Rigaku KT-100 User manual

KT-100™ Handheld LIBS Analyzer
User Manual
Document Revision B
May 26, 2016

Copyright © 2016 Rigaku Analytical Devices, Inc.
All rights reserved. Neither this publication nor any part thereof can be copied, photocopied, reproduced,
translated, or converted to any electronic or machine-readable form in whole or in part without prior written
approval of Rigaku Analytical Devices, Inc. This documentation is furnished under license and can be used or
copied only in accordance with the terms of such license.
The content of this documentation is furnished for informational use only, is subject to change without notice, and
does not represent a commitment or guaranty by Rigaku Analytical Devices, Inc. The statements, configurations,
technical data, and recommendations in this document are believed to be accurate and reliable as of the time of
publication, but Rigaku Analytical Devices, Inc. assumes no responsibility or liability for any errors or inaccuracies
that may appear in this documentation. DOCUMENTATION IS PROVIDED "AS IS" AND ALL EXPRESS OR IMPLIED
CONDITIONS, REPRESENTATIONS AND WARRANTIES, INCLUDING ANY IMPLIED WARRANTY OF MERCHANTABILITY,
FITNESS FOR A PARTICULAR PURPOSE OR NONINFRINGEMENT, ARE DISCLAIMED. UNDER NO CIRCUMSTANCES,
INCLUDING BUT NOT LIMITED TO RIGAKU ANALYTICAL DEVICES’ NEGLIGENCE, SHALL RIGAKU ANALYTICAL DEVICES
BE LIABLE FOR ANY CONSEQUENTIAL, DIRECT, INCIDENTAL, INDIRECT, PUNITIVE, OR SPECIAL DAMAGES RELATED
TO (A) THE USE OF, (B) THE INABILITY TO USE, OR (C) ERRORS OR OMISSIONS IN THE CONTENTS AND FUNCTIONS
OF THIS SITE, EVEN IF RIGAKU ANALYTICAL DEVICES OR AN AUTHORIZED REPRESENTATIVE THEREOF HAS BEEN
ADVISED OF THE POSSIBILITY OF SUCH DAMAGES.
KT-100, Katana, BLADE, and QuickID are trademarks of Rigaku Analytical Devices, Inc. All other trademarks are the
property of their respective holders.
Software version 1.1.0.0 and higher

Contents i
Contents
Preface ...............................................................................................................1
Document Overview ............................................................................................................ 1
Document Conventions........................................................................................................ 2
Safety and Compliance Notices for the KT-100 Analyzer ...................................................... 3
Laser Safety and Compliance ................................................................................................................ 3
General Safety and Compliance............................................................................................................ 5
Safe Operation Notices ......................................................................................................................... 6
Contacting Rigaku Analytical Devices ................................................................................... 7
Introduction........................................................................................................8
Overview of the KT-100 Analyzer ......................................................................................... 8
Top View ............................................................................................................................................... 9
Front Left View...................................................................................................................................... 9
Front Right View ................................................................................................................................. 10
Power and Micro USB Connectors...................................................................................................... 10
Accessories.......................................................................................................................................... 11
Carrying Your Analyzer....................................................................................................... 12
Understanding LIBS Spectroscopy ...................................................................................... 12
What You Can Do with the KT-100 Analyzer....................................................................... 13
Starting the KT-100 Analyzer.............................................................................14
Installing or Removing Batteries ........................................................................................ 14
Opening the Battery Compartment Door ........................................................................................... 14
Installing the Battery........................................................................................................................... 16
Removing the Battery ......................................................................................................................... 17
Closing the Battery Compartment Door ............................................................................................. 18
Charging Batteries.............................................................................................................. 19
Charging Batteries in the Docking Station .......................................................................................... 19
Charging Installed Batteries with the Docking Station ....................................................................... 20
Charging Installed Batteries with the AC Adapter .............................................................................. 20
Powering On ...................................................................................................................... 21
Logging In and Entering Passcodes ..................................................................................... 22
Correcting Passcodes ......................................................................................................... 23

Contents ii
Reviewing and Accepting the Laser Warning ...................................................................... 24
Responding to the Power Down Warning........................................................................... 26
Powering Off...................................................................................................................... 26
Powering Off with Touchscreen Controls ........................................................................................... 27
Powering Off with Keypad Hard Buttons............................................................................................ 27
Using Analyzer Controls ..................................................................................................... 28
Using the Touchscreen........................................................................................................................ 28
Using the Keypad ................................................................................................................................ 28
Understanding the Touchscreen and Keypad ..................................................................... 29
Accessing Main Menu Features.......................................................................................... 31
Using Common On-screen Controls.................................................................................... 31
Logging Out........................................................................................................................ 32
Operating the KT-100 Analyzer .........................................................................33
Running a System Check .................................................................................................... 33
Preparing a Sample ............................................................................................................ 35
Aligning a Sample............................................................................................................... 35
Analyzing a Sample ............................................................................................................ 36
Using the Drill Down Feature to Analyze Dirty Samples ..................................................... 37
Including Optional Information in Results .......................................................................... 38
Accessing the Data Entry Menu.......................................................................................................... 39
Adding a Sample ID to a Result........................................................................................................... 40
Adding Lot, Purchase Order, and Vendor Information to a Result..................................................... 42
Adding a File Tag to a Result Filename ............................................................................................... 43
Viewing Results.................................................................................................................. 45
Selecting a Result View ....................................................................................................................... 46
Browsing the Results List .................................................................................................................... 51
Filtering the Results List...................................................................................................................... 53
Routine Cleaning of Your Analyzer ..................................................................................... 57
Managing Communications................................................................................................ 57
Accessing Communications Settings................................................................................................... 57
Using Usb ............................................................................................................................................ 58
Using Wifi............................................................................................................................................ 59
Accessing Bluetooth............................................................................................................................ 64
Configuring the KT-100 Analyzer .......................................................................65

Contents iii
Accessing Analyzer Settings................................................................................................ 65
Customizing Results Settings.............................................................................................. 67
Accessing Results Settings .................................................................................................................. 67
Selecting the Grade Specs Naming System for Your Region .............................................................. 68
Setting the Alloy Match Criteria.......................................................................................................... 69
Specifying the Number of Matches Displayed.................................................................................... 70
Configuring Cal Factors ....................................................................................................................... 71
Optimizing Instrument Setup ............................................................................................. 80
Accessing the Instrument Setup Menu............................................................................................... 80
Adjusting Date and Time Settings....................................................................................................... 81
Choosing the Analyzer’s Language ..................................................................................................... 87
Specifying Functionality of Quick Launch Keys ................................................................................... 88
Syncing Results to a Personal Computer ...........................................................91
Connecting a KT-100 Analyzer to Local PCs or Network Workstations ................................ 91
Using USB Connections....................................................................................................................... 91
Using Wifi Connections....................................................................................................................... 92
Logging onto KT-100 Analyzers with a Web Browser ......................................................................... 92
Viewing Analyzer Results on a Web Browser...................................................................... 94
Archiving Analyzer Results ................................................................................................. 95
Downloading System Logs for Technical Support ............................................................... 98
Basic Troubleshooting.....................................................................................100
Viewing Analyzer Status Information ............................................................................... 100
Verifying the Analyzer Serial Number .............................................................................. 101
Appendix A. Operating Specifications .........................................................102
Optical Specifications ....................................................................................................... 102
Physical Specifications ..................................................................................................... 102
Electronics and Data Processing Specifications................................................................. 102
Environmental Specifications ........................................................................................... 102
Electrical Specifications............................................................. Error! Bookmark not defined.
Appendix B. Statements of Compliance ......................................................104
IEC/EN 60529 International Protection Rating.................................................................. 104
Certificate of Conformity.................................................................................................. 104

Contents iv
Appendix C. Regulatory Statements............................................................105
FCC and Industry Canada Statements............................................................................... 105
Export Regulation Statements.......................................................................................... 105
EC Statements.................................................................................................................. 106
European WEEE Recycling and RoHS ................................................................................ 106
WEEE Compliance ............................................................................................................................. 106
WEEE Konformität ............................................................................................................................ 106
Conformité DEEE............................................................................................................................... 107

Preface 1
Preface
This user manual provides instructions for operating and taking care of the Rigaku Analytical Devices
(RAD) KT-100 Handheld LIBS Analyzer (KT-100), which uses Laser Induced Breakdown Spectroscopy
(LIBS) to identify a wide range of ferrous and non-ferrous metals and alloys. This section includes:
•Document Overview
•Document Conventions
•Safety and Compliance Notices for the KT-100 Analyzer
•Contacting Rigaku Analytical Devices
Document Overview
This manual tells operators and owners with various levels of experience how to operate, maintain, and
configure the KT-100 analyzer. Table 1 summarizes the experience and responsibilities of these users.
Table 1. Audiences
Audiences Experience Levels Responsibilities
Operators New or limited users •Preparing samples
•Analyzing samples
•Viewing results
•Maintaining analyzer
•Adding Sample IDs or other search
markers to results
Owners Expert users •Configuring analyzer
•Archiving analyzer data
Table 2 provides an outline of the manual and lists likely audiences and types of information in each
section.
Table 2. Document Overview
These sections… Provide… With information about…
Introduction All users •Finding analyzer features
•Understanding LIBS spectroscopy
•Ways of using the analyzer
Starting the KT-100 Analyzer All users •Performing basic procedures
Operating the KT-100 Analyzer Operators •Preparing and analyzing samples
•Viewing results
•Maintaining the analyzer
•Using the digital camera
Configuring the KT-100 Analyzer Owners •Setting up the analyzer
•Configuring analyzer results

Preface 2
These sections… Provide… With information about…
Syncing Results to a Personal Computer Owners •Connecting to analyzers with PCs and network
workstations
•Viewing results data on PCs and network
workstations
•Archiving analyzer data on PCs and network
workstations
•Downloading System Logs for technical support.
Basic Troubleshooting All users •Collecting customer support information
Appendix A: Operating Specifications All users •Analyzer specifications
Appendix B: Statements of Compliance Owners •Compliance with safety requirements
Appendix C: Regulatory Statements Owners •Compliance with regulatory requirements
Document Conventions
Table 3 lists the document conventions in this user manual.
Table 3. Document Conventions
Convention Purpose
LASER CAUTION notices highlight hazards to humans caused by the integrated Class
3B laser. Each laser caution is accompanied by an appropriate laser CAUTION symbol.
If the listed precautions are not followed, injury to people can occur.
CAUTION notices highlight hazards to humans, property, or the environment. Each
CAUTION notice is accompanied by an appropriate CAUTION symbol. If listed
precautions are not followed, injury to people or damage to property, equipment, or
the environment can occur.
Important:
Important notices highlight information that either is necessary for optimal
performance of the system or is critical to prevent:
•Damage to software
•Loss of data
•Invalid test results
If listed procedures are not followed, data integrity may be affected.
Note:
Note:
Highlights tips for performing procedures and provides information of general
interest.

Preface 3
Convention Purpose
Bold
Is used for:
•Screens, dialogs, dialog items, menus, controls, buttons, fields, and software controls.
For example:
Select (Analyze).
•Named hardware items. For example:
On the keypad, press the Main hard button to display the Main menu.
Italics
Are used for:
•Emphasis. For example:
Do not move your analyzer while analyzing samples.
•Terms that the text defines or explains. For example:
The Alloy Match Criteria (AMC) setting specifies the threshold above which the KT-100
analyzer returns matching results.
•Titles of book and manuals. For example:
For more information, see the Quick Start Guide.
Safety and Compliance Notices for the KT-100 Analyzer
The following sections provide the safety and compliance notices for safely and effectively using the KT-
100 analyzer in facilities, warehouses, and recycling yards. Please read these sections before operating
your analyzer.
This analyzer uses Class 3B lasers. Consequently, before setting up or operating this analyzer and
its accessories:
Read the sections “Laser Safety and Compliance,” “General Safety and Compliance,” and “Safe
Operation Notices”.
Complete appropriate training about your organization’s procedures and policies for using this
analyzer on both known and unknown samples.
Ensure that your KT-100 analyzer is set up correctly for analysis of the samples you are testing.
Laser Safety and Compliance
This section lists laser-specific safety and compliance notices for operating your analyzer.
This analyzer is certified as a Class 3B laser product to the requirements of the U.S. Federal
Product Performance Standard for Laser Products contained in the regulations of 21 CFR Sub-
Chapter “J” except for deviations pursuant to Department of Health and Human Services issued
Laser Notices. The KT-100 analyzer also complies with IEC 60825-1 Ed. 3 (2014)
.

Preface 4
When analyzing, each KT-100 analyzer uses a laser-emitting diode to produce a laser beam of
specific properties for analyzing samples. Table 4 lists laser properties of the KT-100 analyzer.
Table 4. Laser Properties for the KT-100 Analyzer
Properties KT-100
Max power 150 uJ
Frequency 1064 nm
Repetition frequency 150 Hz
Beam divergence 34.6 mrad
Pulse Duration 1 ns
AEL Class 3B
MPE 962.2 W/m2
NOHD 6.34 in. (16.1 cm)
Laser warning labels
This label marks position of the laser warning indicator
(see Figure 1). When the indicator is lit and red, the laser
is active. When the indicator is not lit, the laser is not
active.
This label is located by the analyzer’s trigger (see Figure
3) It provides information about properties of the
analyzer’s laser.
CAUTION: Exposure to levels of laser energy greater than the maximum permissible exposure
(MPE) can harm the eye. MPE for this analyzer is 962.2 W/m2. The laser energy must travel a
minimum distance of 6.34 inches (16.1 cm) before its concentration is lower than the MPE. This
distance is defined as the hazard zone. With proper use, exposure to levels above the MPE can
be avoided. Avoid exposure to the laser beam.
CAUTION: Because exposure to Class 3B laser energy can be hazardous, avoid exposure to the
beam. In addition, avoid exposure to specular, or mirror-like, reflections. Never point the
analyzer at anyone.
CAUTION: If your workplace does not have established safety standards or requirements, consult
both the American National Standard ANSI Z136.1 for policies about the safe use of lasers and
the International Standard IEC 60825-14 for information about identifying and controlling
hazards of laser use.
CAUTION:Calculations performed in accordance with the recommended practices of ANSI
Z136.1 and IEC 60825-1 give a Nominal Ocular Hazard Distance (NOHD) of approximately 6.34
inches (16.1 cm) from the focal point of the lens and an estimated optical density (OD) greater
than 2 for laser safety eyewear.