Hanna Instruments HI 2212 User manual

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www.hannainst.com
pH/mV/°C
Bench Meters
with Custom Buffers
HI 2212 HI 2213
Instruction Manual

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Dear Customer,
Thank you for choosing a Hanna Instruments product.
Please read this instruction manual carefully before using these instruments.
This manual will provide you with the necessary information for correct
use of these instruments, as well as a precise idea of their versatility.
If you need additional technical information, do not hesitate to e-mail us
at [email protected] or view our worldwide contact list at
www.hannainst.com.
WARRANTYWARRANTY
WARRANTYWARRANTY
WARRANTY
HI 2212, HI 2213 are guaranteed for two years against defects in
workmanship and materials when used for their intended purpose
and maintained according to instructions. Electrodes and probes are
guaranteed for six months. This warranty is limited to repair or
replacement free of charge.
Damage due to accidents, misuse, tampering or lack of prescribed
maintenance is not covered.
If service is required, contact the dealer from whom you purchased the
instrument. If under warranty, report the model number, date of
purchase, serial number and the nature of the problem. If the repair is
not covered by the warranty, you will be notified of the charges incurred.
If the instrument is to be returned to Hanna Instruments, first obtain a
Returned Goods Authorization number from the Technical Service
department and then send it with shipping costs prepaid. When shipping
any instrument, make sure it is properly packed for complete protection.
TABLE OF CONTENTSTABLE OF CONTENTS
TABLE OF CONTENTSTABLE OF CONTENTS
TABLE OF CONTENTS
WARRANTY ............................................................................................. 2
PRELIMINARY EXAMINATION ...................................................................... 3
GENERAL DESCRIPTION ............................................................................ 3
FUNCTIONAL DESCRIPTION HI 2212 AND HI 2213 .................................... 4
HI 2212 AND HI 2213 SPECIFICATIONS ................................................... 5
OPERATIONAL GUIDE ................................................................................ 6
pH CALIBRATION ...................................................................................... 8
pH BUFFER TEMPERATURE DEPENDENCE ................................................. 13
GOOD LABORATORY PRACTICE (GLP) ........................................................ 14
SETUP .................................................................................................. 17
TEMPERATURE CALIBRATION (for technical personnel only) .......................... 20
mV CALIBRATION (for technical personnel only) .......................................... 22
RELATIVE mV CALIBRATION (HI 2213).................................................... 23
ELECTRODE CONDITIONING & MAINTENANCE ............................................. 24
TROUBLESHOOTING GUIDE ..................................................................... 27
TEMPERATURE CORRELATION FOR pH SENSITIVE GLASS ............................. 28
ACCESSORIES ........................................................................................ 29

3
The HANNA HI 2212 and HI 2213 are microprocessor based pH and
temperature bench meters.
HI 2213 can also measure Oxidation Reduction Potential (ORP) in mV
range. Relative mV feature is also provided.
pH measurements are compensated for temperature effect manually or
automatically with the HI 7662temperature probe.
Calibration can be performed at up to three-points using two custom
buffers and five standard buffers.
The GLP feature provides data consistency.
A calibration due alarm can be set to alert the user that too much time
elapsed since the last pH calibration.
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully
to make sure that no damage has occurred during shipping. If there is
any damage, notify your Dealer or the nearest Hanna Customer Service
Center.
Each instrument is supplied with:
• HI 1131B Glass-body Combination pH Electrode with 1 m (3.3')
Cable
• HI 7662 Temperature Probe
• HI 76404N Electrode Holder
• pH 4.01 & 7.01 Buffer Solutions (20 mL each)
• HI 7071 Electrolyte Solution
• HI 700661 Electrode Cleaning Solution
• 12VDC Power Adapter
• Instruction Manual
Note: Save all packing material until you are sure that the instrument
functions correctly. All defective items must be returned in the
original packing with the supplied accessories.
GENERAL DESCRIPTIONGENERAL DESCRIPTION
GENERAL DESCRIPTIONGENERAL DESCRIPTION
GENERAL DESCRIPTION

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Front Panel
Rear Panel
1) Liquid Crystal Display (LCD).
2) CAL key, to enter and exit calibration mode.
3) CFM/GLP key, to confirm different values or to display Good
Laboratory Practice information.
4) ºC key, to manually increase temperature value or other parameters.
5) ºC key, to manually decrease temperature value or other parameters.
6) SETUP key, to enter/exit SETUP mode.
7) RANGE key, to select measurement range or to toggle between the
buffer value and temperature during calibration or to change the
focused data in setup (HI 2213 only).
ukey, to toggle between the buffer value and temperature during
calibration or to change the focused data in setup (HI 2212 only).
8) MEM key, to store a value into memory.
9) MR key, memory recall.
10) ON/OFF switch.
11) Power supply socket.
12) BNC electrode connector.
13) Temperature probe socket.
14) Electrode reference socket.
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTION
HI 2212 AND HI 2213HI 2212 AND HI 2213
HI 2212 AND HI 2213HI 2212 AND HI 2213
HI 2212 AND HI 2213

5
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HI 2212 AND HI 2213HI 2212 AND HI 2213
HI 2212 AND HI 2213HI 2212 AND HI 2213
HI 2212 AND HI 2213
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS

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3 cm
(1¼")
POWER CONNECTION
Plug the 12 VDC adapter into the power supply socket.
Notes:•These instruments use non volatile memory to retain the pH,
mV, temperature calibrations and all other settings, even
when unplugged.
•Make sure a fuse protects the main line.
ELECTRODE AND PROBE CONNECTIONS
For pH or ORP measurements connect an electrode with internal reference
to the BNC connector on the back of the instrument.
For electrodes with a separate reference connect the electrode’s BNC to the
BNC connector and the reference electrode plug to the reference socket.
For temperature measurements and automatic temperature compensation
connect the temperature probe to the appropriate socket.
INSTRUMENT START-UP
•Turn the instrument on by pressing the ON/OFF switch located on
the rear panel.
•All LCD tags are displayed and a beep is sounded while the instruments
perform a self test.
pH MEASUREMENTS
Make sure the instrument has been calibrated before
taking pH measurements.
•Submerse the electrode tip and the temperature
probe approximately 3 cm (1¼”) into the sample
to be tested and stir gently. Allow time for the
electrode to stabilize.
•The pH is displayed on the primary LCD and the temperature on the
secondary LCD.
•If the reading is out of range, the closest full-scale value will be
displayed blinking on the primary LCD.
OPERATIONAL GUIDEOPERATIONAL GUIDE
OPERATIONAL GUIDEOPERATIONAL GUIDE
OPERATIONAL GUIDE

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Ifmeasurementsaretakensuccessivelyindifferentsamples,itisrecommended
to rinse the electrode thoroughly with deionized water or tap water and
then with some of the next sample to prevent cross-contamination.
The pH reading is affected by temperature. In order to measure the pH
accurately, the temperature effect must be compensated for. To use the
Automatic Temperature Compensation feature, connect and submerse
the HI 7662 temperature probe into the sample as close as possible to
the electrode and wait for a few seconds.
If the temperature of the sample is known, manual temperature
compensation can be used by disconnecting the temperature probe.
The display will show the last temperature reading
with the “ºC” tag blinking.
The temperature can now be adjusted with the
ARROW keys (from –20.0 ºC to 120.0 ºC).
mV/ORP MEASUREMENTS (HI 2213)
An optional ORP electrode must be used to perform ORP measurements
(see Accessories).
Oxidation-Reduction Potential (REDOX) measurements provide the
quantification of the oxidizing or reducing power of the tested sample.
The surface of the ORP electrode must be clean and
smooth in order to obtain an accurate measurement.
•Press RANGE to enter mV range.
•Submerse the tip of the ORP electrode 3 cm (1¼”)
into the sample to be tested and allow a few
seconds for the reading to stabilize.
•The instrument displays the mV reading on the primary LCD and the
temperature on the secondary LCD.
•If the reading is out of range, the closest full-scale value will be
displayed blinking on the primary LCD.
3 cm
(1¼")

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RELATIVE mV MEASUREMENTS (HI 2213)
•Press RANGE until “rEL” message will be displayed on the secondary
LCD line for one second and “mV” tag will blink. After one second the
temperature will be displayed on the secondary LCD.
The reading displayed by the instrument is equal to the difference
between the current mV input value and relative mV offset established in
the relative mV calibration.
TEMPERATURE MEASUREMENTS
Connect the HI 7662 temperature probe to the
appropriate socket and turn the instrument on.
Submerse the temperature probe into the sample and
allow the reading on the secondary LCD to stabilize.
MEMORY FUNCTION
Press and hold down MEM key to store the last reading
in the meters memory. The “MEM” tag will be
displayed.
Press MR (memory recall) key to display the memorized
reading. The “MEM” tag will be displayed.

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Calibrate the instrument frequently, especially if high accuracy is
required.
The instrument should be recalibrated:
•Whenever the pH electrode is replaced.
•At least once a week.
•After testing aggressive chemicals.
•If “CAL” “INTV” tags are blinking during measurement.
Every time you calibrate the instrument use fresh buffers and perform an
electrode Cleaning Procedure (see page 26).
PREPARATION
Pour small quantities of the buffer solutions into clean beakers. If
possible, use plastic or glass beakers to minimize any EMC interferences.
For accurate calibration and to minimize cross-contamination, use two
beakers for each buffer solution. One for rinsing the electrode and one for
calibration.
If you are measuring in the acidic range, use pH 7.01 or 6.86 as first
buffer and pH 4.01 as second buffer. If you are measuring in the alkaline
range, use pH 7.01 or 6.86 as first buffer and pH 10.01, 9.18 as second
buffer.
PROCEDURE
Calibration can be performed up to three-points.
For accurate measurements, a three-point calibration is recommended.
However, a one or two point calibration can also be used.
The calibration buffers can be selected from the calibration buffer list that
includes custom buffers and the memorized standard buffers:
•pH 4.01, 6.86, 7.01, 9.18 and 10.01.
The custom buffers allow the user to calibrate in a buffer solution different
from a standard one. Up to two custom buffers can be set in SETUP menu
(see page 17). Each custom buffer value can be changed in a ±1.0 pH
window around the set value (in according with temperature), during
calibration, when it is selected; the “BUFFER pH” tag will blink.
The instruments will automatically skip the buffer used during calibration
and the buffers which are in a ±0.2 pH window, around one of the
calibrated buffers.
All new calibrations will override existing stored calibration data in a
±0.2 pH window. The slopes adjacent to the new points will be reevaluated.
pp
pp
pH CALIBRATIONH CALIBRATION
H CALIBRATIONH CALIBRATION
H CALIBRATION

10
3 cm
(1¼")
THREE-POINT CALIBRATION
•Submerse the pH electrode and the temperature
probe approximately 3cm (1¼”) into a buffer
solution and stir gently. The temperature probe
should be close to the pH electrode.
•Press CAL. The “CAL” and “
BUF
” tags will
appear and the “7.01” buffer will be displayed
on the secondary LCD.
•If necessary, press the ARROW keys to select a different buffer value.
•The “ ” tag will blink on the LCD until the reading is stable.
•When the reading is stable and close to the
selected buffer, the “READY” tag will be
displayed and the “CFM” tag will blink.
•Press CFM to confirm calibration.
•The calibrated value will be displayed on the
primary LCD and the second expected buffer value
on the secondary LCD.
•After the first calibration point is confirmed, submerse the pH electrode
and the temperature probe approximately 3 cm (1¼”) into the
second buffer solution and stir gently. The temperature probe should
be close to the pH electrode.
•If necessary, press the ARROW keys to select a different buffer value.
•The “ ” tag will blink on the LCD until the reading is stable.
•When the reading is stable and close to the
selected buffer, the “READY” tag will be
displayed and the “CFM” tag will blink.
•Press CFM to confirm calibration.
•The calibrated value is then displayed on the
primary LCD and and the third expected buffer
value on the secondary LCD.
•After the second calibration point is confirmed,
submerse the pH electrode and the temperature
probe approximately 3 cm (1¼”) into the next buffer solution and
stir gently. The temperature probe should be close to the pH electrode.
•If necessary, press the ARROW keys to select a different buffer value.

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•The “ ” tag will blink on the LCD until the reading
is stable.
•When the reading is stable and close to the selected
buffer, the “READY” tag will be displayed and the
“CFM” tag will blink.
•Press CFM to confirm calibration.
•The instrument stores the calibration value and
returns to measurement mode.
TWO-POINT CALIBRATION
•Proceed as described in “THREE-POINT CALIBRATION” section.
•Press CAL after the second calibration point was confirmed. The
instrument will memorize the calibration data and return to
measurement mode.
ONE-POINT CALIBRATION
Two SETUP selectable options are available: “Pnt” and “OFFS”.
If the “Pnt” option is selected, the new calibration point overrides an
existing one. The adjacent slopes will be reevaluated.
If the “OFFS” option is selected, an electrode offset correction is performed.
The existing slopes will remain unchanged.
•Proceed as described in “THREE-POINT CALIBRATION” section.
•Press CAL after the first calibration point was confirmed. The
instrument will memorize the one-point calibration data and return
to measurement mode.
Notes:•If the value measured by the instrument is not close to the
selected buffer, “WRONG” “ ” and “WRONG” “ ” tags
will blink alternately. Check if the correct buffer has been
used, or clean the electrode by following the Cleaning Procedure
(see page 26). If necessary, change the buffer or the electrode.
•When a custom buffer is displayed, the “BUFFER pH” tag
blinks. To change the custom buffer value in according with
the buffer temperature proceed as described in “WORKING
WITH CUSTOM BUFFERS” (see page 12).
•If the buffer temperature or the manual temperature
exceeds the temperature limits of the buffer, “WRONG” tag
and temperature reading will blink.
•If “WRONG”, “BUFFER pH” tags and “OLd” message are
displayed blinking on the secondary LCD line, an inconsistency
between new and previous (old) calibration is detected.
Clear calibration parameters and proceed with calibration
from the current calibration point. The instrument will keep
all confirmed values during current calibration.

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•To clear calibration parameters for all buffers starting with
current buffer, press and hold down CFM, then press CAL.
The calibration will continue from the current point. If
this procedure is performed while calibrating in the first
calibration point “CLr ALL” message is displayed for a few
seconds then the instrument
returns to measurement.
•Press RANGE (ufor HI 2212)
to toggle between pH buffer and
temperature reading.
•Each time a buffer is confirmed, the new calibration data
replaces the old calibration data of the corresponding buffer.
If current confirmed buffer has no previous data stored and
the calibration is not full (three buffers), the current buffer
is added to the existing data. If the existing calibration is
full, the instrument asks which buffer to replace.
Press the ARROW keys to select another buffer to be replaced.
Press CFM to confirm the buffer that will be replaced.
Press CAL to leave calibration without replacing.
Note:If the replaced buffer is outside the ±0.2 pH window,
around each of the calibrated buffers, it is possible to
select this buffer for next calibration during current
calibration.
WORKING WITH CUSTOM BUFFERS
If a custom buffer was set in SETUP menu, it can be selected for calibration
by pressing the ARROW keys. The “BUFFER pH” tag will blink.
Press SETUP if you want to adjust the buffer value. The buffer value will
start blinking.
Use the ARROW keys to change the buffer value.
After 5 seconds the buffer value is updated. Press SETUP if you want to
change it again.
Note:Custom buffer value can be adjusted in a ±1.00 pH window,
around the set value.

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The temperature has an effect on pH. The calibration buffer solutions are
affected by temperature changes to a lesser degree than normal
solutions. During calibration the instrument will automatically calibrate
to the pH value corresponding to the measured or set temperature.
During calibration the instrument will display the pH buffer value at 25 ºC.
PMET SREFFUBHp
Cº Fº 10.4 68.6 10.7 81.9 10.01
0 23 10.4 89.6 31.7 64.9 23.01
5 14 00.4 59.6 01.7 93.9 42.01
01 05 00.4 29.6 70.7 33.9 81.01
51 95 00.4 09.6 40.7 72.9 21.01
02 86 00.4 88.6 30.7 22.9 60.01
52 77 10.4 68.6 10.7 81.9 10.01
03 68 20.4 58.6 00.7 41.9 69.9
53 59 30.4 48.6 99.6 01.9 29.9
04 401 40.4 48.6 89.6 70.9 88.9
54 311 50.4 38.6 89.6 40.9 58.9
05 221 60.4 38.6 89.6 10.9 28.9
55 131 70.4 48.6 89.6 99.8 97.9
06 041 90.4 48.6 89.6 79.8 77.9
56 941 11.4 58.6 99.6 59.8 67.9
07 851 21.4 58.6 99.6 39.8 57.9
57 761 41.4 68.6 00.7 19.8 47.9
08 671 61.4 68.6 10.7 98.8 37.9
58 581 71.4 78.6 20.7 78.8 47.9
09 491 91.4 88.6 30.7 58.8 57.9
59 302 02.4 98.6 40.7 38.8 67.9
pp
pp
pH BUFFER TEMPERATUREH BUFFER TEMPERATURE
H BUFFER TEMPERATUREH BUFFER TEMPERATURE
H BUFFER TEMPERATURE
DEPENDENCEDEPENDENCE
DEPENDENCEDEPENDENCE
DEPENDENCE

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GLP is a set of functions that allows storage and retrieval of data
regarding the maintenance and status of the electrode.
All data regarding the last calibration (one, two, or three point) is stored
for the user to review when necessary. This data includes the following:
calibration time stamp, offset (mV), average of slope (%), calibration
buffers and the time until a new calibration is required.
EXPIRED CALIBRATION
These instruments allow the user to set the number of days before the
next required calibration. This value can be set from 1 to 7 days. The
default setting is OFF (disabled).
The instruments check if the time-out time has expired. If the time
elapsed, the “CAL” “INTV” tags will blink as a reminder.
Note:If the instruments were not calibrated, the “CAL” “INTV” tags
will be displayed even if the feature is disabled in SETUP menu.
pH CALIBRATION DATA
Calibration data is stored automatically after a successful calibration.
To view the pH calibration data, press GLP while in measurement mode.
The instruments will display the time (hh:mm) of the last calibration.
Use the ARROW keys to scroll through the calibration data:
•The date (yyyy.mm.dd).
•The pH calibration offset.
•The pH calibration slope (the GLP slope is the average of the calibration
slopes; the percentage is referred to the ideal value of 59.16 mV/pH).
GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GLP)
GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GLP)
GOOD LABORATORY PRACTICE (GLP)

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•The pH calibration buffers in calibrating order.
The first pH calibration buffer:
The second pH calibration buffer:
The third pH calibration buffer:
Notes:•The “OLd” message displayed beside the pH value means
that this buffer was not used during last calibration. Press
and hold down SETUP if you want to see calibration date
(or time, if old calibration was performed on the same day
as the current calibration).
•For each custom buffer used in calibration, the “BUFFER
pH” tag will blink.
•If “no bUF” message appears on the LCD, the instrument
informs you that the calibration was performed with less than
three buffers.
•Calibration Expiration status:
-if disabled

16
-or the number of days until the calibration alarm will be displayed
-or if expired (7 days ago)
Notes:•Press GLP to return to measurement mode.
•If calibration has not been performed, the instrument
displays “no CAL”.

17
EXPIRED CALIBRATION ALARM
Press CAL when the calibration time-out is displayed. Calibration time-out
(“OFF” or “1” to “7” days) and “CFM” will start blinking.
Press the ARROW keys to change the calibration time-out value.
Press CFM to save the modified calibration time-out value.
Press CAL to escape without saving.
FIRST CUSTOM BUFFER
Press CAL when “cb1” is displayed. The custom buffer (disabled –
“no” or “0”to “16”pH) and “CFM”will start blinking.
Press the ARROW keys to change the custom buffer value.
Press CFM to save the modified custom buffer value.
Press CAL to escape without saving.
Setup mode allows viewing and modifying the following parameters:
•Expired Calibration Alarm
•First Custom Buffer
•Second Custom Buffer
•One-point Calibration Behavior
•Current Time (hour & minute)
•Current Date (year, month & day)
•Beep Status
•Temperature Unit
To enter SETUP mode press SETUP while the instrument is in
measurement mode.
Select a parameter with the ARROW keys.
Press CAL if you want to change a parameter value. The selected
parameter will start blinking.
Press RANGE (ufor HI 2212) to toggle between displayed parameters.
Press the ARROW keys to increase or decrease the displayed value.
Press CFM to save the modified value or CAL to escape.
SETUPSETUP
SETUPSETUP
SETUP

18
SECOND CUSTOM BUFFER
Press CAL when “cb2” is displayed. The custom buffer (disabled –
“no” or “0”to “16”pH) and “CFM”will start blinking.
Press the ARROW keys to change the custom buffer value.
Press CFM to save the modified custom buffer value.
Press CAL to escape without saving.
ONE-POINT CALIBRATION BEHAVIOR
Press CAL when “1 Pnt” message is displayed on the secondary LCD.
One of the two options (“Pnt” or “OFFS”) and “CFM”will start
blinking (see pH CALIBRATION PROCEDURE for details, page 8).
Press the ARROW keys to toggle between “Pnt” and “OFFS” options.
Press CFM to save the behavior for one-point calibration.
Press CAL to escape without saving.
CURRENT TIME
Press CAL when the current time is displayed. The hour and “CFM”will
start blinking.
Press the ARROW keys to change the hour.
Press RANGE (HI 2213) or u(HI 2212). The minutes and “CFM”will
start blinking.
Press the ARROW keys to change the minutes.
Press CFM to save the modified value.
Press CAL to escape without saving.

19
CURRENT DATE
Press CAL when the current date is displayed. The year and “CFM” will
start blinking.
Press the ARROW keys to change the year.
Press RANGE (HI 2213) or u(HI 2212). The month and “CFM” will
start blinking.
Press the ARROW keys to change the month.
Press RANGE (HI 2213) or u(HI 2212). The day and “CFM” will start
blinking.
Press the ARROW keys to change the day.
Press CFM to save the modified value.
Press CAL to escape without saving.
BEEP STATUS
Press CAL when the beep status is displayed. Beep status (“On” or
“OFF”) and “CFM” will start blinking.
Press the ARROW keys to change the beep status (On or OFF).
Press CFM to save the modified beep status.
Press CAL to escape without saving.
TEMPERATURE UNIT
Press CALwhen “tnP is displayed. The temperature unit and “CFM” will
start blinking.
Press the ARROW keys to change the option.
Press CFM to save the modified temperature unit.
Press CAL to escape without saving.

20
All the instruments are factory calibrated for temperature.
Hanna’s temperature probes are interchangeable and no temperature
calibration is needed when they are replaced.
If the temperature measurements are inaccurate, temperature recalibration
should be performed.
For an accurate recalibration, contact your dealer or the nearest Hanna
Customer Service Center, or follow the instructions below.
•Prepare a vessel containing ice and water and another one containing
hot water (around 50 ºC). Place insulation material around the
vessels to minimize temperature changes.
•Use a calibrated thermometer with a resolution of 0.1 ºC as a reference
thermometer.
•With the instrument off, press and hold down the CFM & SETUP
keys, then power on the instrument. The “CAL” tag will appear and
the secondary LCD will show “0.0 ºC”.
•Submerse the temperature probe in the vessel with ice and water as
near as possible to the reference thermometer. Allow a few seconds for
the probe to stabilize.
•Use the ARROW keys to set the reading on the secondary LCD to that
of ice and water, measured by the reference thermometer. When the
reading is stable and close to the selected calibration point, “READY”
tag will appear and “CFM” tag will blink.
•Press CFM to confirm. The secondary LCD will show “50.0 ºC”.
•Submerse the temperature probe in the second vessel as near as
possible to the reference thermometer. Allow a few seconds for the
probe to stabilize.
TEMPERATURE CALIBRATIONTEMPERATURE CALIBRATION
TEMPERATURE CALIBRATIONTEMPERATURE CALIBRATION
TEMPERATURE CALIBRATION
((
((
(for technical personnel onlyfor technical personnel only
for technical personnel onlyfor technical personnel only
for technical personnel only))
))
)