ThermoFisher Scientific Thermo Scientific iCE 3000 Series User manual

iCE 3000 Series AA Spectrometers
Pre-Installation Requirements Guide
9499 500 30031 Version 1.6 March 2018

9499 500 30031 Version 1.6 March 2018
iCE 3000 Series AA Spectrometers
Pre-Installation Requirements Guide

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Fisher Scientific Inc.
Release History: Version 1.3 released in September 2011.
Version 1.4 released in July 2014.
Version 1.5 released in November 2014.
Version 1.6 released in March 2018.

Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) i
Contents
Chapter 1 Using this Manual .................................................................1-1
About this Manual ......................................................... 1-1
Typographical Conventions ........................................... 1-2
Signal Words............................................................... 1-2
Safety Symbols ............................................................ 1-2
Viewpoint Orientation................................................ 1-2
Data Input .................................................................. 1-3
Topic Headings........................................................... 1-3
Reference Documentation.............................................. 1-4
Contacting Us................................................................ 1-5
Chapter 2 Introduction ............................................................................2-1
Chapter 3 System Accessories..............................................................3-1
Required Accessories ...................................................... 3-1
Optional Accessories ...................................................... 3-1
Chapter 4 Transportation........................................................................4-1
Package Size ................................................................... 4-2
Short Term Storage........................................................ 4-3
Transit Damage ............................................................. 4-3
Warranty........................................................................ 4-3
Chapter 5 Working Area Requirements...............................................5-1
Introduction................................................................... 5-2
Location......................................................................... 5-3
Environmental Requirements......................................... 5-4
Electrical Requirements.................................................. 5-4
Spectrometer Size........................................................... 5-6
Gas Requirements .......................................................... 5-7
Acetylene..................................................................... 5-8
Air............................................................................... 5-9
Argon and Nitrogen.................................................... 5-9
Nitrous Oxide............................................................. 5-9
Water Temperature Control ........................................ 5-10
Waste Storage .............................................................. 5-11
Spectrometer Fume Extraction..................................... 5-12
Requirements of the Exhaust System......................... 5-12
Sample Fume Extraction .............................................. 5-15

Contents
ii iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) Thermo Scientific
Chapter 6 Communications Interface .................................................. 6-1
Chapter 7 Special Agreements ............................................................. 7-1

Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 1-1
Chapter 1 Using this Manual
Welcome to the Thermo Scientific iCE 3000 Series AA spectrometers!
Contents
•About this Manual on page 1-1
•Typographical Conventions on page 1-2
•Reference Documentation on page 1-4
•Contacting Us on page 1-5
About this Manual
This iCE 3000 Series Pre-Installation Requirements Guide describes the
environment and the resources required at the installation site of the
iCE 3000 Series AA spectrometer and associated equipment. Safety
requirements for the installation are also detailed.
Thermo Scientific iCE 3000 Series AA spectrometers are designed to
operate reliably under carefully controlled environmental conditions.
Operating a system or maintaining it in a condition outside the power
and operating environment specifications described in this guide might
cause failures of many types. The repair of such failures is specifically
excluded from the standard warranty and service contract coverage.
For additional information, request specific pre-installation support
directly through your local Thermo Fisher Scientific office.

Using this Manual
Typographical Conventions
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Typographical Conventions
This section describes typographical conventions that have been
established for Thermo Scientific manuals.
Signal Words
Make sure that you follow the precautionary statements presented in
this manual. The special notices appear different from the main flow of
text:
Safety Symbols
Notices that concern the safety of the personnel who operate the
iCE 3000 Series mass spectrometer appear different from the main flow
of text:
Viewpoint Orientation
The expressions left and right used in this manual always refer to the
viewpoint of a person that is facing the front side of the instrument.
NOTICE
Points out possible material damage, data loss, impaired data quality
and other important information in connection with the instrument.
Tip Highlights helpful information that can make a task easier.
Always be aware of what to do with and the effect of safety
information.
CAUTION
Points out a hazardous situation that can lead to minor or medium
injury if it is not avoided.
WARNING
Points out a hazardous situation that can lead to severe injury or death
if it is not avoided.
DANGER
Points out a hazardous situation that will lead to severe injury or death
if it is not avoided.

Using this Manual
Typographical Conventions
Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 1-3
Data Input
Throughout this manual, the following conventions indicate data input
and output via the computer:
•Messages displayed on the screen are represented by capitalizing the
initial letter of each word and by italicizing each word.
•Input that you enter by keyboard is identified by quotation marks:
single quotes for single characters, double quotes for strings.
•For brevity, expressions such as “choose File > Directories” are used
rather than “pull down the File menu and choose Directories.”
•Any command enclosed in angle brackets < > represents a single
keystroke. For example, “press <F1>” means press the key labeled
F1.
•Any command that requires pressing two or more keys
simultaneously is shown with a plus sign connecting the keys. For
example, “press <Shift> +<F1>” means press and hold the <Shift>
key and then press the <F1> key.
•Any button that you click on the screen is represented in bold face
letters. For example, “click Close.”
Topic Headings
The following headings are used to show the organization of topics
within a chapter:
Chapter 1 Chapter Name
Second Level Topics
Third Level Topics
Fourth Level Topics

Using this Manual
Reference Documentation
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Reference Documentation
In addition to this guide, Thermo Fisher Scientific provides other
documents for the iCE 3000 Series AA spectrometers. Reference
documentation for the iCE 3000 Series spectrometers includes the
following:
•iCE 3000 Series Operating Manual
This manual is provided on the software CD.

Using this Manual
Contacting Us
Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 1-5
Contacting Us
There are several ways to contact Thermo Fisher Scientific. You can use
your smartphone to scan a QR Code, which opens your email
application or browser.
Contact Link / Remarks QR Code
Brochures and Ordering
Information www.thermofisher.com/AAS
Service Contact www.unitylabservices.com
Technical Documentation
SharePoint
❖To get user manuals for your product
1. With the serial number (S/N) of your instrument, request
access on our customer SharePoint as a customer at
www.thermoscientific.com/Technicaldocumentation
2. For the first login, you have to create an account. Follow the
instructions given on screen. Accept the invitation within six
days and log in with your created Microsoft™ password.
3. Download current revisions of user manuals and other
customer-oriented documents for your product. Translations
into other languages may be available there as well.
Customer Feedback ❖To suggest changes to this manual
You are encouraged to report errors or omissions in the text or
index. Send an email message to the Technical Editor at
[e-mail].

Using this Manual
Contacting Us
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Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 2-1
Chapter 2 Introduction
This manual is designed to help ensure that your iCE 3000 Series AA
spectrometer will be installed efficiently and will be able to meet your
requirements quickly and completely.
It will minimize installation time if the services and facilities detailed
here are available before the equipment is delivered.
Properly installed and maintained, your system will provide you with
years of reliable service. Inform your local Thermo Fisher Scientific
organization what aspects of support are most important to you, and a
tailored agreement can be provided to prolong the life of your
instrument. Contact details for your local support office can be found
on www.thermofisher.com.
This guide describes the environment and the resources required at the
installation site of the iCE 3000 Series AA spectrometer and associated
equipment. Safety requirements for the installation are also detailed.
The choice of an operating site for the instrument will be influenced by
local considerations, for example ease of access and availability of
electrical power.
Logical planning of the installation can save both time and money. The
objective of this guide is to provide information that will enable the best
site to be chosen and to highlight the essential requirements.
If further information or advice is required, contact your local Thermo
Fisher Scientific representative. A list of Thermo Fisher Scientific
organizations and agents can be found on www.thermofisher.com.
Installation of the system will include some familiarization training.
However, comprehensive method development and software training
will require additional training that should be ordered separately.
The installation of all services must comply with the appropriate rules
and regulations required by the local authorities responsible for those
services in the workplace at the installation site. An installation
engineer is not responsible for the fitting, or compliance of the
facilities, or services.

Introduction
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Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 3-1
Chapter 3 System Accessories
Required Accessories
•Data Station. See Chapter 6, “Communications Interface”.
Optional Accessories
•Thermo Scientific™ GFS33 Graphite Furnace and Autosampler for
iCE™ 3300 AA spectrometer
•Thermo Scientific™ SOLAAR Validator Package
•Thermo Scientific™ SOLAARSecurity Software
•Thermo Scientific™ ID100 Auto Dilutor
•Thermo Scientific™ VP100 Continuous Flow Vapor Generator
(includes T-Cell and Mercury Cell)
•Thermo Scientific™ EC100 Electrically Heated Cell System
•Thermo Scientific™ STAT (Slotted Tube Atom Trap) Accessory
•Air Compressor KNF N035 (Series N 035 A_.18 Pumps,
Diaphragm Vacuum Pumps and Compressors, KNF Neuberger,
Inc.)
•CETAC™ ASX-520 Autosampler (requires dedicated RS-232 on
Data Station)
•CETAC™ ASX-260 Autosampler (requires dedicated RS-232 on
Data Station)
•Thermo Scientific™ NESLAB ThermoFlex™ recirculating chiller
Request site requirement guides for any purchased accessories.

System Accessories
Optional Accessories
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Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 4-1
Chapter 4 Transportation
Contents
•Package Size on page 4-2
•Short Term Storage on page 4-3
•Transit Damage on page 4-3
•Warranty on page 4-3
The spectrometer is supplied with all compatible accessories that have
been purchased to meet the customer's system requirements. Items may
be shipped in separate packages.
Proposed routes from the customer receiving area to the installation site
must be checked for suitability. The largest pallet size should be used to
calculate clearances.
All items should be transported to the installation site on pallets, in
their original packaging and the right way up. Under no circumstances
may any package be moved without its pallet unless under the direct
control of an authorized Thermo Fisher Scientific field service
engineer.
The boxed spectrometer, the graphite furnace and the power supply
should be moved using a mechanical lift. To distribute the weight, two
people should lift the equipment from the box. To avoid trapping
fingers, take care in doorways, corridors or when lowering.

Transportation
Package Size
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Package Size
The instrument and accessories will be supplied inside especially
designed packaging. Table 4-1 and Table 4-2 list the dimensions and
weights of the packages.
Transportation to some destinations may necessitate additional
packaging (a packing crate, for example). Dimensions and exact
specifications may vary.
Table 4-1. Dimensions and weights of packed spectrometers
Spectrometer Width Depth Height Weight
iCE 3500 1070 mm
(42.2 in)
740 mm
(29.2 in)
760 mm
(30 in)
64 kg
(141 lbs)
iCE 3400 1070 mm
(42.2 in)
740 mm
(29.2 in)
760 mm
(30 in)
60 kg
(132 lbs)
iCE 3300 660 mm
(26 in)
700 mm
(27.6 in)
760 mm
(30 in)
55 kg
(121 lbs)
iCE 3300GF 660 mm
(26 in)
700 mm
(27.6 in)
760 mm
(30 in)
48 kg
(106 lbs)
Table 4-2. Dimensions and weights of packed accessories
Accessory Width Depth Height Weight
Furnace 715 mm
(28.2 in)
550 mm
(21.7 in)
620 mm
(24.5 in)
57 kg
(126 lbs)
Zeeman
Furnace
715 mm
(28.2 in)
550 mm
(21.7 in)
720 mm
(28.4 in)
71 kg
(157 lbs)
Furnace
Autosampler
510 mm
(20.1 in)
420 mm
(16.6 in)
530 mm
(20.9 in)
10 kg
(22.1 lbs)
EC100 720 mm
(28.4 in)
620 mm
(25.5 in)
350 mm
(13.8 in)
20 kg
(44.1 lbs)
VP100 690 mm
(27.2 in)
500 mm
(19.7 in)
400 mm
(15.8 in)
9.5 kg
(21 lbs)

Transportation
Short Term Storage
Thermo Scientific iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6) 4-3
Short Term Storage
To maintain the instrument in serviceable condition and to comply with
the conditions of warranty, ensure that storage of each item is
maintained within the stated parameters detailed in Chapter 5,
“Working Area Requirements.” Make sure that the packages are stored
the correct way up.
When the packages are opened before installation, the contents will be
checked against the packing list(s).
Spectrometers ordered with Validation packages should not be opened
by other people than the trained Thermo Fisher Scientific field service
engineer performing the installation. This is an explicit requirement for
the Installation Qualification of the Validation. Opening the boxes of
the spectrometer or peripherals by an untrained person can make the IQ
process become invalid.
Transit Damage
Before accepting delivery of any equipment, the packages should be
inspected for signs of obvious damage. The nature of the damage should
be noted on the delivery notice and signed by the carrier's
representative.
Within the time stated in the Thermo Fisher Scientific terms and
conditions, an inspection should be performed for concealed damage.
The local Thermo Fisher Scientific organization should be advised of
any damage in writing and, on receipt of specific instructions, the
customer should return the equipment complete and in the original
packing material.
Warranty
The instrument is warranted against defects in material and
workmanship for a period of 12 months from installation, or 15 months
from shipment, whichever comes first. This warranty does not cover
damage sustained as a result of improper storage by the customer before
installation, or resale to a third party.
NOTICE
Do not open the packages without the permission of the Thermo
Fisher Scientific field service engineer.
NOTICE
Warranty is not transferable to a third party without approval by
Thermo Fisher Scientific.

Transportation
Warranty
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