Buchi SyncorePlus User manual

SyncorePlus
Operation Manual
11594118 | A en

Imprint
Product Identification:
Operation Manual (Original) SyncorePlus
11594118
Publication date: 06.2020
BÜCHI Labortechnik AG
Meierseggstrasse 40
Postfach
CH-9230 Flawil 1
E-Mail: [email protected]
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experi-
ence, especially with respect to structure, illustrations and technical details.
This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for com-
petitive purposes, nor made available to third parties. The manufacture of any component with the aid of
this manual without prior written agreement is also prohibited.

BÜCHI Labortechnik AG Table of contents
Operation Manual SyncorePlus iii
Table of contents
1 About this document...........................................................................................................6
1.1 Warning notices in this document........................................................................................................ 6
1.2 Symbols............................................................................................................................................... 6
1.2.1 Warning symbols .....................................................................................................................6
1.2.2 Mark-ups and symbols.............................................................................................................7
1.3 Trademarks.......................................................................................................................................... 7
1.4 Connected devices .............................................................................................................................. 7
2 Safety....................................................................................................................................8
2.1 Proper use ........................................................................................................................................... 8
2.2 Use other than intended ...................................................................................................................... 8
2.3 Location of warning signs on the product ............................................................................................ 9
2.4 Protection devices ............................................................................................................................. 10
2.5 Staff qualification ............................................................................................................................... 10
2.6 Residual risks .................................................................................................................................... 11
2.6.1 Glass breakage......................................................................................................................11
2.6.2 Faults during operation ..........................................................................................................11
2.6.3 Hot surfaces...........................................................................................................................11
2.6.4 Dangerous vapors..................................................................................................................11
2.6.5 High internal pressure............................................................................................................12
2.6.6 Rotating parts.........................................................................................................................12
2.7 Personal protective equipment .......................................................................................................... 12
2.8 Modifications...................................................................................................................................... 12
3 Product description...........................................................................................................13
3.1 Description of function ....................................................................................................................... 13
3.2 Configuration ..................................................................................................................................... 14
3.2.1 Front view ..............................................................................................................................14
3.2.2 Rear view ...............................................................................................................................15
3.2.3 Cover .....................................................................................................................................16
3.3 Type plate.......................................................................................................................................... 16
3.4 Scope of delivery ............................................................................................................................... 17
3.5 Technical data ................................................................................................................................... 17
3.5.1 SyncorePlus...........................................................................................................................17
3.5.2 Ambient conditions.................................................................................................................18
3.5.3 Materials ................................................................................................................................18
4 Transport and storage ......................................................................................................19
4.1 Transport ........................................................................................................................................... 19
4.2 Storage .............................................................................................................................................. 19
4.3 Lifting the instrument ......................................................................................................................... 19

Table of contents BÜCHI Labortechnik AG
iv Operation Manual SyncorePlus
5 Installation..........................................................................................................................20
5.1 Before installation .............................................................................................................................. 20
5.2 Installation site................................................................................................................................... 20
5.3 Establishing electrical connections.................................................................................................... 20
5.4 Securing against earthquakes ........................................................................................................... 21
5.5 Connecting the instrument to the control system............................................................................... 21
5.6 Installing the condenser..................................................................................................................... 21
5.6.1 Installing the condenser......................................................................................................... 22
5.6.2 Connecting the coolant to the condenser ..............................................................................23
5.6.3 Connecting the vacuum pump to the condenser ...................................................................23
5.6.4 Connecting the vacuum hose for the heater cover ................................................................23
5.6.5 Installing the cap nut (Polyvap and Analyst configuration only).............................................24
5.6.6 Installing the vapor sensor (Option)....................................................................................... 24
5.7 Installing the waste vessel (SPE configuration only) ......................................................................... 25
6 Preparing the instrument for a configuration .................................................................27
6.1 Preparing a Polyvap configuration..................................................................................................... 27
6.2 Preparing an Analyst configuration.................................................................................................... 29
6.3 Preparing a SPE configuration .......................................................................................................... 32
6.3.1 Position SPE advanced valves ..............................................................................................34
7 Operation............................................................................................................................35
7.1 Operating the control panel ............................................................................................................... 35
7.1.1 Layout of the control panel.....................................................................................................35
7.1.2 Status panel...........................................................................................................................35
7.1.3 Setting the evaporation temperature...................................................................................... 36
7.1.4 Setting the cooling water follow-up time ................................................................................36
7.2 Carrying out an evaporation (with control system) ............................................................................ 36
7.3 Carrying out an evaporation (without control system) ....................................................................... 37
7.3.1 Preparing the instrument........................................................................................................ 37
7.3.2 Starting an evaporation..........................................................................................................37
7.3.3 Ending an evaporation........................................................................................................... 38
7.3.4 Shutting down the instrument ................................................................................................38
8 Cleaning and servicing .....................................................................................................39
8.1 Regular maintenance work................................................................................................................ 39
8.2 Locking and unlocking the rotation .................................................................................................... 40
8.3 Moving and retrieving the heating plate into a pre-defined position .................................................. 40
8.4 Adjusting the unbalance compensation............................................................................................. 40
8.5 Testing the vortex movement ............................................................................................................ 41
9 Help with faults ..................................................................................................................42
9.1 Troubleshooting................................................................................................................................. 42
9.2 Error messages ................................................................................................................................. 43
9.3 Changing the fuse.............................................................................................................................. 45
10 Taking out of service and disposal..................................................................................46
10.1 Taking out of service.......................................................................................................................... 46
10.2 Disposal............................................................................................................................................. 46
10.3 Returning the instrument ................................................................................................................... 46

BÜCHI Labortechnik AG Table of contents
Operation Manual SyncorePlus v
11 Appendix ............................................................................................................................47
11.1 Schematics ........................................................................................................................................ 47
11.1.1 Cooling...................................................................................................................................47
11.1.2 Communication connections..................................................................................................47
11.2 Spare parts and accessories ............................................................................................................. 48
11.2.1 Racks .....................................................................................................................................48
11.2.2 Cover .....................................................................................................................................49
11.2.3 Flushback Module..................................................................................................................49
11.2.4 Tubes .....................................................................................................................................50
11.2.5 Gaskets..................................................................................................................................51
11.2.6 Condenser .............................................................................................................................52
11.2.7 Receiving flask.......................................................................................................................52
11.2.8 Sample preparation rack........................................................................................................52
11.2.9 Cocking lever .........................................................................................................................52
11.2.10Sleeves ..................................................................................................................................53
11.2.11Accessories SPE configuration.............................................................................................. 53
11.2.12Sensors..................................................................................................................................55
11.2.13Tubing .................................................................................................................................... 55
11.2.14Tools ......................................................................................................................................55

1 | About this document BÜCHI Labortechnik AG
6/56 Operation Manual SyncorePlus
1 About this document
This operation manual is applicable for all variants of the instrument.
Read this operation manual before operating the instrument and follow the instruc-
tions to ensure safe and trouble-free operation.
Keep this operation manual for later use and pass it on to any subsequent user or
owner.
BÜCHI Labortechnik AG accepts no liability for damage, faults and malfunctions re-
sulting from not following this operation manual.
If you have any questions after reading this operation manual:
uContact BÜCHI Labortechnik AG Customer Service.
https://www.buchi.com/contact
1.1 Warning notices in this document
Warning notices warn you of dangers that can occur when handling the device. There
are four danger levels, each identifiable by the signal word used.
Signal word Meaning
DANGER Indicates a danger with a high level of risk which could result in
death or serious injury if not prevented.
WARNING Indicates a danger with a medium level of risk which could result in
death or serious injury if not prevented.
CAUTION Indicates a danger with a low level of risk which could result in mi-
nor or medium-severity injury if not prevented.
NOTICE Indicates a danger that could result in damage to property.
1.2 Symbols
The following symbols are displayed in this operation manual or on the device:
1.2.1 Warning symbols
Symbol Meaning
General warning
Device damage
Hot surface
Hand injuries
Dangerous electrical voltage

BÜCHI Labortechnik AG About this document | 1
Operation Manual SyncorePlus 7/56
Symbol Meaning
Breakable items
Explosive substances
1.2.2 Mark-ups and symbols
NOTE
This symbol draws attention to useful and important information.
RThis character draws attention to a requirement that must be met before the in-
structions below are carried out.
uThis character indicates an instruction that must be carried out by the user.
ðThis character indicates the result of a correctly carried out instruction.
Mark-up Explanation
Window Software Windows are marked-up like this.
Tab Tabs are marked-up like this.
Dialog Dialogs are marked-up like this.
[Button] Buttons are marked-up like this.
[Field names] Field names are marked-up like this.
[Menu / Menu item] Menus or menu items are marked-up like this.
Status Status is marked-up like this.
Signal Signals are marked-up like this.
1.3 Trademarks
Product names and registered or unregistered trademarks that are used in this docu-
ment are used only for identification and remain the property of the owner in each
case.
1.4 Connected devices
In addition to these operating instructions, follow the instructions and specifications in
the documentation for the connected devices.

2 | Safety BÜCHI Labortechnik AG
8/56 Operation Manual SyncorePlus
2 Safety
2.1 Proper use
The instrument is designed and built for laboratories.
The instrument can be used for the following tasks:
Parallel evaporation of solvents in various formats and containers across a range
of temperatures from room temperature up to + 100 °C and within a range of pres-
sures from 1 mbar up to ambient pressure.
Evaporation and recycling of solvents.
Concentration of extracts.
Drying of powders and granulates.
Purification of chemicals.
2.2 Use other than intended
Use of any kind other than that described in Chapter2.1 "Proper use", page8 and
any application that does not comply with the technical specifications (Chapter3.5
"Technical data", page17) constitutes use other than intended.
In particular, the following applications are not permissible:
Use of the instrument in rooms which require ex-protected instruments.
Use of samples, which can explode or inflame (example: explosives, etc.) due to
shock, friction, heat or spark formation.
Use of the instrument with solvents containing peroxides.
Use of the instrument in overpressure situations.
Use of the instrument as a reactor platform.
Damage or hazards attributable to use of the product other than as intended are en-
tirely at the risk of the operator alone.

BÜCHI Labortechnik AG Safety | 2
Operation Manual SyncorePlus 9/56
2.3 Location of warning signs on the product
4
Fig.1: Location of warning signs
Symbol Meaning
Hot surface
Hand injuries

2 | Safety BÜCHI Labortechnik AG
10/56 Operation Manual SyncorePlus
2.4 Protection devices
1
2
3
Fig.2: Protection devices
1 Protective cover 2 Crush protection
3 Button STOP
2.5 Staff qualification
Unqualified persons are unable to identify risks and are therefore exposed to greater
dangers.
The device may only be operated by suitably qualified laboratory staff.
These operating instructions are aimed at the following target groups:
Users
Users are persons that meet the following criteria:
They have been instructed in the use of the device.
They are familiar with the contents of these operating instructions and the applica-
ble safety regulations and apply them.
They are able on the basis of their training or professional experience to assess
the risks associated with the use of the device.

BÜCHI Labortechnik AG Safety | 2
Operation Manual SyncorePlus 11/56
Operator
The operator (generally the laboratory manager) is responsible for the following as-
pects:
The device must be correctly installed, commissioned, operated and serviced.
Only suitably qualified staff may be assigned the task of performing the operations
described in these operating instructions.
The staff must comply with the local applicable requirements and regulations for
safe and hazard-conscious working practices.
Safety-related incidents that occur while using the device should be reported to the
manufacturer ([email protected]).
BUCHI service technicians
Service technicians authorized by BUCHI have attended special training courses and
are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair
measures.
2.6 Residual risks
The device has been developed and manufactured using the latest technological ad-
vances. Nevertheless, risks to persons, property or the environment can arise if the
device is used incorrectly.
Appropriate warnings in this manual serve to alert the user to these residual dangers.
2.6.1 Glass breakage
Broken glass can cause severe cuts.
Minor damage to the ground joints impairs the sealing effect and may therefore dimin-
ish suction capacity.
Handle the glass components carefully and do not drop them.
Always place the glassware in a suitable holder when they are not in use.
Always visually inspect glass components for damage every time they are to be
used.
Do not continue to use glass components that are damaged.
Always wear protective gloves when disposing of broken glass.
2.6.2 Faults during operation
If a device is damaged, sharp edges, moving parts or exposed electrical wires can
cause injuries.
uRegularly check device for visible damage.
uIf faults occur, switch off the device immediately, unplug the power cord and in-
form the operator.
uDo not continue to use devices that are damaged.
2.6.3 Hot surfaces
The surfaces of the device can become very hot. If touched they can cause skin
burns.
uDo not touch hot surfaces or else wear suitable protective gloves.
2.6.4 Dangerous vapors
Distillation can produce dangerous vapors that are capable of causing life-threatening
toxic effects.
uDo not inhale any vapors produced during distillation.

2 | Safety BÜCHI Labortechnik AG
12/56 Operation Manual SyncorePlus
uEnsure that vapors are removed by a suitable fume hood.
uOnly use the device in well ventilated areas.
uIf vapors escape from joints or connections, check the seals concerned and re-
place them if necessary.
uDo not distill any unknown fluids.
uObserve the safety data sheets for all fluids used.
2.6.5 High internal pressure
The evaporation of fluids can produce high pressures inside the tubes or the con-
denser. If that pressure becomes too great, the glass components could explode.
uMake sure that the internal pressure inside the glass components is never greater
than atmospheric pressure.
uWhen distilling without a vacuum, set the vacuum pump to atmospheric pressure
so that excess pressure is automatically dissipated.
uIf a vacuum pump is not used, leave the vacuum connection open.
2.6.6 Rotating parts
Hair, clothing or jewelry can become caught up if allowed to come into contact with
the rotating parts.
At high speeds, the heating fluid may be sprayed out by the rotation.
uWear work overalls or protective clothing.
uDo not wear loose or baggy items of clothing such as scarves or neck-ties.
uTie up long hair.
uDo not wear jewelry such as necklaces or bracelets.
uAt high speeds and/or high temperatures, use the additional protective arrange-
ments.
2.7 Personal protective equipment
Depending on the application, hazards due to heat and/or corrosive chemicals may
arise.
uAlways wear appropriate personal protective equipment such as safety goggles,
protective clothing and gloves.
uMake sure that the personal protective equipment meets the requirements of the
safety data sheets for all chemicals used.
2.8 Modifications
Unauthorized modifications may impair safety and lead to accidents.
uUse only genuine BUCHI accessories, spare parts and consumables.
uTechnical modifications to the device or accessories should only be carried out
with the prior written approval of BÜCHI Labortechnik AG and only by authorized
BUCHI technicians.
BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized
modifications.

BÜCHI Labortechnik AG Product description | 3
Operation Manual SyncorePlus 13/56
3 Product description
3.1 Description of function
The instrument is a parallel evaporator which can carry out distillations of solvents in
various formats and containers across a range of temperatures from room tempera-
ture up to + 100 °C and within a range of pressures from 1 mbar up to ambient pres-
sure.
The basis of the process is the evaporation and condensing of solvents under vac-
uum.
uThe product is heated in the rack.
uThe even rotation of the rack induces a vortex on the surface of each liquid sam-
ple.
ðBy this vortex, the evaporation surface is enlarged and, therefore, the evapo-
ration is accelerated.
ðThis also constantly mixes the product which prevents localized overheating
and delayed evaporation.
uThe vapor is converged and reheated in the cover.
uThen it passes on via the vacuum hose to the condenser.
uThere, the latent heat of the vapor is transferred to the coolant fluid so that the va-
por condenses.

3 | Product description BÜCHI Labortechnik AG
14/56 Operation Manual SyncorePlus
3.2 Configuration
3.2.1 Front view
4
5
10
11
12
3
6
8
9
7
Fig.3: Front view
1 Protective cover 2 Heating base
3 Screws fixing cover 4 Connection cover
5 Venting slots 6 Crush protection
7 Unbalance compensation adjustment 8 Handle protective cover
9 On/Off master switch 10 Control panel
11 Handle protective cover

BÜCHI Labortechnik AG Product description | 3
Operation Manual SyncorePlus 15/56
3.2.2 Rear view
1
3
2
4
8
7
6
5
9 10
Fig.4: Rear view
1 Tap hole 2 Fuse
3 Mains power supply 4 Type plate Chapter3.3 "Type plate",
page16
5 BUCHI standard communication port
(COM)
6 BUCHI standard communication port
(COM)
7 Cooling water valve
(marked CW)
8 Reserve
(marked AV)
9 Ventilation slots 10 Tap hole

3 | Product description BÜCHI Labortechnik AG
16/56 Operation Manual SyncorePlus
3.2.3 Cover
123
4
Fig.5: Cover top
1 Sealing 2 Clamping nut
3 Connector cover 4 Vacuum connection
123
4
Fig.6: Cover bottom
1 Handle 2 Sealing disk
3 Screw cap 4 Support disk
3.3 Type plate
The type plate identifies the instrument. The type plate is located at the rear of the in-
strument. See Chapter3.2.2 "Rear view", page15

BÜCHI Labortechnik AG Product description | 3
Operation Manual SyncorePlus 17/56
Buchi Labortechnik AG
9230 Flawil / Switzerland
Type: xxx
SN: 10xxxxxxxx
Volt: xxx-xxx VAC
Freq.: xx Hz
Power: xxxxW Built 20xx
6
7
8
11
9
10
3
2
1
5
4
Fig.7: Type plate
1 Approval 2 Product code
3 Approval 4 Symbol for "Do not dispose of as
household waste"
5 Year of manufacture 6 Power consumption maximum
7 Frequency 8 Input voltage range
9 Serial number 10 Instrument name
11 Company name and address
3.4 Scope of delivery
NOTE
The scope of delivery depends of the configuration of the purchase order.
Accessories are delivered as per the purchase order, order confirmation, and deliv-
ery note.
3.5 Technical data
3.5.1 SyncorePlus
SyncorePlus
100 V
SyncorePlus
115 V
SyncorePlus
230 V
Dimensions (W x D x H)
(main unit)
500 x 520 x
325 mm
500 x 520 x
325 mm
500 x 520 x
325 mm
Weight
(main unit)
30 kg 30 kg 30 kg
Minimum clearance left & right 150 mm 150 mm 150 mm
Minimum clearance back 80 mm 80 mm 80 mm
Connection voltage 100 ± 10 %
VAC
115 ± 10 %
VAC
230 ± 10 %
VAC
Frequency 50/60 Hz 50/60 Hz 50/60 Hz
Power consumption 1250 W 1250 W 1400 W
Power consumption heater
cover
120 W 120 W 120 W
Rotation speed range 60 - 400 rpm 60 - 400 rpm 60 - 400 rpm
Temperature range heater cover 20 - 70 °C 20 - 70 °C 20 - 70 °C

3 | Product description BÜCHI Labortechnik AG
18/56 Operation Manual SyncorePlus
SyncorePlus
100 V
SyncorePlus
115 V
SyncorePlus
230 V
Temperature range heater base 20 - 100 °C 20 - 100 °C 20 - 100 °C
Fuse
(100 / 115 V)
SPT 12.5 SPT 12.5 FST 10
Connections external valves
(MiniDIN)
24 V ± 5 % 24 V ± 5 % 24 V ± 5 %
Connections communication
(COM)
30 V ± 5 % 30 V ± 5 % 30 V ± 5 %
Overvoltage category II II II
IP Code IP 20 IP 20 IP 20
Pollution degree 2 2 2
Approvals CE/CB CE/CB CE/CB
3.5.2 Ambient conditions
For indoor use only.
Max. altitude above sea level 2000 m
Ambient temperature 5‒40 °C
Maximum relative humidity 80% for temperatures up to 31 °C
decreasing linearly to 50 % relative hu-
midity at 40 °C
Storage temperature max. 45 °C
3.5.3 Materials
Component Materials of construction
Main unit St 1.4301
Protective shield PMMA
Rack Aluminum anodized
Vacuum connection Aluminum with PFA coating
Glass in vacuum connection Borosilicate glass
Vacuum hose Ribbed PFA
Condenser Borosilicate glass
Sealing discs Rack R4 and R-6 PTFE coating
Glass with residual volume appendix
Glass R-4 and Glass R-6
Borosilicate glass
Sealing discs, Rack R-24, R48 and R-96 Polyethylene
Crush protection POM

BÜCHI Labortechnik AG Transport and storage | 4
Operation Manual SyncorePlus 19/56
4 Transport and storage
4.1 Transport
NOTICE
Risk of breakage due to incorrect transportation
Make sure that the instrument is fully dismantled.
Pack every instrument components properly to prevent breakage. Use the original
packaging whenever possible.
Avoid sharp movements during transit.
uAfter transporting, check the instrument and all glass components for damage.
uDamage that has occurred in transit should be reported to the carrier.
uKeep packaging for future transportation.
4.2 Storage
uMake sure that the ambient conditions are complied with (see Chapter3.5 "Tech-
nical data", page17).
uWherever possible, store the device in its original packaging.
uAfter storage, check the device, all glass components, seals and tubing for dam-
age and replace if necessary.
4.3 Lifting the instrument
NOTICE
Dragging the instrument can damage the feet of the instrument.
uLift the instrument when positioning or re-locating.
uLift the instrument at the points indicated.

5 | Installation BÜCHI Labortechnik AG
20/56 Operation Manual SyncorePlus
5 Installation
5.1 Before installation
NOTICE
Instrument damage due to switching it on too early.
Switching on the instrument too early after transportation can cause damage.
uClimatize the instrument after transportation.
5.2 Installation site
NOTE
Make sure that the power supply can be disconnected at any time in an emergency.
The installation site must meet the following requirements:
Firm, level surface.
Take into account the maximum product dimensions and weight. See Chapter3.5
"Technical data", page17
Take into account the weight of the set up and the samples.
Do not place loose papers or cloths below or to the sides of the instrument, as
these could impede the air circulation if drawn in.
Do not place the instrument near vibration-sensitive devices.
Make sure that cables / tubes can be routed safely.
Own mains outlet socket
5.3 Establishing electrical connections
NOTE
Observe the legal requirements when connecting the instrument to the power supply.
4Use additional electrical safety features (e.g., residual-current circuit breakers) to
comply with local laws and regulations.
The power supply must fulfil the following conditions:
1. Provide the mains voltage and frequency specified on the type plate of the instru-
ment.
2. Be designed for the load imposed by the instruments connected.
3. Be equipped with suitable fuses and electrical safety features.
4. Be equipped with proper earthing.