calibration gas, sample tubing, and a fixed flow regulator with an on/off knob.
The required sample flow rate and calibration cup depend on the transmitter being calibrated.
Table 3 below lists the required calibration cups and regulators for the various toxic gas
transmitters.
WARNING: RKI Instruments, Inc. recommends that you dedicate a regulator for use with
chlorine (Cl2) gas and that you do not use that dedicated regulator for any
other gases, particularly hydrogen sulfide (H2S).
WARNING: Not using the recommended calibration cup, sample flowrate, and specified
flow direction (for 81-1138RK calibration cup only) will result in an
inaccurate calibration. Make sure to use the calibration cup and sample flow
rate listed in Table 3 for your target gas when performing a calibration. Also
make sure to connect the sample tubing to the calibration cup port that results
in the specified flow direction for the 81-1138RK calibration cup.
Table 3: Required Calibration Cups and Flow Rates
Transmitter Type Required
Calibration Cup
Required Regulator/
Flowrate for Calibration
Gas
Flow Direction
Specified on
Calibration Cup
Arsine (AsH3) 81-1138RK 81-1051RK, 0.5 LPM (liters
per minute)
Yes
Chlorine (Cl2), 0 - 3.00 ppm
and 0 - 10.0 ppm
81-1138RK-CL2 81-1051RK, 0.5 LPM No
Hydrogen Cyanide (HCN) 81-1138RK-HCN 81-1051RK, 0.5 LPM Yes
Ammonia (NH3) 81-1138RK-NH3 81-1051RK-25, 0.25 LPM No
Phosphine (PH3) 81-1138RK 81-1051RK, 0.5 LPM Yes
Sulphur Dioxide (SO2) 81-1138RK 81-1051RK, 0.5 LPM Yes

65-2340RK Toxic Gas Transmitter • 19
Preparing for Calibration
1. Place the controller into its calibration mode or disable external alarms.
2. Unscrew and remove the junction box cover.
3. Set a voltmeter to measure in the millivolt (mV) range.
4. Plug the voltmeter leads into the test points on the amplifier. Plug the positive lead into the
red + test point; plug the negative lead into the black - test point.
5. Use the following formula to determine the correct test points output for the calibrating
sample.
Output (mV) = (calibrating sample/fullscale) X 400 + 100
For example, with a calibrating sample of .50 ppm and a fullscale setting of 1.00, the
correct output is 300 mV.
300(mV) = (.50/1.00) X 400 +100
NOTE: Calibrating the toxic gas transmitter may cause alarms. Be sure to put the controller
into its calibration program or disable external alarms before continuing.
6. Unscrew the splashguard from the detector housing cap. Make sure the cap remains
securely screwed onto the housing body.
7. Push the calibration cup onto the plug-in sensor that sticks through the housing cap. The
calibration cup seals to the sensor with an O-ring.
Setting the Zero (Fresh Air) Reading
NOTE: If you can verify that the toxic gas transmitter is in a fresh air environment, you do not
need to apply zero air to the detector before adjusting the fresh air reading.
1. Screw the regulator into the zero air calibration cylinder.
2. Use the sample tubing to connect the regulator to the calibration cup. Make sure to
connect the tube to the inlet side of the calibration cup if using the 81-1138RK calibration
cup which is marked on the outside bottom to show the required flow direction through
the cup.
3. Turn the regulator knob counterclockwise to open the regulator.
4. Allow the gas to flow for two minutes and verify a reading of 100 mV (±2 mV). If
necessary, use the zero pot on the amplifier to adjust the reading to 100 mV (±2 mV).
5. Turn the regulator knob clockwise to close the regulator.
6. Unscrew the regulator from the zero air calibration cylinder. Leave the sample tubing
connected to the regulator and the calibration cup.

20 • 65-2340RK Toxic Gas Transmitter
NOTE: Depending on the size of your zero air cylinder, it is possible that you will have a
different regulator for the zero air cylinder and toxic gas cylinder. If necessary to fit
the calibration toxic gas cylinder, change the regulator.
Setting the Span (Response) Reading
1. Verify that the calibration gas is representative of the transmitter’s target gas.
2. For toxic gas cylinders (like Cl2, NH3, etc.), it is important to vent the regulator while
installing it onto the cylinder. Venting the regulator during installation helps prevent air
from getting into the cylinder and degrading the gas. Open the regulator by turning the
knob counterclockwise and then install it onto the cylinder.
3. Allow the calibration gas to flow for two minutes and verify that the reading matches the
response reading (±2 mV) you determined earlier. If necessary, use the span pot on the
amplifier to adjust the reading to match the correct response reading.
4. Turn the regulator knob clockwise to close the regulator.
5. Unscrew the regulator from the calibration cylinder and gently pull the calibration cup off
of the plug-in sensor.
Returning to Normal Operation
1. Remove the voltmeter leads from the amplifier test points.
2. Gently pull the calibration cup off of the plug-in sensor
NOTE: For convenience, leave the regulator and calibration cup connected by the sample
tubing.
3. Screw the splashguard firmly back onto the housing cap.
4. Secure the junction box cover to the junction box.
5. When the controller display reading falls below the alarm setpoints, return the controller
to normal operation.
NOTE: If you do not allow the gas reading to decrease below the alarm points, then unwanted
alarms may occur.
6. Verify that the controller display reading decreases and stabilizes at 0 ppm.
7. Store the components of the calibration kit in a safe and convenient place.