Thermo Scientific Nicolet iS10 User manual

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269-213200, Rev B

Contents
Getting Started.....................................................................................1
What’s in the box? ...........................................................................2
What are the features?......................................................................3
What’s on the rear panel? ............................................................7
Collecting a Spectrum ..........................................................................8
How do I collect a spectrum?...........................................................8
Taking the Next Steps........................................................................16
What options are available?............................................................16
How do I check performance? .......................................................19
How do I maintain my spectrometer? ............................................20
Where is the documentation?.........................................................21
What if I have a question?..............................................................22
What about the warranty?..............................................................22

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Thermo Fisher Scientific Getting Started with an iS10 Spectrometer 1
Getting Started
Congratulations on your purchase! The Thermo Scientific Nicolet™
iS™10 spectrometer is designed with integrated validation features, a
powerful software suite, and many other features that make it easy for
you to collect data and get the answers you need.
This manual explains the features of your spectrometer and takes you
through a basic sample collection. The topics that are covered include:
•The contents of the shipping box.
•An introduction to the instrument.
•The procedure for collecting a spectrum.
•System options.
•Maintenance and performance checks.
•Important documents.
•Contact information.
•The instrument warranty.

2 Getting Started with an iS10 Spectrometer Thermo Fisher Scientific
What’s
in the box?
Your spectrometer will be unpacked and installed by one of our service
representatives, but if necessary, you can unpack the shipping box
before the installation. The following drawing shows the typical
contents of the box.
Notice To avoid permanent damage to the optical components in your
spectrometer, do not open anything, especially the plastic bag that
protects the spectrometer, until the entire shipping box has come to
room temperature. Please see “What about the warranty?’ in the
“Taking the Next Steps” chapter for more information. S
Stop
Sample
OK/Enter
Background
Macro
Accessory
User's manual
and Safety guide
Smart
Accessory
clip
Purge
connector
USB 2.0
cable
Desiccant
canisters (2)
Power
supply
Spectrometer

Thermo Fisher Scientific Getting Started with an iS10 Spectrometer 3
What are
the features?
The following drawing shows the main features of your spectrometer.
After the drawing, you will find descriptions of these features. For
additional information, please see the spectrometer help available
through the Help menu in the OMNIC™ software.
Stop
Sample
OK/Enter
Background
Macro
Operations
panel
Sample compartment area
Protective
windows
External beam port
(on right side)
Humidity indicator
Auxiliary signals port
Source
Desiccant
canisters cover
1
2
3
4
5
6
7
8
➀Your spectrometer is protected from excessive humidity by two
desiccant canisters located in a compartment below the desiccant
canisters cover. For information about regenerating and replacing
these canisters, choose the spectrometer help from the Help menu
in OMNIC, and then refer to the “Replacing the desiccant” and
“Regenerating the desiccant” topics.

4 Getting Started with an iS10 Spectrometer Thermo Fisher Scientific
➁The humidity indicator monitors the level of humidity inside the
spectrometer. The status is indicated by the color of the indicator:
BLUE
Good Change desiccant Call service
LIGHT BLUE PINK
➂The external beam port on the right side of the spectrometer allows
the spectrometer to be connected to an FT-IR microscope or a
Nicolet iZ10 module.
➃The operations panel has buttons and indicators that allow you to
perform many operations without needing to use the computer. For
information about advanced operations using the Macro button,
please see OMNIC software help (available through the Help menu
in OMNIC). The other buttons are explained in the “How Do I
Collect a Spectrum” chapter and in the spectrometer help system
available through the Help menu in OMNIC.
➄You can use the sample compartment with many different
accessories, such as a:
Stop
Sample
OK/Enter
Background
Macro
Stop
Sample
OK/Enter
Background
Macro
Stop
Sample
OK/Enter
Background
Macro
TGA
INTERFACE
Smart OMNI-Transmission
Accessory
Other Smart Accessories Large baseplate-
mounted accessories

Thermo Fisher Scientific Getting Started with an iS10 Spectrometer 5
¾The Smart OMNI-Transmission Accessory:
Use the transmission accessory to collect data from samples held
in any of the typical transmission cells or holders, including:
•Standard liquid cells
•Film holders
•KBr pellet holders
•ST-IR cards
•Mineral oil mulls
•Gas cells up to 10 cm
¾Other Smart Accessories™:
A wide range of Smart Accessories can be used, including:
•Attenuated total reflectance (ATR)
•Diffuse reflectance (DRIFTS)
•Specular reflectance
•Temperature controlled accessories
•Near-Infrared Integrating Sphere
Note The included tray provides storage below the accessory and protects the
cover of the instrument. S
¾Large baseplate-mounted accessories:
An optional sample compartment extension allows you to
install specialized accessories, including:
•Thermal gravimetric analysis (TGA) interface
•Micro-Well Plate accessory (reflection or transmission)
•Multi-pass (long pathlength) gas cells
•Other accessories

6 Getting Started with an iS10 Spectrometer Thermo Fisher Scientific
➅Your spectrometer is protected from environmental humidity and
other chemical vapors by two windows. These windows isolate the
optics in the spectrometer and are coated to improve their resistance
to water vapor. You still, however, need to be careful when cleaning
your spectrometer to avoid damaging the optics or the windows.
For more information, please refer to the “Cleaning your
spectrometer” topic in the spectrometer help (available through the
Help menu in OMNIC).
➆The auxiliary signals port is used for accessories with detectors or
power needs, such as the Micro Well Plate accessory and the near-
IR integrating sphere.
➇You can replace the source in your instrument without removing
the cover. Two sources are available: one for the mid-IR range
(EverGlo™) and another for the near-IR range (tungsten-halogen).
(For information about installing a new source, open the
spectrometer help from the Help menu in OMNIC. Choose the
“Source” topic from the “Replacing existing hardware” book in the
“Service” book of the spectrometer help system.)