ThermoFisher Scientific 43iQHL User manual

43iQHL
Instruction Manual
High Level Sulfur Dioxide Analyzer
119015-00 • 1Apr2022

Thermo Scientific 43iQHL Instruction Manual iii
Contents
Introduction........................................................................................................ 1-1
iQ Series Instrument Platform............................................................. 1-1
43iQHL Principle of Operation.......................................................... 1-3
Specifications ...................................................................................... 1-5
Dimensions......................................................................................... 1-7
Installation and Setup...................................................................................... 2-1
Unpacking and Inspection .................................................................. 2-1
Cover Removing and Replacing .......................................................... 2-2
Mounting Options.............................................................................. 2-3
Bench Mount................................................................................... 2-3
Rack Mount..................................................................................... 2-4
Setup Procedure.................................................................................. 2-6
Startup ................................................................................................ 2-8
Operation ............................................................................................................ 3-1
Instrument Display ............................................................................. 3-1
Main Menus and Keypads................................................................ 3-5
Numeric Keypad........................................................................... 3-6
Alphanumeric Keypad................................................................... 3-7
Calibration.......................................................................................... 3-9
Calibrate Background..................................................................... 3-11
Calibrate Span Coefficient ............................................................. 3-12
Zero/Span Schedule ....................................................................... 3-14
Advanced Calibration..................................................................... 3-16
Manual Calibration..................................................................... 3-18
Multipoint Calibration................................................................ 3-23
Calibration History..................................................................... 3-26
Data.................................................................................................. 3-27
View Data Log (Last Hour)............................................................ 3-28
View Data Log (Last 24 Hours) ..................................................... 3-29
View Data Log (User Defined Time) ............................................. 3-30
Advanced Data Setup..................................................................... 3-32
Data Logging Setup .................................................................... 3-33
Select Data Logging Variables ..................................................... 3-34
Streaming Data Setup ................................................................. 3-35
Select Streaming Variables........................................................... 3-36
Settings ............................................................................................. 3-37
Chapter 1
Chapter 2
Chapter 3

Contents
iv 43iQHL Instruction Manual Thermo Scientific
Health Check................................................................................. 3-38
Status and Alarms........................................................................ 3-39
Valve and Pump Resets............................................................... 3-48
Predictive Diagnostics................................................................. 3-54
Maintenance ............................................................................... 3-55
Preventive Maintenance .............................................................. 3-56
Change Part ................................................................................ 3-58
Maintenance History................................................................... 3-59
Service Tips................................................................................. 3-60
File Sharing and Support............................................................. 3-61
iQ360 ......................................................................................... 3-62
Measurement Settings.................................................................... 3-65
Averaging Time........................................................................... 3-67
Range Mode Selection................................................................. 3-69
Range Setting.............................................................................. 3-71
Gas Mode ................................................................................... 3-72
Gas Units.................................................................................... 3-73
Advanced Measurement Settings................................................. 3-74
Communications............................................................................ 3-80
Wired TCP/DHCP .................................................................... 3-82
Serial RS-232/485....................................................................... 3-84
Analog I/O.................................................................................. 3-85
Digital I/O.................................................................................. 3-86
Email Server (SMTP).................................................................. 3-87
Bayern Hessen Settings ............................................................... 3-88
Ethernet Protocol Selection......................................................... 3-89
Instrument Settings........................................................................ 3-90
Display Setup.............................................................................. 3-91
Alarm Setpoints........................................................................... 3-92
Clock .......................................................................................... 3-95
Time Zone.................................................................................. 3-99
Configuration .............................................................................. 3-102
Security Access Levels................................................................... 3-103
Change Security to View Only Access....................................... 3-105
Change Full Access Security Password....................................... 3-106
Change Instrument Password.................................................... 3-108
Reset Instrument Password ....................................................... 3-110
USB Drive ................................................................................... 3-111
Firmware Update Via USB Drive.............................................. 3-112
Download Data To USB Drive................................................. 3-116
Change USB Password.............................................................. 3-119
Reset USB Password.................................................................. 3-121
User Contact Information............................................................ 3-122
Update Bootloader....................................................................... 3-123

Contents
Thermo Scientific 43iQHL Instruction Manual v
Calibration.......................................................................................................... 4-1
Equipment Required........................................................................... 4-1
Zero Air Generation......................................................................... 4-2
Commercial Heatless Air Dryers ................................................... 4-2
Absorbing Column........................................................................ 4-3
SO2Concentration Standard............................................................ 4-3
Calibration Gas Generation ............................................................. 4-3
Cylinder Gas Dilution................................................................... 4-3
External Flow Meter(s) and Controller(s)...................................... 4-4
Commercial Precision Dilution Systems........................................ 4-5
Calibration.......................................................................................... 4-5
Calibration in Dual/Auto Range Mode............................................... 4-7
Zero and Span Check........................................................................ 4-10
Manual Calibration........................................................................... 4-11
Adjust Background......................................................................... 4-12
Adjust Span Coefficient.................................................................. 4-12
Reset Bkg to 0.000 and Span Coef to 1.000................................... 4-13
Multipoint Calibration...................................................................... 4-14
High and Low Multipoint Calibration........................................... 4-16
Calibration Frequency.................................................................... 4-16
Zero/Span Schedule .......................................................................... 4-17
Next Time ..................................................................................... 4-17
Period ............................................................................................ 4-17
Zero/Span/Purge Duration Minutes .............................................. 4-18
Schedule Averaging Time............................................................... 4-18
Background Calibration and Span Calibration............................... 4-18
Zero/Span Ratio............................................................................. 4-18
Maintenance...................................................................................................... 5-1
Safety Precautions ............................................................................... 5-1
Fan Filter Inspection and Cleaning ..................................................... 5-1
Pump Rebuilding................................................................................ 5-2
Leak Test ............................................................................................ 5-5
Lamp Voltage Check........................................................................... 5-6
Lamp Voltage Adjustment .................................................................. 5-6
Troubleshooting ................................................................................................ 6-1
Safety Precautions ............................................................................... 6-1
Troubleshooting Guide....................................................................... 6-1
Servicing............................................................................................................. 7-1
Safety Precautions ............................................................................... 7-1
Firmware Updates............................................................................... 7-3
Chapter 4
Chapter 5
Chapter 6
Chapter 7