ANTEK 9000 Series Manual

Install/Operation/ServiceManual
9000 Series
Nitrogen/Sulfur
Analyzers
300 Bammel Westfield Road • Houston, Texas 77090 • USA
Telephone: [phone] • [phone] • FAX: [phone]
e-mail: [email protected] • web site: http://www.antekhou.com
ANTEK®INSTRUMENTS L.P.

IMPORTANT
INFORMATION
CONCERNING
YOUR COMPUTER
HARDWARE!
Every computer supplied with our
ANTEK Analyzer carries a warranty
from the original computer manu-
facturer. The terms of the warranty
will vary based on the manufacturer
of the computer and the final
destination of the system. ANTEK
Instruments DOES NOT warrant
the computer systems sold with
its analytical systems.
ANTEK will warrant, under the
provisions of its standard Warranty
and Service Policy the following items:
1. ANTEK 9000 Software
2. ANTEK/NIDAQ communications
printed circuit board
3. Modem (if installed at the factory)
ANTEK does not accept liability
beyond the remedies set forth in
its standard Warranty and Service
Policy or liability for incident, or
consequential damages, including
without limitation, any liability for
products not being available for
use or for lost data or software.
GLOBAL
WARRANTIES
ON HEWLETT-
PACKARD (HP)
COMPUTERS
The HP Computer that is a part
of your 9000 Series Analyzer
is warranted directly by
Hewlett-Packard. The serial
numbers on the CPU and Monitor
are the way these computers
get tracked. When ANTEK sends
you the computer, the ownership
is automatically transferred.
If HP Support is ever necessary,
they will be able to assist you
globally with the Serial Number
on the CPU and Monitor.
For further information, please
consult your Computer Owners
Manual.
Computer Warranty 10/01

InstallationDate: _______________________________
Installed By: __________________________________
AntekRepresentative: ___________________________
SalesOrder#: _________________________________
INSTALLATION/PROBLEM REPORT ANTEK®
Company: ___________________________________
Contact:_____________________________________
Address: ____________________________________
Address: ____________________________________
City:__________________ St: _____ Zip:_________
Country:____________________ Territory:_________
Phone: ________________ Fax: _________________
E-mail: ______________________________________
System Information: Instruments & Accessories
PurchaseDate S/N Model# Install Date
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
Problem(s)
Model: __________________ S/N: ____________________
Part # DescriptionofProblem
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
Model: __________________ S/N: ____________________
Part # DescriptionofProblem
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
Model: __________________ S/N: ____________________
Part # DescriptionofProblem
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
____________________________________________________________________________________________
* Type of Problem: Appearance Broken Electronic Missing Off Spec Wrong
Assembly Electric Leak Mechanical Non-function
Form 254C 10/01
Fax or e-mail complete report to Service Manager
fax: [phone] • e-mail: [email protected]

ThismanualcontainsconfidentialandproprietaryinformationwhichisthepropertyofAntek
Instruments L.P. This manual and all information disclosed herein shall not be used to
manufacture,construct,orfabricatethegoodsdisclosedherein;shallnotbeexploitedorsold;
shall not be copied or otherwise reproduced in whole or in part and shall not be revealed or
disclosed to others or in any manner made public without the express written permission of
AntekInstrumentsL.P.
Copyright©2002,byAntekInstrumentsL.P.,Houston,Texas.
PrintedintheUnitedStatesofAmerica
Allrightsreserved.
Contentsofthispublicationmaynotbereproducedinanyform
withoutpermissionofthecopyrightowner.
2.28.02

CEDeclaration
CE DECLARATION OF
CONFORMITY
Equipment: Nitrogen Specific HPLC Detector
Model #: 8060
Date of Issue: January 1998
Manufacturer: AntekInstrumentsL.P.
300 Bammel Westfield Road
Houston, TX 77090
USA
This equipment complies with the following standards:
EN 55011: Limits and Methods of Measurement of Radio Disturbances Characteristics of
Industrial, Scientific and Medical (ISM) Radio-Frequency Equipment
IEC 801-2; IEC 1000-4-2; Cenelec 60801-2:
Electromagnetic Compatibility for Industrial-Process Measurement and Control
Equipment:
Part 2: Electrostatic Discharge Requirements
IEC 801-3; IEC 1000-4-3; Cenelec 50140:
Electromagnetic Compatibility for Electrical and Electronic Equipment:
Part 3: Immunity to Radiated, Radio Frequency, Electromagnetic Fields
IEC 801-4; IEC 1000-4-4:
Electromagnetic Compatibility for Industrial-Process Measurement and Control
Equipment
Part4: Electrical Fast Transient/Burst Requirements
IEC 801-6; IEC 1000-4-6:
Electromagnetic Compatibility for Electrical and Electronic Equipment
Part 6: Immunity to conducted disturbances induced by radio frequency fields
EN 50082-2; ELECTROMAGNETIC COMPATIBILITY, GENERIC IMMUNITY STAN-
DARD:
Part 2: Industrial Environment
ThiscertifiesthattheaforementionedequipmentconformswiththeprotectionrequirementsofCouncil
Directive89/336/EECon theapproximation ofthelaws ofthe MemberStatesrelating toElectromag-
netic Compatibility.
Signature of the Manufacturer:
John Crnko
Production Manager
(by authorization of the Chief Operating Officer)
AntekInstrumentsL.P.

Warranty and Service Policy
ANTEK Instruments L.P. warrants, to the original owner/purchaser, this instrument to be free of defects in
material and workmanship for a period of one (1) yearone (1) year
one (1) yearone (1) year
one (1) year from the date of shipment. This warranty is subject
to the following conditions and limitations:
1. ANTEK will repair or replace defective and/or nonconforming parts without charge for material or
labor or, at ANTEK’s option, demand return of instrumentation and tender repayment of
purchase price.
2. The buyer’s exclusive remedy is repair or replacement of defective and/or nonconforming parts or,
at ANTEK’s option, return of the instrumentation and repayment of the purchase price.
3. ANTEK excludes and disclaims any liability for lost profits or interruption of service or for
consequential, incidental, or special damages arising out of, resulting from, or relating in any
manner to this instrumentation.
4. This warranty does not cover defects, damage, or nonconformity resulting from abuse, misuse,
neglect,lackofreasonablecare,unauthorizedmodification,ortheattachmentofimproperdevices
to the instrumentation.
5. This warranty does not cover certain expendable items such as, but not limited to: septa, fittings,
screws, fuses, pyrolysis tubes, dryer tubes, scrubber tubes, sample boats, and inlet heater elements.
6. Photomultiplier tubes and UV lamps are warranted for ninety (90) daysninety (90) days
ninety (90) daysninety (90) days
ninety (90) days.
7. Primary furnaces are warranted for six (6) monthssix (6) months
six (6) monthssix (6) months
six (6) months.
8. All requests for service or repair under this warranty must be received within the warranty period
by ANTEK or its authorized representative.
9. Should on-site repairs be deemed necessary, ANTEK will bear all travel related expenses during the
first ninety (90) daysninety (90) days
ninety (90) daysninety (90) days
ninety (90) days of the warranty period. Alternatively, the customer may elect to ship the
instrument or component, freight prepaid, to the ANTEK service center in Houston, Texas or
Düsseldorf, West Germany. NO COLLECT SHIPMENTS WILL BE ACCEPTED.NO COLLECT SHIPMENTS WILL BE ACCEPTED.
NO COLLECT SHIPMENTS WILL BE ACCEPTED.NO COLLECT SHIPMENTS WILL BE ACCEPTED.
NO COLLECT SHIPMENTS WILL BE ACCEPTED.
a. Travel provision does not apply to accessory equipment such as, but not limited
to: Models 734, 735, 737, 738, 740, 742, and 748.
b. Travel provision does not apply to software upgrades and software-related issues.
c. Travel provision does not apply to computers, printers, or modem communications.
10. Instruments which have been repaired or replaced during the warranty period are themselves
warranted only for the remaining unexpired portion of the original one (1) year.
11. Repairs, adjustments and service performed after the expiration of the one (1) year warranty period
shallbechargedtotheowner/purchaseratthethencurrentpricesforparts,labor,andtravelrelated
expenses.
12. The warranties contained in this agreement are in lieu of all other warranties, expressed or implied,
including the warranties of merchantability and fitness for a particular purpose.
13. Statements made by any persons, including representatives of ANTEK, which are inconsistent or in
conflict with the terms of this warranty shall not be binding upon ANTEK unless reduced to writing
and approved by an officer of the company.
14. ThiswarrantyshallbegovernedbyandconstruedinaccordancewiththelawsoftheStateofTexas.StateofTexas.
StateofTexas.StateofTexas.
StateofTexas.
REVISED02/02

READ ME FIRST PACKETREAD ME FIRST PACKET
READ ME FIRST PACKETREAD ME FIRST PACKET
READ ME FIRST PACKET
UNPACKING AND INSPECTIONUNPACKING AND INSPECTION
UNPACKING AND INSPECTIONUNPACKING AND INSPECTION
UNPACKING AND INSPECTION
Carefully unpack each module and inspect for damage. If equipment damage exists, keep the
equipment, shipping carton and packaging material and file a claim with the final carrier. Usually,
the carrier will send an inspector to ascertain liability. Send a copy of the claim to:
ANTEK InstrumentsL.P. ANTEK InstrumentsGmbH
300BammelWestfieldRoad300BammelWestfieldRoad
300BammelWestfieldRoad300BammelWestfieldRoad
300BammelWestfieldRoad Wacholderstrabe7Wacholderstrabe7
Wacholderstrabe7Wacholderstrabe7
Wacholderstrabe7
Houston, TX 77090-3533 USAHouston, TX 77090-3533 USA
Houston, TX 77090-3533 USAHouston, TX 77090-3533 USA
Houston, TX 77090-3533 USA D40489 Düsseldorf GermanyD40489 Düsseldorf Germany
D40489 Düsseldorf GermanyD40489 Düsseldorf Germany
D40489 Düsseldorf Germany
Telephone: [phone]Telephone: [phone]
Telephone: [phone]Telephone: [phone]
Telephone: [phone] [phone]+203-74325
[phone]+203-74325
[phone]
Fax: [phone]Fax: [phone]
Fax: [phone]Fax: [phone]
Fax: [phone] [phone]+203-741545
[phone]+203-741545
[phone]
e-mail:[email protected]e-mail:[email protected]
e-mail:[email protected]e-mail:[email protected]
e-mail:[email protected] [email protected][email protected]
[email protected][email protected]
[email protected]
NOTENOTE
NOTENOTE
NOTE: DoDo
DoDo
Do notnot
notnot
not return the system or any module to the factory without factory authorization.return the system or any module to the factory without factory authorization.
return the system or any module to the factory without factory authorization.return the system or any module to the factory without factory authorization.
return the system or any module to the factory without factory authorization.
MATERIALS SUPPLIED BY ANTEK:MATERIALS SUPPLIED BY ANTEK:
MATERIALS SUPPLIED BY ANTEK:MATERIALS SUPPLIED BY ANTEK:
MATERIALS SUPPLIED BY ANTEK:
Customer's Checklist initials_____________
date_____________
The Antek Model 9000 Analyzer SystemAntek Model 9000 Analyzer System
Antek Model 9000 Analyzer SystemAntek Model 9000 Analyzer System
Antek Model 9000 Analyzer System includes the following modules and accessories:
______ Model 9000 Analyzer
______ Model 9000 Computer with Integrated Software
____________ CPU
____________ Monitor
____________ Keyboard
____________ Mouse
______ Computer Accessory Kit
______ Model 9000 Accessory Kit
______ OPTIONAL EQUIPMENTOPTIONAL EQUIPMENT
OPTIONAL EQUIPMENTOPTIONAL EQUIPMENT
OPTIONAL EQUIPMENT(REFER TO PURCHASE ORDER/PACKING SLIP)
MODEL 734 Gas/LPG Sampler
MODEL 735 Sample Drive
MODEL 737-9 Sample Inlet
MODEL 738 Autosampler
MODEL 740 Multi-Matrix
MODEL 748 Autosampler
PRINTER
_____________ Other — Please list ________________
_____________ Other — Please list ________________
ANTEK 9000NS MANUAL

Ifanyaccessoryitemsaremissing,notifyAntekoritsnearestbranchorrepresentative.Ifanyaccessoryitemsaredamaged
due to mishandling, follow instructions as described above.
MATERIALS REQUIRED BUT NOT SUPPLIED:MATERIALS REQUIRED BUT NOT SUPPLIED:
MATERIALS REQUIRED BUT NOT SUPPLIED:MATERIALS REQUIRED BUT NOT SUPPLIED:
MATERIALS REQUIRED BUT NOT SUPPLIED:
In order to install and operate the Antek 9000 system, the following additional materials are required:
• Small set of screw drivers
• Small set of open end wrenches including 7/16", 1/2" and 9/16"
• Small adjustable wrench
• Argon supply, dry, regulated to 3.0 bar (40 psig)
• Oxygen supply, dry, regulated to 3.0 bar (40 psig)
• Silicone stopcock grease
• Cooling water for some accessories
• 1/8" vent tube for system external vent
• 1/4" vent tube for argon purge vent (may not be present)
CAUTION: Become familiar with all modules and accessories and carefully read all instructions beforeCAUTION: Become familiar with all modules and accessories and carefully read all instructions before
CAUTION: Become familiar with all modules and accessories and carefully read all instructions beforeCAUTION: Become familiar with all modules and accessories and carefully read all instructions before
CAUTION: Become familiar with all modules and accessories and carefully read all instructions before
attemptingtoinstalland operate the system.attemptingtoinstalland operate the system.
attemptingtoinstalland operate the system.attemptingtoinstalland operate the system.
attemptingtoinstalland operate the system.
NOTENOTE
NOTENOTE
NOTE: Read Me.txt file included with software. This file can be found on the Antek 9000 software media.: Read Me.txt file included with software. This file can be found on the Antek 9000 software media.
: Read Me.txt file included with software. This file can be found on the Antek 9000 software media.: Read Me.txt file included with software. This file can be found on the Antek 9000 software media.
: Read Me.txt file included with software. This file can be found on the Antek 9000 software media.
It includes updated information regarding software functions. This file can be opened and printed usingIt includes updated information regarding software functions. This file can be opened and printed using
It includes updated information regarding software functions. This file can be opened and printed usingIt includes updated information regarding software functions. This file can be opened and printed using
It includes updated information regarding software functions. This file can be opened and printed using
WindowWindow
WindowWindow
Windowss
ss
s™™
™™
™Notepad or other text file reading software.Notepad or other text file reading software.
Notepad or other text file reading software.Notepad or other text file reading software.
Notepad or other text file reading software.
ANTEK 9000NS MANUAL

ANTEK9000NSMANUAL
TOC– 1
TABLEOFCONTENTS
Warranty/Copyright
CE Declarations
Read Me First
Unpacking and Inspection
Materials Supplied by Antek
Materials Required But Not Supplied
MSDS Sheets
Section 1 – Introduction and General Information
1.1.....................Introduction-Chemistry/Method of Detection
1.2.....................System Components
1.2.1 ..........Basic System
1.2.2 ..........Optional Equipment
1.3.....................General Specification
1.3.1 ..........Physical
1.3.2 ..........Power Requirements
1.3.3 ..........Gas Requirements
1.3.4 ..........Isothermal Temperature Zones
1.3.5 ..........System Backpressure
1.3.6 ..........Methods
1.3.7 ..........Timed Events
1.3.8 ..........Printer
1.4.....................Cautions and Warnings
1.5.....................Environmental Requirements
1.5.1 ..........Ambient Temperature
1.5.2 ..........Corrosive or Dusty Atmosphere
1.5.3 ..........Space Requirements
1.5.4 ..........Ventilation/Flammables
1.5.5 ..........Telephone Connection
1.6.....................Electrical Requirements
1.6.1 ..........Electrical Power
1.6.2 ..........Power Cords
1.7.....................Gas Requirements
1.7.1 ..........Gas Quality
1.7.2 ..........Gas Supply
1.8.....................Rear Panel

ANTEK9000NSMANUAL:TableofContents
TOC– 2
Section 2 – Installation
2.1.....................Instrument Location
2.2.....................Cautions and Warnings
2.3.....................Gas Supply Installation
2.3.1 ..........Gas Connections
2.3.2 ..........Compression Fittings
2.3.3 ..........Gas Source Leak Check
2.4.....................Pyrotube Installation/Replacement
2.4.1 ..........P/N 70061 - Standard Gas/Liquid Pyrolysis Tube
2.4.2 ..........P/N 90022 - Sample Boat Inlet Kit
2.4.3 ..........P/N 71118 - Solids Pyrolysis Tube
2.4.4 ..........P/N 91107 - Multi-matrix Sample Kit
2.5.....................Sample Flowpaths
2.5.1 ..........Gas Control
2.5.2 ..........Typical Flowpaths
2.6.....................Pre-Power-up Checklist
2.7.....................Computer and Software Overview
2.7.1 ..........General Information
2.7.2 ..........Optional Equipment
2.7.3 ..........End-User License Agreement for Antek Software
2.8.....................System Components
2.9.....................Computer Requirements
2.9.1 ..........Cautions and Warnings
2.9.2 ..........Software Criteria
2.9.3 ..........Removal of Screen Savers
2.10 ..................Computer Hardware and Software Operation Criteria
2.10.1 ........Data Acquisition Card (DAC)
2.10.2 ........Installation of the Communication/Control Cable
2.11 ..................Computer Software and Hardware Installation
2.11.1 ........Antek 9000 Software – Installation
2.11.2 ........Data Acquisition (DAQ) Control Software – Installation
2.11.3 ........Installing the Data Acquisition Card (DAQ)
2.11.4 ........Removal and Reinstallation of Software/Hardware
2.11.5 ........DAQ Setup

TOC– 3
ANTEK9000NSMANUAL:TableofContents
Section 3 – Antek Software Tutorials
3.1.....................Lesson 1 – Windows95 Introduction
3.1.1 ..........Using the Mouse
3.1.1.1 Understanding Mouse Terms
3.1.1.2 Using the Mouse Pointer within Antek Software
3.1.2 ..........Navigating the Desktop
3.5.2.1 Start Button
3.5.2.2 Task-Bar
3.5.2.3 Icons
3.1.3 ..........Working with Files and Folders
3.1.3.1 Saving Files
3.1.3.2 Specifying Paths
3.1.3.3 Locating Folders
3.1.4 ..........Finishing Lesson 1
3.2.....................Lesson 2 – Getting Started in the Antek Software
3.2.1 ..........Opening the Antek Software
3.2.2 ..........Software Demo Mode
3.2.3 ..........The 738 Autosampler Communication Window
3.2.4 ..........Antek Software Initial Screen
3.2.5 ..........Antek Software Hot Keys
3.2.6 ..........Log On Protocol
3.2.6.1 Initial Log On
3.2.6.2 Edit Users
3.2.7 ..........Antek Software Active Main Screen
3.2.8 ..........Finishing Lesson 2
3.3.....................Lesson 3 – Working with Methods
3.3.1 ..........Opening the Method Screen
3.3.2 ..........Working with Files
3.2.2.1 Opening Method Files
3.3.2.2 Creating a New Method
3.3.2.3 Editing Method Description
3.3.2.4 Saving Methods
3.3.2.5 Saving a File (Method) Under a New Name
3.3.2.6 Exporting Files
3.3.3 ..........Finishing Lesson 3
3.4.....................Lesson 4 – Setting Instrument Control Parameters
3.4.1 ..........Opening the Hardware Setting Screen
3.4.2 ..........Editing Hardware Settings
3.4.2.1 Setting Gas Flows
3.4.2.2 Turning on Detector Sources
3.4.2.3 Setting Detector Gain
3.4.2.4 Setting Detector Sensitivity
3.4.2.5 Setting Defector Voltage
3.4.2.6 Entering Manual Setpoints
3.4.3 ..........Finishing Lesson 4

ANTEK9000NSMANUAL:TableofContents
TOC– 4
3.5.....................Lesson 5 – Time Functions
3.5.1 ..........Opening the Timed Events Screen
3.5.2 ..........Editing Events
3.5.2.1 Editing a Timed Event
3.5.2.2 Adding Timed Events
3.5.2.3 Deleting an Event
3.5.2.4 Setting the Run Time
3.5.2.5 Clearing the Event Table
3.5.2.6 Recalling Timed Events Saved in a Method
3.5.3 ..........Operating the Standard Operating Procedures (SOP) Screen
3.5.3.1 Steps to SOP Setup Screen
3.5.4 ..........Finishing Lesson 3
3.6.....................Lesson 4 - Autosampler Controls
3.6.1 ..........Opening the Autosampler Screen
3.6.2 ..........Autosampler (Model 738) Method Parameters
3.6.2.1 Pre-injection Solvent Clean Cycles
3.6.2.2 Clean Cycle Fill Volume
3.6.2.3 Sample Clean Cycles
3.6.2.4 Pullup Delay Time
3.6.2.5 Sample Pullup Speed
3.6.2.6 Sample Pullup Count
3.6.2.7 Sample Fill Volume
3.6.2.8 Air Fill Volume
3.6.2.9 Needle Punch to Injection Delay
3.6.2.10 Sample Inj Speed
3.6.2.11 Inj to Needle Pullout delay
3.6.2.12 Post Injection Solvent Clean Cycles
3.6.2.13 Set A200S State
3.6.2.14 A200S State
3.6.2.15 Clean Syringe
3.6.2.16 Syringe Size
3.6.2.17 Last Function Executed
3.6.2.18 Value Set
3.6.2.19 Lock Terminal Keypad
3.6.2.20 Okay
3.6.3 ..........Editing Antek Model 738 Autosampler Injection Parameters
3.6.3.1 Two Phases of Autosampler Programming
3.6.3.2 Editing/Setting Injection Parameters with the 9000 Software
3.6.3.3 Manually Editing/Setting Injection Parameters
3.6.3.4 Selecting Changing Syringe Size
3.6.3.5 Common Problems
3.6.4 ..........Finishing Lesson 6
3.7.....................Lesson 7 – Instrument Status
3.7.1 ..........Opening the System Status Screen
3.7.2 ..........System Status
3.7.3 ..........Opening the View Trends Screen
3.7.4 ..........View Trends Screen
3.7.5 ..........Update Collection Rate
3.7.6 ..........Finishing Lesson 7

TOC– 5
ANTEK9000NSMANUAL:TableofContents
3.8.....................Lesson 8 – Print Functions
3.8.1 ..........Opening the Print Screens
3.8.2 ..........Finishing Lesson 8
3.9.....................Lesson 9 – Calibration, Tables and Files
3.9.1 ..........Opening the Calibration Screen
3.9.2 ..........Calibration Table
3.9.3 ..........Calibration Chart
3.9.4 ..........Peak Height/Peak Area Calculations
3.9.5 ..........Calibration File Management
3.9.5.1 Open File…
3.9.5.2 New File…
3.9.5.3 Save File
3.9.5.4 Save File As…
3.9.5.5 Export File
3.9.5.6 Cancel
3.9.5.7 Calibration File Help
3.9.6 ..........Finishing Lesson 9
3.10 ..................Lesson 8 - Editing Calibration Curves
3.10.1 ........Opening Calibration Edit Screen
3.10.2 ........Names, ID, Uses - Calibration
3.10.2.1 Standard Name Change
3.10.2.2 Standard Injection Name Change
3.10.2.3 Standard Concentration Change
3.10.2.4 Standard Use Modification
3.10.2.5 Standard Injection Use Modification
3.10.3 ........Display Preferences - Calibration
3.10.3.1 Calibration Chart Color Changes
3.10.3.2 Calibration Table Color Changes
3.10.3.3 Column Preferences
3.10.3.4 Decimal Displays
3.10.3.5 Cancel
3.10.3.6 Help
3.10.4 ........File Information Calibration
3.10.4.1 Text Insertion
3.10.4.2 Cancel
3.10.4.3 Help
3.10.5 ........Calibration Information
3.10.5.1 Calibration Graph
3.10.5.2 Blank Correction
3.10.5.3 Calibration Curve Order
3.10.5.4 Cancel
3.10.5.5 Help
3.10.6 ........Remove Calibration Standards
3.10.6.1 Remove Standards
3.10.6.2 Remove Standard Injections
3.10.6.3 Cancel
3.10.6.4 Help

ANTEK9000NSMANUAL:TableofContents
TOC– 6
3.10.7 ........Clear Calibration Table
3.10.8 ........Cancel
3.10.9 ........Calibration Edit Help
3.10.10 ......Finishing Lesson 10
3.11 ..................Lesson 9 - Viewing and Printing Calibration Results
3.11.1 ........Opening the View Calibration Screen
3.11.2 ........Virtual Environment
3.11.3 ........Check Standard (Control sample) Statistics
3.11.4 ........Detector Baseline Trends
3.11.5 ........Comparing Calibration Strip Charts
3.11.6 ........Calibration Sample Charts
3.11.7 ........Calibration Injection Charts
3.11.8 ........System Status Screen
3.11.9 ........Cancel - View
3.11.10 ......Help - View
3.11.11 ......Printing Calibration Curves
3.11.12 ......Finishing Lesson 11
3.12 ..................Lesson 12 – Running Calibrations
3.12.1 ........Opening the Run Calibration Screen
3.12.2 ........Setting up a Calibration Autorun File and Running a Calibration
3.12.3 ........Running a Calibration Manually
3.12.4 ........Running and Viewing a Check Standard
3.12.5 ........Recalculating a Calibration Curve
3.12.6 ........Finishing Lesson 12
3.13 ..................Lesson 11 - Sample Analysis, Tables and Files
3.13.1 ........Opening the Run Sample Screen
3.13.2 ........Sample Table - Component Description
3.13.3 ........Sample Table File Management
3.13.3.1 Open Sample File
3.13.3.2 New File
3.13.3.3 Save File
3.13.3.4 Save Sample File As
3.13.3.5 Cancel
3.13.3.6 Sample File Help
3.13.4 ........Finishing Lesson 11
3.14 ..................Lesson 14 – Editing Sample Tables
3.14.1 ........Opening the Sample Edit Screen
3.14.2 ........Names, ID's, Uses - Sample
3.14.3 ........Display Preferences - Calibration
3.14.3.1 Sample Chart Color Changes
3.14.3.2 Sample Table Color Changes
3.14.3.3 Column Preferences
3.14.3.4 Decimal Displays
3.14.3.5 Cancel
3.14.3.6 Help

TOC– 7
ANTEK9000NSMANUAL:TableofContents
3.14.4 ........File Information Samples
3.14.4.1 Text Insertion
3.14.4.2 Cancel
3.14.4.3 Help
3.14.5 ........Remove Samples
3.14.5.1 Remove Samples
3.14.5.2 Remove Sample Injections
3.14.5.3 Cancel
3.14.5.4 Help
3.14.6 ........Clear Sample Table
3.14.7 ........Cancel
3.14.8 ........Sample Edit Help
3.14.9 ........Finishing Lesson 14
3.15 ..................Lesson 15 - Viewing and Printing Sample Results
3.15.1 ........Opening the View Sample Screen
3.15.2 ........Detector Baseline Trends
3.15.3 ........Comparing Sample Stripcharts
3.15.4 ........Sample Charts
3.15.5 ........Sample Injection Charts
3.15.6 ........System Status Screen
3.15.7 ........Cancel - View
3.15.8 ........Help - View
3.15.9 ........Printing Sample Reports
3.15.10 ......Finishing Lesson 15
3.16 ..................Lesson 16 – Running Samples
3.16.1 ........Opening the Run Sample Screen
3.16.2 ........Setting Up a Sample Autorun File and Running Samples
3.16.3 ........Running Samples Manually
3.16.4 ........Recalculating a Sample Table
3.16.5 ........Finishing Lesson 16

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Section 4 – Optional Equipment and Accessories
4.1.....................Model 734 Gas/Liquefied Gas Inlet System
4.1.1 ..........Installation
4.1.1.1 Manual Systems
4.1.1.2 Automatic Systems
4.1.2 ..........Operation
4.1.2.1 Manual Systems
4.1.2.2 Automatic Systems
4.1.3 ..........Servicing Guidelines
4.1.3.1 Sample Valve
4.1.3.2 Heater Cartridge
4.1.3.3 Sight Glass
4.1.3.4 Flowmeter Assembly
4.1.3.5 Valve Actuator
4.1.3.6 Electrical/Electronic Components
4.1.4 ..........Parts List - Model 734
4.1.5 ..........Drawings - Model 734
4.2.....................Model 735 - Controlled Rate Sample Drive
4.2.1 ..........Installation
4.2.2 ..........Operation
4.2.3 ..........Servicing Guidelines
4.2.3.1 Stepper Motor
4.2.3.2 Main Printed Circuit Bond Assembly
4.2.3.3 Electrical/Electronic Components
4.2.4 ..........Parts List - Model 735
4.2.5 ..........Drawings - Model 735
4.3.....................Model 737 Temperature Programmable Inlet
4.3.1 ..........Installation
4.3.2 ..........Operation
4.3.3 ..........Servicing Guidelines
4.3.3.1 Thermocouple
4.3.3.2 Heater Element
4.3.3.3 Solid State Relay (SSR)
4.3.3.4 Rotary Actuator
4.3.3.5 Cooling Fan
4.3.3.6 Printed Circuit Board Assembly
4.3.4 ..........Parts List - Model 737
4.3.5 ..........Drawings - Model 737
4.4.....................Model 738 - Robotic Autosampler
4.4.1 ..........Installation
4.4.1.1 Direct Liquid Injection
4.4.1.2 Multi-Matrix Sample Injection
4.4.2 ..........Autosampler Method Parameters
4.4.3 ..........Sample Analysis
4.4.4 ..........Servicing Guidelines
4.4.5 ..........Parts List - Model 738
4.4.6 ..........Drawings - Model 738

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ANTEK9000NSMANUAL:TableofContents
4.5.....................Model 740 Multi-Matrix Sample Inlet
4.5.1 ..........Installation
4.5.2 ..........Operation
4.5.2.1 Model 740/Model 735
4.5.2.2 Model 740/Model 734/Model 735
4.5.2.3 Model 740/Model 734
4.5.2.4 Model 740/Model 738/Model735
4.5.3 ..........Servicing Guidelines
4.5.3.1 Cooling Fan
4.5.3.2 Thermoelectric Cooler
4.5.3.3 Printed Circuit Board Assembly
4.5.3.4 Power Supply
4.5.4 ..........Drawings
4.6.....................Installation Checklist

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Section 5 – Computer Power-up and Primary Tests
5.1.....................Power-up
5.1.1 ..........Cautions and Warnings
5.1.2 ..........Power-up
5.1.3 ..........Editing Gas Flow Settings
5.2.....................Pressure/Leak Tests
5.2.1 ..........Cautions and Warnings
5.2.2 ..........Gas Supply to Instrument Leak Check
5.3.....................Instrument Leak Check Preparations
5.3.1 ..........Instrument Leak Check (Complete Flowpath)
5.3.2 ..........Furnace Section Leak Check
5.3.3 ..........Detector Section Leak Check Procedure
5.4.....................Mass Flow Controller (MFC) Testing
5.4.1 ..........Cautions and Warnings
5.4.2 ..........Inlet Argon
5.4.3 ..........Inlet Oxygen
5.4.4 ..........Pyro Oxygen
5.4.5 ..........Ozone Oxygen
5.4.6 ..........Mass Flow Controller Accuracy Adjustment
5.5.....................Relay Control Testing
5.6.....................Furnace Power-up
5.6.1 ..........Cautions and Warnings
5.6.2 ..........Furnace Control
5.6.3 ..........Furnace Operations Overview
5.7.....................Detector Cooling
5.7.1 ..........Cautions and Warnings
5.7.2 ..........Detector Cooling Control
5.7.3 ..........Detector Cooling Overview
5.8.....................Set Backpressure
5.8.1 ..........Cautions and Warnings
5.8.2 ..........Backpressure Control
5.8.3 ..........System Backpressure Overview
5.9.....................Adjust Vacuum
5.9.1 ..........Cautions and Warnings
5.9.2 ..........Vacuum Control
5.9.3 ..........Vacuum Control Overview
5.10 ..................Obtain Operational Standby
5.10.1 ........Cautions and Warnings
5.10.2 ........Operations Study/Correcting Hardware Error Messages
5.11 ..................Primary Test Check List

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Section 6 – Start-up Basics
6.1.....................Cautions and Warnings
6.2.....................Recall (open) Antek Default Methods
6.2.1 ..........Methods Available
6.2.2 ..........Selecting and Opening a Method
6.3.....................Instrument Blank
6.4.....................Set-up to Analyze Antek Check Test Samples
6.4.1 ..........Calibration with Antek Check Test Standards
6.4.2 ..........Analyzing Samples with the Antek Check Test Standards
6.5.....................Peak Integration Techniques
6.5.1 ..........Integrate Enable and Inhibit
6.5.2 ..........Autozero Functions
6.5.3 ..........Baseline Noise Control
6.5.4 ..........Baseline Delay
6.5.5 ..........Photomultiplier Tube (PMT) Voltage
6.5.6 ..........Instrument Blank Procedure to Confirm PMT Settings

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Section 7 – Analytical Procedures and Suggestions
7.1.....................System Gas Flow Considerations
7.2.....................Furnace Temperature
7.2.1 ..........Pyro-Furnace
7.2.2 ..........Programmable Inlet Furnace (Model 737-9)
7.3.....................Sample Handling
7.3.1 ..........Liquid Sample Materials
7.3.2 ..........Solid Sample Materials
7.3.3 ..........Gas and Liquefied Gas (LPG) Sample Materials
7.4.....................Calibration
7.4.1 ..........Calibration Standard Preparation
7.4.1.1 Liquid Calibration Material
7.4.1.2 Gas Calibration Material
7.4.1.3 Solid Calibration Material
7.4.2 ..........Standard Calibration Curve(s) for Liquid Materials
7.4.3 ..........Standard Calibration Curve(s) for Gaseous Materials
7.4.4 ..........Standard Calibration Curve(s) for Solid Materials
7.5.....................Sample Analysis
7.5.1 ..........Sample Analysis
7.5.2 ..........Calculation and Interpretation of Results
7.6.....................Operational Hints
7.6.1 ..........General
7.6.2 ..........Analytical
7.6.3 ..........Important Factors for Certain Sample Types
7.6.3.1 Nitrogen and Sulfur in Liquid Hydrocarbons (Direct Injection)
7.6.3.2 Nitrogen and Sulfur in Liquid Hydrocarbons (Boat-Inlet)
7.6.3.3 Nitrogen and Sulfur in Aqueous Samples (Direct Injection)
7.6.3.4 Nitrogen and Sulfur in Aqueous Samples (Boat-Inlet)
7.6.3.5 Nitrogen and Sulfur in Gaseous & Liquefied Hydrocarbons