Thermo Scientific Savant SpeedVac SPD140DDA Owner's manual

Installation and Operation
80302134 • Revision A • July 2018
SpeedVac™ SPD140DDA
Vacuum Concentrator

IMPORTANT: Read this instruction manual. Failure to follow the instructions in this manual can result in
damage to the unit, injury to operating personnel, and poor equipment performance.
CAUTION: All internal adjustments and maintenance must be performed by qualified service personnel.
DISCLAIMER: Thermo Fisher Scientific Inc. does not accept any responsibility for any damage caused to its
products by unauthorized personnel.
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the
product operation. This document is copyright protected and any reproduction of the whole or any part of this
document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.
The contents of this document are subject to change without notice. All technical information in this document
is for reference purposes only. System configurations and specifications in this document supersede all
previous information received by the purchaser.
© 2018 Thermo Fisher Scientific Inc. All rights reserved.

Contents
Introduction ................................................................. 1
Safety Precautions....................................................... 2
Operating Standards.................................................... 3
Product Specifications ............................................. 3
Environmental Conditions......................................... 3
Installation.................................................................... 4
Contents .................................................................. 4
Installation of SPD140DDA....................................... 4
Operation..................................................................... 6
Description Of Control Panel .................................... 6
Manual Run.............................................................. 8
Auto Run.................................................................. 9
Drying Rate .............................................................. 9
Preset Program Settings .......................................... 9
Exporting Live Run Data........................................... 10
HyperTerminal Configuration .................................... 10
Lid Stay Mechanism................................................. 11
Other Topics ............................................................ 11
Rotors...................................................................... 13
Accessories ............................................................. 13
SUMAX SPD Maintenance ....................................... 14
Appendix 1 .................................................................. 15
Additional SPD140DDA System Setup ..................... 15

Appendix 2 .................................................................. 17
Additional SPD140DDA System Setup for
DMSO Applications ................................................. 17
Warranty ...................................................................... 18

SpeedVac™ SPD140DDA Introduction | 1
Introduction
Thermo Scientific Savant SpeedVac™ SPD140DDA vacuum
concentrator offers fast, reliable processing of samples. It
effectively removes a broad range of aggressive and volatile
solvents to concentrate or dry solutes, analytes and residues
while providing complete sample recovery.
The combination of vacuum, applied to the sample chamber
from an external source, and centrifugal action promotes
solvent evaporation without sample loss due to foaming or
bumping. The evaporation process is accelerated with the
addition of chamber heat to counteract the extreme
evaporative cooling of the samples. The concentration
process is completed with the addition of a vapor
condensation trap available separately for virtually 100%
solvent recovery. This results in a thorough evaporation
process in a safe environment for both the sample and the
user. The unit features an advanced front panel with dual
timer for automatic or manual control of run conditions, it also
features preset and user defined programs which enable user
to retrieve and store application protocols for future use.
The compact, industrial strength SPD140DDA features:
• Ultimate chemical resistance to aggressive solvents with
the following provisions:
- Rugged stainless steel magnetic drive lubricated with
acid-resistant grease
- Components made of Teflon®and Teflon®coated
materials used exclusively in the vapor path
- Dual valve manifold positioned to reduce solvent
vapor exposure
- Dedicated bleed port added to assure unidirectional
vapor flow and to purge bearings with fresh air
• Faster evaporation rate with the following enhancements:
- Built-in chamber radiant lamps positioned for optimal
evaporation temperature of samples
- Heated glass cover adds radiant heat to samples
and prevents condensation of DMSO on cover
• Microprocessor control of run and heat times offer fully
unattended, automatic operation
• Built-in digital vacuum gauge allows continuous
monitoring of process
• 4 preset programs pre-loaded with default application-
based run parameters
• 8 user-defined programs for custom application-based
run parameters that enables user to retrieve and store
protocols for future use.

2 | Safety Precautions SpeedVac™ SPD140DDA
Safety Precautions
In this manual, the following symbols and conventions are
used:
Below are important safety precautions that apply to this
product:
This symbol when used alone indicates
important operating instructions which reduce
the risk of injury or poor performance of the unit.
CAUTION: This symbol, in the context of a
CAUTION, indicates a potentially hazardous
situation which if not avoided could result in
minor to moderate injury or damage to the
equipment.
WARNING: This symbol, in the context of a
WARNING, indicates potentially hazardous
situations which, if not avoided, could result in
serious injury or death.
This symbol indicates situations where
dangerous voltages exist and potential for
electrical shock is present.
The snowflake symbol indicates extreme low
temperatures and high risk of frostbite. Do not
touch bare metal or samples with unprotected
body parts.
This symbol indicates possible pinch points
which may cause personal injury.
This symbol indicates a need to use gloves
during the indicated procedures. If performing
decontamination procedures, use chemically
resistant gloves.
Before installing, using or maintaining this
product, please be sure to read the manual and
product warning labels carefully. Failure to follow
these instructions may cause the product to
malfunction, which could result in injury or
damage.
This symbol represents protective conductor
terminal.
WARNING: Disconnect the unit from all power
sources before cleaning, troubleshooting, or
performing other maintenance on the product or
its controls.
WARNING: Do not use this device in
radioactive, highly reactive or explosive
atmosphere.
Do not use this device to process any explosive,
radioactive, highly reactive or explosive
atmosphere creating substances.

SpeedVac™ SPD140DDA Operating Standards | 3
Operating Standards
Product Specifications
*Dependent upon ambient temperature, line voltage fluctuation, and load capacity.
Environmental Conditions
Indoor use only, in the absence of hoarfrost, dew, percolating water, rain and solar radiation.
Main supply voltage fluctuations not to exceed ±10% of the nominal voltage.
Transient overvoltages per Installation Categories II.
Operative Power* 115 VAC; 60 Hz; 6 amps
230 VAC; 50 Hz; 3 amps
Vacuum Chamber TEFLON®coated, chemical resistant aluminum casting, includes two built-in radiant
lamps
Cover Heated cover - includes a safety interlock
Induction Motor Maintenance free
Bearings Acid resistant TEFLON®bearings
Chamber temperature 35°C to 80°C, 5°C increments
Vacuum Level Control 20 to 0.1 Torr in 0.1 increments
Vacuum Ramp Setting 1 to 5
Weight 62 lbs
28 kg
Dimensions (W x D x H) 14 in x 18 in x 14 in
36 cm x 46 cm x 36 cm
Fuse 6 A, 250 VAC, Time-lag
3 A, 250 VAC, Time-lag
Maximum altitude 2000 meters above mean sea level
Ambient temperature range 17°C to 32°C
Humidity 20% to 80% non-condensing
Pollution degree 2

4 | Installation SpeedVac™ SPD140DDA
Installation
Contents
Unpacking. Open the shipping cartons. Carefully remove the
instrument and accessories. Lift and carry with two
people, holding securely underneath with both hands.
Use proper lifting technique (lift with the legs, not the
back) to avoid personal injury. Compare the contents with
the packing list. If there is a discrepancy, call Thermo
Scientific technical service.
Inspection. Inspect the unit and accessories for damage that
may have occurred during shipment. Should there be any
damage, report it to the carrier and contact Thermo Scientific
immediately. Make sure the carrier inspects the damage and
leaves an inspection report. Register any claims for shipping
damage against the carrier or his agent. Save the shipping
carton in the event a return is necessary. Call Thermo
Scientific technical service for further assistance.
Site preparation. The SPD140DDA requires a stable surface
that is clean, dry, level, and within 4 feet (1.2 meters) of a
compatible electrical outlet. Place the unit in a convenient
location with access to a vacuum source and a vapor trap1.
The SPD140DDA units configured for 115 VAC, 60 Hz,
should be plugged into a circuit rated for at least 6 amps. The
SPD140DDA units configured for 230 VAC, 50 Hz, should be
plugged into a circuit rated for at least 3 amps.
Note: Do not use any detachable power cord that is not
adequately rated for the unit.
Installation of SPD140DDA
Figure 1. Front View of System
For combinatorial chemistry application, refer Ta bl e 2 for
recommended DDA components. Call Thermo Scientific for
the complete line of vacuum pumps and refrigerated vapor
traps.
Table 1. Contents
Qty. Description
1
Thermo Scientific Savant SpeedVac™
SPD140DDA Concentrator with attached
SUMAX SPD
1Teflon®tubing 1/2” I.D. x 3’ long
1Line Cord
1.To prevent damage to pump due to vapor exposures from sample solvent and to extend pump life, a vapor trap that condenses and traps vapors must be
placed in line between the SpeedVac™ concentrator and vacuum pump. We offer integrated universal vacuum systems (integrated vapor trap with the
vacuum pump) or component vacuum system (vapor trap plus vacuum pump).
CAUTION: Be sure to leave at least 4 inch
clearance on all sides of the unit. Overhead
clearance, equal to 18 inch (46cm), is required for
raising the cover. Verify that the unit is on a
leveled and stable platform. If necessary, move
the unit to a more suitable location.
WARNING: Before connecting the unit to an
electrical outlet, make certain that voltage,
frequency, and amperage match the
requirements indicated on the product label,
name plate of the instrument. Use sockets with a
protective earth conductor and correct mains
cable.
CAUTION: Cold trap should be in line between
the vacuum source and the SPD Unit.
Vacuum
Tubing
SPD140DDA
SpeedVac
Concentrator
UVS850DDA
Universal Vacuum
Source

SpeedVac™ SPD140DDA Installation | 5
Table 2. Recommended DDA components
Vacuum System Solvents To Be
Evaporated
UVS850DDA Universal
Vacuum System
Volatile, low boiling
solvents (MeCl2),
corrosive solvents (TFA)
and mixtures,
Small amounts of high
boiling solvents (DMSO,
DMF)
RVT450 Refrigerated Vapor
Trap + VLP80DDA High
Vacuum Pump
Large volumes of high
boiling solvents (DMSO,
DMF)
RVT5105 Ultra-Low
Temperature Refrigerated
Vapor Trap+ VLP80DDA
High Vacuum Pump
Large volumes of low
boiling solvents (MeCl2)
RVT450 Refrigerated Vapor
Trap + RVT5105 Ultra-Low
Temperature Refrigerated
Vapor Trap+ VLP80DDA
High Vacuum Pump
All types of solvents

6 | Operation SpeedVac™ SPD140DDA
Operation
Connect the power cord to the power inlet on the back of the
unit and plug it into the appropriate outlet. Turn on the main
power switch located on the front of the unit in the lower right
to energize the unit. The safety lid locking mechanism on the
SPD140DDA will automatically disengage. Do not attempt to
open the lid unless the unit is plugged in.
Note: The SPD140DDA Concentrator is an important
component in a complete concentration system that should
also include a refrigerated vapor trap and a vacuum pump
along with other applicable accessories. Please refer to
operating instructions of each component for details on
usage.
Rotor installation. Open the lid of the rotor chamber.
Visually align the pin on the drive shaft with the groove on the
bottom of the rotor. Carefully lower the rotor onto the drive
shaft. Rotate the rotor by hand to ensure alignment of the pin
with the groove. Secure the assembly by screwing the
retaining knob into the drive shaft above the rotor. Tighten it
firmly but not excessively.
Description Of Control Panel
1. Lid locked - Indicates whether or not the lid of the
concentrator is locked, the indicator will be illuminated
when locked.
2. Program navigator - Selects a program in a cyclical
way to prepare the next action that will be applied to it.
Typically, the next action will be a program saving action
but it can also be a program loading action (see next
point).
Pressing this button will only highlight the indicator
associated with the selected program. It will not load its
parameters to the user interface.
This button is only associated with the Program buttons
and not with the Preset buttons.
3. Program buttons - 4 buttons that allow access to 8
user-defined programs that are modifiable (2 programs
per button).
CAUTION: Use appropriate Thermo Fisher
Scientific designed rotors recommended for the
Product.
CAUTION: Load the rotor and close the lid.
Always balance rotor loads. An imbalanced rotor
causes vibration that will damage the system’s
bearings and equipment. Load the rotor
symmetrically. There need not be a tube in each
holder, but the load must be evenly distributed.
When using a rotor with aluminum tube holders,
insert all the tube holders.
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