Peak Scientific Genius 3010 User manual

Genius3010-3013-3020-3022 User Manual Rev 1 PN UM-0008 03/02/17
Genius 3010/13/20/22
User Manual

Page 2
Contents
Change History 3
How to use this Manual 3
Introduction 4
Warranties and Liabilities 5
Safety Notices 6
Symbols 6
Safety Notice to Users 6
Declaration of Conformity 7
Environmental Declaration 8
Technical Specification 9
Unpacking 13
Fittings Kit Contents 14
Installation 15
Generator Environment 15
3010/3013 General Dimensions 16
3010/3013 Rear Connections 17
3020/3022 General Dimensions 18
3020/3022 Rear Connections 19
Electrical Connection 20
Start-Up Sequence 21
Normal Operation 22
On Demand Gas 22
Generator Cycling 22
Unusual Operation 22
Connecting to the application 23
Tubing Lengths 23
Service Requirements 24
Service Schedule 24
Peak Protected 26
Cleaning 27
Troubleshooting 28

Page 3
Change History
Rev Comment Name Date
How to use this Manual
This manual is intended for end users and has been written as a reference document
where you can skip to the relevant information.
Users can refer to the contents page to find the relevant information.
Please review each of the following sections carefully.
Thank you for selecting Peak Scientific to meet your gas generation needs, and should
you require any further assistance or support please do not hesitate to contact Peak
Scientific or the Peak Partner from which you purchased your generator.

Page 4
Introduction
The Genius 3010, 3013, 3020 & 3022 have been developed to provide a supply of
nitrogen gas for your LC/MS instrument. We’ve built them with internal air compressors
as standard, removing the reliance upon an in-house air supply.
These model provide a source of nitrogen gas with other features including:
• Quiet in operation – Insulated compressor compartment for minimum disruption
• Cool – Minimal heat build-up in the lab
• Intelligent – High duty service indicator
• Mobile – Flexibility to position the generator where required
• Simple installation – Generator designed as a plug and play system
• Economical – More cost effective than any other gas supply method
• Convenient – Gas on demand, no hazards, no need to worry about running out of
gas
The Genius 3010, 3013, 3020 & 3022 are based on proven technology, and selectively
remove oxygen, moisture and other gases to leave clean, dry, phthalate free nitrogen.
Internal air compressors make these units independent from in-house air supplies and
fitted castors allow the user to easily position the units in the lab.
To ensure these Generator models meet our high expectations with regards to reliability
and performance, we have tested them extensively at our manufacturing plant and with
end users around the world to ensure reliability and longevity of the system.

Page 5
Warranties and Liabilities
1. The Company warrants that it has title to the Goods.
2. Subject to the provisions of this clause the Company warrants that the Goods
shall comply in all material respects with any specification referred to in the Order
Confirmation (as the same may be amended) and shall, subject thereto, be free
from defects in material and workmanship for the lesser of a period of twelve
months from the date of delivery or thirteen months from the date of dispatch
from the factory.
3. Save as provided in this clause and except where the Goods are sold to a person
dealing as a consumer (within the meaning of the Unfair Contract Terms Act
1977) all warranties, conditions or other terms implied by statute or common
law are hereby expressly excluded save to the extent they may not be lawfully
excluded. When the Goods are sold to a consumer within the meaning of the Unfair
Contract Terms Act 1977 their statutory rights are not affected by the provisions of
this clause.
4. In the event of the Customer making a claim in respect of any defect in terms of
clause 2 hereof the Customer must.
1. Reasonably satisfy the Company that the Goods have been properly installed,
commissioned, stored, serviced and used and without prejudice to the generality
of the foregoing that any defect is not the direct or indirect result of lack of repair
and/or servicing, incorrect repair and/or servicing, use of wrong materials and/or
incorrect spare parts
2. Allow the company to inspect the Goods and/or any installation and any relevant
packaging as and when reasonably required by the Company.
5. Subject to the Company being notified of any defect as is referred to in sub-
clause 2 hereof within a reasonable time of it becoming apparent and subject always
to the terms of sub-clause 4 hereof, the Company shall, in its option, replace or
repair the defective Goods or refund a proportionate part of the Price. The Company
shall have no further liability to the Customer (save as mentioned in sub-clause 6
hereof).
6. The Company shall be liable to indemnify the Customer in respect of any claim
for death or personal injury to any person in so far as such is attributable to the
negligence or breach of duty of the Company or any failure by the Company to
comply with the provisions of sub-clause 2 hereof.
7. Save as provided in sub-clause 2 hereof the Company shall not be liable in respect
of any claim by the Customer for costs, damages, loss or expenses (whether direct,
indirect, consequential or otherwise) or indemnity in any respect howsoever arising
including, but not by way of limitation, liability arising in negligence (other than
pursuant to clause 6 above) that may be suffered by the Customer or any third
party.

WARNING
WARNING
WARNING
WARNING
CAUTION
Page 6
Safety Notices
Peak Scientific Instruments cannot anticipate every possible circumstance which may
represent a potential hazard. The warnings detailed within this manual refer to the most
likely potential hazards, but by definition cannot be all inclusive. If the user employs
an operating procedure, item of equipment or a method of working which is not
specifically recommended by Peak Scientific, the user must ensure that the equipment
will not be damaged or become hazardous to persons or property.
Symbols
This manual uses the following symbols to highlight specific areas important to the safe
and proper use of the generator.
A WARNING notice denotes a hazard. It calls attention to an operating procedure,
process or similar, which if not correctly performed or adhered to, could cause
personal injury or in the worst case death. Do not proceed beyond a WARNING
notice until the indicated conditions are fully understood or met.
A CAUTION notice denotes a hazard. It calls attention to an operating procedure,
process or similar, which if not correctly performed or adhered to, could cause
damage to the generator or the application. Do not proceed beyond a CAUTION
notice until the indicated conditions are fully understood or met.
Caution, risk of electric shock. Ensure power to the generator has been removed
before proceeding.
Safety Notice to Users
These instructions must be read thoroughly and understood before
installation and operation of your Peak Generator. Use of the generator
in a manner not specified by Peak Scientific MAY impair the SAFETY
provided by the equipment.
When handling, operating or carrying out any maintenance, personnel
must employ safe engineering practices and observe all relevant local
health and safety requirements and regulations. The attention of UK
users is drawn to the Health and Safety at Work Act 1974, and the
Institute of Electrical Engineers regulations.
If the equipment is used in a manner not specified by the manufacturer,
the protection provided by the equipment maybe impaired.

Page 7
Declaration of Conformity
We Peak Scientific Instruments Ltd.
Of Fountain Crescent, Inchinnan, Renfrewshire, PA4 9RE
Declare that:
Equipment: Nitrogen Gas Generator
Models: Genius 3010, 3013, 3020 & 3022
To which this declaration relates, is in conformity with the applicable EC directives,
harmonized standards, and other normative requirements.
• Low Voltage Directive 2015/35/EU
EN 61010-1: 2010 Electrical Equipment for measurement, control and laboratory use.
• Electromagnetic Compatibility Directive 2014/30/EU
EN 61326-1: 2013 Electrical Equipment for measurement, control and laboratory use.
• FCC47 CFR Part 15 Class B
Unintentional radiators; Conducted and Radiated emissions limits.
All evaluation, testing and certification issued by:
Nemko Canada Inc.
303 River Road
Ottawa
Ontario
Canada
K1V 1H2
Signed: Name: Chris Pugh
Date: 03/02/2017 Position: Chief Technology Officer

Page 8
Environmental Declaration
We Peak Scientific Instruments Ltd.
Of Fountain Crescent, Inchinnan, Renfrewshire, PA4 9RE
Declare that:
Equipment: Nitrogen Gas Generator
Models: Genius 3010, 3013, 3020 & 3022
Is fully compliant with the following Directives
• 2012/19/EU WEEE (Waste of Electrical and Electronic Equipment)
• 2011/65/EU RoHS 2 (Restriction of Hazardous Substance)
Peak Scientific Instruments Ltd fully complies with its obligations towards the European
WEEE (Waste of Electrical and Electronic Equipment) Directive 2012/19/EU. These
obligations are being met within the B2B compliance group.
Peak Scientific Instruments Ltd has developed all reasonable ‘due diligence’ controls to
ensure that our products comply with the principles and requirements of the European
recast RoHS (Restriction of Hazardous Substances) Directive 2011/65/EU. Similar
directives in the United States and China, for example, have also been captured within
this program.
Where a specific certificate of compliance is required, this can be requested, on
a product serial number basis, directly from Peak Scientific Instruments Ltd, by
contacting us through our website on www.peakscientific.com
Signed: Name: Chris Pugh
Date: 10/06/2015 Position: Engineering & Operations Director

Page 9
Technical Specification
Genius 3010
Environment
Minimum Operating Ambient Temperature 5°C (41°F)
Maximum Operating Ambient Temperature 35°C (95°F)
Maximum Altitude 2000 m
Maximum Relative Humidity 80% Non-Condensing
Minimum Storage Temperature* -20°C (-4°F)
Maximum Storage Temperature* 60°C (140°F)
Generator Outlets
Maximum Gas Output Pressure 6.9 bar (100 psi)
Maximum Outlet Flow Rate 64 L/min (2.26 cfm)
Start-Up Time 30 mins
Particles <0.01µm
Phthalates NONE
Suspended Liquids NONE
Gas Outlets 1 x ¼” BSPP
Drain Outlets 1 x ¼” BSPP
Pressure Gauges 1
Electrical Requirements
Voltage 230 VAC ± 10%
Frequency 50/60 Hz
Current 12 Amps
Input Connection C20 Plug
Power Cord (Supplied) C19 socket to local connection (13A minimum)
Pollution Degree 2
Insulation Category II
General
Dimensions cm (inches) WxDxH 60 x 85 x 132.2 (23.6 x 33.5 x 52.0)
Generator Weight Kg (lbs) 189 kg (417lb)
Shipping Weight Kg (lbs) 265.5 kg (585lb)

Page 10
Technical Specification
Genius 3013
Environment
Minimum Operating Ambient Temperature 5°C (41°F)
Maximum Operating Ambient Temperature 35°C (95°F)
Maximum Altitude 2000 m
Maximum Relative Humidity 80% Non-Condensing
Minimum Storage Temperature* -20°C (-4°F)
Maximum Storage Temperature* 60°C (140°F)
Generator Outlets
Maximum Gas Output Pressure 6.9 bar (100 psi)
Maximum Outlet Flow Rate 64 L/min (2.26 cfm)
Chip Cube Mode increased O2 content to 10%
Start-Up Time 30 mins
Particles <0.01µm
Phthalates NONE
Suspended Liquids NONE
Gas Outlets 1 x ¼” BSPP
Drain Outlets 1 x ¼” BSPP
Pressure Gauges 1
Electrical Requirements
Voltage 230 VAC ± 10%
Frequency 50/60 Hz
Current 12 Amps
Input Connection C20 Plug
Power Cord (Supplied) C19 socket to local connection (13A minimum)
Pollution Degree 2
Insulation Category II
General
Dimensions cm (inches) WxDxH 60 x 85 x 132.2 (23.6 x 33.5 x 52.0)
Generator Weight Kg (lbs) 189 kg (417lb)
Shipping Weight Kg (lbs) 265.5 kg (585lb)

Page 11
Technical Specification
Genius 3020
Environment
Minimum Operating Ambient Temperature 5°C (41°F)
Maximum Operating Ambient Temperature 35°C (95°F)
Maximum Altitude 2000 m
Maximum Relative Humidity 80% Non-Condensing
Minimum Storage Temperature* -20°C (-4°F)
Maximum Storage Temperature* 60°C (140°F)
Generator Outlets
Maximum Gas Output Pressure 2 x independant outlet of 6.9 bar (100 psi)
Maximum Outlet Flow Rate 2 x independant outlet of 32 L/min (1.13 cfm)
Start-Up Time 30 mins
Particles <0.01µm
Phthalates NONE
Suspended Liquids NONE
Gas Outlets 2 x ¼” BSPP
Drain Outlets 1 x ¼” BSPP
Pressure Gauges 2
Electrical Requirements
Voltage 230 VAC ± 10%
Frequency 50/60 Hz
Current 12 Amps
Input Connection C20 Plug
Power Cord (Supplied) C19 socket to local connection (13A minimum)
Pollution Degree 2
Insulation Category II
General
Dimensions cm (inches) WxDxH 60 x 85 x 132.2 (23.6 x 33.5 x 52.0)
Generator Weight Kg (lbs) 189 kg (417lb)
Shipping Weight Kg (lbs) 265.5 kg (585lb)

Page 12
Technical Specification
Genius 3022
Environment
Minimum Operating Ambient Temperature 5°C (41°F)
Maximum Operating Ambient Temperature 35°C (95°F)
Maximum Altitude 2000 m
Maximum Relative Humidity 80% Non-Condensing
Minimum Storage Temperature* -20°C (-4°F)
Maximum Storage Temperature* 60°C (140°F)
Generator Outlets
Maximum Gas Output Pressure 2 x independant outlet of 8.1 bar (116 psi)
Maximum Outlet Flow Rate 2 x independant outlet of 32 L/min (1.13 cfm)
Start-Up Time 30 mins
Particles <0.01µm
Phthalates NONE
Suspended Liquids NONE
Gas Outlets 2 x ¼” BSPP
Drain Outlets 1 x ¼” BSPP
Pressure Gauges 2
Electrical Requirements
Voltage 230 VAC ± 10%
Frequency 50/60 Hz
Current 12 Amps
Input Connection C20 Plug
Power Cord (Supplied) C19 socket to local connection (13A minimum)
Pollution Degree 2
Insulation Category II
General
Dimensions cm (inches) WxDxH 60 x 85 x 132.2 (23.6 x 33.5 x 52.0)
Generator Weight Kg (lbs) 189 kg (417lb)
Shipping Weight Kg (lbs) 265.5 kg (585lb)

Page 13
Unpacking
Although Peak Scientific takes every precaution with safe transit and packaging, it is
advisable to fully inspect the unit for any sign of transit damage.
Check ‘SHOCKWATCH’ and ‘TIP-N-TELL’ labels for signs of rough handling prior to
unpacking
Any damage should be reported immediately to the carrier and Peak Scientific or the
Peak Partner from where the unit was purchased.
Follow the unpacking instructions posted on the side of the crate. It will require two
people to remove the unit from the shipping crate and to manoeuvre the generator to
the desired location.
Please save the product packaging for storage or future shipment of the generator.
Note: Included with the generator is a “Fittings Kit” containing mains power leads for
UK, EU & US and also all the required fittings and warranty registration card. Be careful
not to discard these with the packaging.
Page 13

Page 14
Fittings Kit Contents
Supplied in the Fittings Kit are all the fittings required to connect the generator to the
application. The contents of the Fittings Kit are as follows:
1. 6mm Teflon Tubing x 3m*
2. ¼” Teflon Tubing x 3m*
3. 6mm PE Tubing x 3m
4. ¼” Compression Fitting x 1**
5. 6mm Push Fit Fitting x 2**
6. Flow Control Silencer x 1***
7. UK Mains Power Cable x 1
8. EU Mains Power Cable x 1
9. US Mains Power Cable 230v x 1
10. 8mm Hex Key x 1
* x6m in Genius 3020/22
** x3 in Genius 3020/22
*** x2 in Genius 3020/22
All of the generators output ports are located on the output panel at the rear of the
unit.

Page 15
Installation
Generator Environment
The generator is designed for indoor use only. It should be installed adjacent to
the application(s) it is supplying. If this is not convenient then the unit can be sited
elsewhere, however, consideration should be made of the lengths of pipe runs as
pressure drops can result from extended runs of pipe.
Performance of the generator (like all sophisticated equipment) is affected by ambient
conditions. Note should also be taken to the proximity of Air Conditioning outlets.
These can sometimes give rise to “pockets” of air with high relative humidity. Operation
of the unit within such a pocket could adversely affect its performance. Consideration
should also be given to the air flow around the unit. It is recommended that an air gap
of 75mm (3”) should be maintained down both sides and at the rear of the unit. Please
refer to the drawing below for the general dimensions of the unit.
Minimum Operating Ambient Temperature: 5 °C (41 °F)
Maximum Operating Ambient Temperature: 35 °C (95 °F)

Page 16
Generator Overview
General Dimensions
The generator must always be placed on a flat, level surface. Failure to
do so will affect the performance of the generator.
WARNING
600 mm / 23.6” 850 mm / 33.5”
1322 mm / 52"

Page 17
3010/3013 Rear Connections
¼" Compression Fitting
6mm Push-Fit Fitting
Mains Cable

Page 18
3020/3022 Rear Connections
¼" Compression Fitting
6mm Push-Fit Fitting
Mains Cable

Page 19
WARNING
Electrical Connection
Connect the generator to an appropriate 110 or 230 volt single-phase supply, refer to
the generator serial plate for input specification and ensure your supply matches the
requirements.
If the appropriate power cord is not supplied; a new plug, rated to at least 12 amps, can
be fitted by a qualified electrician.
This unit is classified as SAFETY CLASS 1. THIS UNIT MUST BE
EARTHED. Before connecting the unit to the mains supply, please
check the information on the serial plate. The mains supply must be of
the stated AC voltage and frequency.
EARTH/GROUND (E):- Green & Yellow or Green
LIVE (L):- Brown or Black
Neutral (N):- Blue or White
Electrical requirements for 230V generators is 195V - 253V 50/60Hz. For 195V - 219V a
06-3210 Dual Tap Transformer is required.
If the equipment is used in a manner not specified by the manufacturer,
the protection provided by the equipment maybe impaired.
WARNING

Page 20
Start-Up Sequence
Before the Generator is connected to the application, the Generator
should be operated in isolation (i.e. not connected to the application)
for thirty minutes. This is to ensure any impurities present are purged
from the system. Failure to do this may harm the application.
Before re-connecting the Generator to the mains and switching it on for the isolation
run, it is necessary to fit the silencers (supplied in the fittings kit) to the outlet ports of
the output panel as shown below.
Once this is done, the Generator can be re-connected to the mains and switched on.
Pressure will start to build in the internal storage tanks which can be monitored by
watching the output pressure gauges on the front panel. This will climb to the factory
set pressure as noted in the specifications.
Once this pressure is reached, the compressors will continue to run until the internal
tank upper pressure limit is reached and the compressor has run for a period of at least
two and a half minutes.
The compressors will then rest until the internal tank lower pressure limits is reached.
Once this limit is reached the compressors will switch back on again. This compressor
cycling is normal and will continue throughout the operation of the Generator.
When the system has been operated for a period of 30 minutes, all the internal pipe-
work and storage tanks will have been purged with nitrogen.
Once purged, and the tubes can be connected at the rear of the unit. The generator
should be allowed to run for 1 hour to allow the gas to reach purity.
CAUTION