Teledyne Analytical Instruments 3110XL User manual

Teledyne Analytical Instruments
OPERATING INSTRUCTIONS FOR
Model 3110XL
Portable Trace
Oxygen Analyzer
DANGER
Toxic gases and or flammable liquids may be present in this monitoring system.
Personal protective equipment may be required when servicing this instrument.
Hazardous voltages exist on certain components internally which may persist
for a time even after the power is turned off and disconnected.
Only authorized personnel should conduct maintenance and/or servicing.
Before conducting any maintenance or servicing, consult with authorized
supervisor/manager.
P/N M3110XL
5/15/15

Use and Disclosure of Data
Information contained herein is classified as EAR99 under the
U.S. Export Administration Regulations.
Export, reexport or diversion contrary to U.S. law is prohibited.

Model 3110XL
Teledyne Analytical Instruments ii
Copyright © 2015 Teledyne Instruments/ Analytical Instruments
All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed,
stored in a retrieval system, or translated into any other language or computer language in
whole or in part, in any form or by any means, whether it be electronic, mechanical,
magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne
Instruments/Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 91748.
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us free from
defects of material and of construction, and that our liability shall be limited to replacing or
repairing at our factory (without charge, except for transportation), or at customer plant at
our option, any material or construction in which defects become apparent within one year
from the date of shipment, except in cases where quotations or acknowledgements provide
for a shorter period. Components manufactured by others bear the warranty of their
manufacturer. This warranty does not cover defects caused by wear, accident, misuse,
neglect or repairs other than those performed by TI/AI or an authorized service center. We
assume no liability for direct or indirect damages of any kind and the purchaser by the
acceptance of the equipment will assume all liability for any damage which may result from
its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus,
and to make any alterations in the dimensions, shape or weight of any parts, in so far as
such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which
valuable data can be gathered. The information provided by the instrument may assist the user
in eliminating potential hazards caused by his process; however, it is essential that all
personnel involved in the use of the instrument or its interface, with the process being
measured, be properly trained in the process itself, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process
conditions. While this instrument may be able to provide early warning of imminent
danger, it has no control over process conditions, and it can be misused. In particular, any
alarm or control systems installed must be tested and understood, both as to how they
operate and as to how they can be defeated. Any safeguards required such as locks, labels,
or redundancy, must be provided by the user or specifically requested of TI/AI at the time
the order is placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser
is responsible for the training of personnel, for providing hazard warning methods and
instrumentation per the appropriate standards, and for ensuring that hazard warning devices
and instrumentation are maintained and operated properly.
Teledyne Instruments/ Analytical Instruments, the manufacturer of this instrument, cannot
accept responsibility for conditions beyond its knowledge and control. No statement
expressed or implied by this document or any information disseminated by the
manufacturer or its agents, is to be construed as a warranty of adequate safety control under
the user’s process conditions.

Portable Trace Oxygen Analyzer
Teledyne Analytical Instruments iii
Specific Model Information
The instrument for which this manual was supplied may
incorporate one or more options not supplied in the standard instrument.
Commonly available options are listed below, with check boxes. Any
that are incorporated in the instrument for which this manual is supplied
are indicated by a check mark in the box.
Instrument Serial Number: _______________________
Sensor Options Available for the Instrument with the Above Serial
Number:
 B-2CXL (Default)
 A-2CXL
Other options Included in the Instrument with the Above Serial
Number:
 Cell Block:
 Nylon cell block
 316 SS cell block
 Sample System:
 Standard sample system
 Stainless steel with glass flowmeter
 Stainless steel with regulator and glass flowmeter
 Data Logger Option
 Quick Disconnect Fittings

Model 3110XL
Teledyne Analytical Instruments iv
Safety Messages
Your safety and the safety of others is very important. We have
provided many important safety messages in this manual. Please read
these messages carefully.
A safety message alerts you to potential hazards that could hurt you
or others. Each safety message is associated with a safety alert symbol.
These symbols are found in the manual and inside the instrument. The
definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the instructions
for details on the specific danger. These cautions warn of
specific procedures which if not followed could cause bodily
Injury and/or damage the instrument.
CAUTION: HOT SURFACE WARNING: This warning is
specific to heated components within the instrument. Failure
to heed the warning could result in serious burns to skin and
underlying tissue.
WARNING: ELECTRICAL SHOCK HAZARD: Dangerous
voltages appear within this instrument. This warning is
specific to an electrical hazard existing at or nearby the
component or procedure under discussion. Failure to heed this
warning could result in injury and/or death from
electrocution.
Technician Symbol:All operations marked with this symbol
are to be performed by qualified maintenance personnel only.
NOTE: Additional information and comments regarding a
specific component or procedure are highlighted in the form
of a note.
CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE
PURPOSE AND IN THE MANNER DESCRIBED IN
THIS MANUAL.
IF YOU USE THE ANALYZER IN A MANNER OTHER
THAN THAT FOR WHICH IT WAS INTENDED,
UNPREDICTABLE BEHAVIOR COULD RESULT
No
Symbol

Portable Trace Oxygen Analyzer
Teledyne Analytical Instruments v
POSSIBLY ACCOMPANIED WITH HAZARDOUS
CONSEQUENCES.
This manual provides information designed to guide you through
the installation, calibration operation and maintenance of your new
analyzer. Please read this manual and keep it available.
Occasionally, some instruments are customized for a particular
application or features and/or options added per customer requests.
Please check the front of this manual for any additional information in
the form of an Addendum which discusses specific information,
procedures, cautions and warnings that may be peculiar to your
instrument.
Manuals do get lost. Additional manuals can be obtained from TAI
at the address given in the Appendix. Some of our manuals are available
in electronic form via the internet. Please visit our website at:
www.teledyne-ai.com.

Model 3110XL
Teledyne Analytical Instruments vi
Table of Contents
Specific Model Information ......................................................... iii
Safety Messages .......................................................................... iv
List of Figures ............................................................................ viii
Introduction ................................................................................... 1
1.1 Introduction 1
1.2 Features 2
1.3 Method of Analysis 3
1.4 Micro-Fuel Cell 4
1.4.1 Cell Warranty 4
1.5 Accuracy and Response 5
1.6 Signal Output 5
1.7 Range 5
1.8 Compact Packaging 5
Installation ..................................................................................... 7
2.1 Charging the Batteries 7
2.2 Gas Connections 8
2.3 Sensor Installation 9
2.3.1 Installing the Trace Sensor 10
2.4 Calibration 10
2.4.1 Calibration Using Air for Percent Analysis 10
2.4.2 Calibration Procedure for Trace Analysis 11
2.4.3 Bleeding the Regulator and Purging the Gas Line 12
2.5 Set the Sample Flowrate 13
2.6 External Signal 13
Operation ..................................................................................... 15
3.1 Front Panel Interface 15
3.1.1 ENTER Key 15
3.1.2 ESCAPE Key 16
3.1.3 UP/DOWN Keys 16

Portable Trace Oxygen Analyzer
Teledyne Analytical Instruments vii
3.2 Operation and Setup Screens and Menus 16
3.2.1 POWER ON Screen 17
3.2.2 HOME Screen 18
3.2.3 DATE Screen 18
3.2.4 TIME Screen 19
3.2.5 AO Rng Screen 19
3.2.6 SPAN VALUE Screen 20
3.2.7 SPAN Screen 21
3.2.8 Filter Screen 22
3.2.9 LOG INTV Screen (Optional) 22
3.2.10 LOG RESET & START Screen (Optional) 23
3.2.11 LOG TRANSMIT Screen 24
3.2.12 POWER DOWN Screen 25
Maintenance & Troubleshooting ................................................ 27
4.1 Routine Maintenance 27
4.2 Opening the Instrument Case 27
4.3 Replacing the Battery 27
4.4 Battery Power Supply Service 28
4.5 Cell Replacement 29
4.6 Cell Warranty 30
4.7 Temperature Compensation 30
4.8 Leak Testing 32
Appendix ...................................................................................... 33
A.1 Specifications 33
A.2 Spare Parts List 34

Model 3110XL
Teledyne Analytical Instruments viii
List of Figures
Figure 1-1: Model 3110 Portable Trace Oxygen Analyzer .............. 2
Figure 2-1: Model 3110 Rear Panel ................................................ 8
Figure 3-1: Front Panel Keys ........................................................ 16
Figure 3-2: Available Menus and Their Sequence ........................ 17
Figure 4-1: Battery Charger Port on the Model 3110 .................... 28
Figure 4-2: Effects of CO2 on B-2 Cell Life ................................... 31

Portable Trace Oxygen Analyzer
Teledyne Analytical Instruments ix
DANGER
COMBUSTIBLE GAS USAGE
WARNING
This instrument is approved as an intrinsically safe gas
analyzer for use in a Division 1 Group A-D hazardous area.
Note that this approval does not apply to the non-conductive
LCD window and micro-fuel cell. Also, although the analyzer
is capable of being ranged up to 25% oxygen, the approval
does not apply to oxygen exposure above 20.9%. This
approval applies only to the equipment specified and
installed in accordance with the information contained within
this manual. It is the customer's responsibility to ensure
safety especially when combustible gases are being
analyzed since the potential of gas leaks always exist.
The customer should ensure that the principles of operating
this equipment are well understood by the user. Misuse of
this product in any manner, tampering with its components,
or unauthorized substitution of any component may
adversely affect the safety of this instrument.
Since the use of this instrument is beyond the control of
Teledyne Analytical Instruments, referred as TAI, no
responsibility by TAI, its affiliates, and agents for damage or
injury from misuse or neglect of this equipment is implied or
assumed.

Portable Trace Oxygen Analyzer Introduction
Teledyne Analytical Instruments 1
Introduction
1.1 Introduction
The Teledyne Analytical Instruments (TAI) Model 3110XL
Portable Oxygen Analyzer is a portable, intrinsically safe oxygen
analyzer capable of analyzing oxygen levels from 0-2 parts per million
(ppm) oxygen to 25% oxygen (dependent on configuration). These units
are rated as intrinsically safe and may be used in a Class I, Div 1, Group
A-D hazardous environment. The instrument operates from internal
rechargeable batteries and is supplied with a universal AC charge
adapter. It features quick-disconnect fittings for sample connections and
a rugged, lightweight housing with handle. This versatile instrument can
be brought to the sample site and set up for analysis quickly and easily.
Because of the intrinsically safe design, the instrument can be employed
even in hazardous environments without compromise once calibrated.
The Model 3110XL incorporates a large standard feature list designed
for versatile, accurate oxygen analysis for a wide range of applications.
Figure 1-1 shows the standard Model 3110XL Portable Trace Oxygen
Analyzer.
The microprocessor based Model 3110XL instrument provides one
user settable analysis range at trace sensitivities. The single user-defined
range can be set anywhere from 0-2 ppm to 0-25% oxygen.
Sample oxygen is displayed on a 2-line 20 character alphanumeric
LCD display mounted on the front panel. Four buttons are used to
interface with the instrument and access all of the analyzer features.
Sample gas is introduced and vented via a pair of quick-disconnect
fittings that feature integral shutoff valves which automatically close
when the mating male fitting is withdrawn. The fittings are an integral
part of the measuring cell manifold so that internal sample passage
volume is at an absolute minimum.

Introduction Model 3110XL
Teledyne Analytical Instruments 2
Figure 1-1: Model 3110XL Portable Trace Oxygen Analyzer
1.2 Features
This instrument is designed to be versatile analytical instrument
and to perform reliably and accurately in analyzing oxygen
concentrations in gas mixtures from low ppm levels through 25%
oxygen. The following features are standard on the Model 3110XL:
• Display: A 2-line 20 character alphanumeric LCD
on the front panel displays data and
operational information through various
screens. The contrast is adjustable for
various lighting conditions.
• Four-Button User Interface: Operation is performed using the
four front panel mounted buttons. These
buttons are used to enter data, select items
and move through operational screens that
appear on the display.
• Universal AC Charge Adapter: The batteries can be recharged
without removing them from the
instrument. The charger operates over the
range of 100-240 VAC.
Alphanumeric
LCD
Contrast
Ad
j
ustment
User Interface
Buttons
Low Battery
Indicato
r
Battery
Charging
Indicator

Portable Trace Oxygen Analyzer Introduction
Teledyne Analytical Instruments 3
• LEDs: Two front panel-mounted LEDs are used
to indicate low battery condition and when
the battery is recharging.
• Contrast Control: This feature allows the user to easily
adjust the contrast of the display for
optimum viewing under different lighting
conditions. The adjustment is made using
a front panel control dial.
• Percent of Range Voltage Output: A 0-1 VDC output is
available that represents the percentage of
the current analysis range.
• Data Logger: The optional built-in data logging feature
allows the user to specify the time interval
between data recording sets. The date,
time, and oxygen concentration readings
are stored in internal RAM at the user
specified interval. The data set can be
downloaded using the instrument’s 9-pin
serial interface.
• Real-time Clock: This feature allows the Model 3110XL to
date and time stamp the data set recorded
on the data logger. It uses a 24 hour clock.
• Quick Disconnect Fittings: Dual self-sealing quick disconnect
fittings are installed for easy sample
connections.
1.3 Method of Analysis
The sample oxygen is measured by a unique electrochemical
transducer which functions as a fuel cell; in this instance, the fuel is
oxygen. Oxygen diffusing into the cell reacts chemically to produce an
electrical current that is proportional to the oxygen concentration in the
gas phase immediately adjacent to the transducer’s sensing surface. The
linear signal produced by the transducer from the oxygen sensor is
amplified and digitized and then fed to the microprocessor. Additional
signal conditioning and temperature compensation are handled
electronically and appropriate signals are directed to the display and
output ports.

Introduction Model 3110XL
Teledyne Analytical Instruments 4
1.4 Micro-Fuel Cell
The micro-fuel cell (U.S. Pat. Nos. 3,767,552 and 3,668,101) is a
sealed electrochemical transducer with no electrolyte to change or
electrodes to clean. When the cell reaches the end of its useful life, it is
thrown away and replaced. The life of the cell is warranted by TAI (see
below).
The cell is specific for oxygen and is not sensitive to flowrate or
reducing agents such as hydrocarbons, carbon monoxide, sulfur dioxide,
etc. In the absence of oxygen, no current is produced; thus, no zeroing is
required.
1.4.1 Cell Warranty
The Class B-2CXL and A-2CXL micro-fuel cells are generally
used in the Model 3110XL. They carry a six (6) month warranty.
With regard to spare cells, service time starts when the cell is
removed from its shipping package. You should stock only one spare
cell per instrument at a time.
If a cell was working satisfactorily but ceases to function before the
warranty period expires, you will receive credit on a pro-rated basis
toward the purchase of a new cell.
If you have a warranty claim, return the cell in question to the
factory for evaluation. If it is determined that failure is due to faulty
workmanship or material, the cell will be replaced at no cost to you.
WARNING: EVIDENCE OF DAMAGE DUE TO TAMPERING OR
MISHANDLING WILL RENDER THE CELL
WARRANTY NULL AND VOID.
The Model 3110XL is rated as intrinsically safe and may be used in
a Class I, Div 1, Group A-D hazardous environments.
This safety feature does not apply when the instrument is being
charged with the 100- 240 VAC external charge adapter. The instrument
should be removed from hazardous areas when the batteries are being
charged.
Note: Do not use the analyzer when the battery level is low.

Portable Trace Oxygen Analyzer Introduction
Teledyne Analytical Instruments 5
1.5 Accuracy and Response
The Model 3110XL provides monitoring accuracies of ±2% of full
scale or ±1 ppm, whichever is greater, at constant temperature.
With a sample flowrate of 1 SCFH, a 90% response can be
achieved in 10 seconds when analyzing in the percent range. The
response time on the 3110XL is limited by the filter setting.
1.6 Signal Output
This analyzer includes a 0-1 VDC output as standard. This signal is
suitable for driving external devices that have an input impedance of
10,000 Ω or more. The signal output is available from a port on the rear
panel.
1.7 Range
The Model 3110XL has one user defined range extending from 0-2
ppm to 0-25% with a display resolution of 0.1 ppm when analyzing at
less than 1%. When measuring oxygen at levels greater than or equal to
1%, the display resolution is 0.01%.
1.8 Compact Packaging
The instrument is housed in 6 1/8" × 9 1/2" × 5 5/8" (156 × 241 ×
143mm) aluminum case that is equipped with a carrying handle and foot
pads.

Introduction Model 3110XL
Teledyne Analytical Instruments 6
BLANK PAGE

Portable Oxygen Analyzer Installation
Teledyne Analytical Instruments 7
Installation
The Model 3110XL Trace Oxygen Analyzer is designed to be
portable and easy to setup and configure. To setup the analyzer:
• Read the manual
• Charge the batteries
• Install the sample and vent gas lines
• Install the trace sensor and purge the analyzer
• Set the sample gas flowrate
• Calibrate the analyzer
2.1 Charging the Batteries
The unit is powered by two intrinsically safe rated sub-C Ni-Cd
batteries and is shipped with batteries fully charged. The batteries,
however, will require periodic recharging. For recharging, access to an
AC power source of 100 to 240 volt, 50/60 Hz will be required. The
instrument should not be recharged in a hazardous area. Connect the
universal AC charger adapter supplied with the instrument to the AC
power outlet. Plug the other end of the charger into the port on the rear
panel as shown in Figure 2-1. The green charge indicator LED should be
illuminated to indicate that the unit is charging.
To fully recharge a set of batteries will take approximately 16
hours. The instrument should not be left on the charger for longer than
20 hours nor should the charger be left attached to the instrument when
the unit is not charging. The Model 3110XL cannot be operated while
the battery charger is attached.
CAUTION: DO NOT CHARGE THE BATTERY IN A HAZARDOUS
AREA. THE INTRINSICALLY SAFE CLASSIFICATION
OF THIS INSTRUMENT DOES NOT APPLY WHEN
THE CHARGER IS ATTACHED TO THE
INSTRUMENT. REMOVE THE INSTRUMENT TO A
NON-HAZARDOUS AREA BEFORE CONNECTING
THE BATTERY CHARGER TO THE INSTRUMENT.
The unit can operate continuously for approximately 4 days on a set
of fully charged batteries. If more frequent charging is required, the

Installation Model 3110XL
Teledyne Analytical Instruments 8
batteries are approaching the end of their useful life and should be
replaced. See Battery Replacement in Section 4.3 of this manual.
A low battery condition is indicated by a blinking red Low Battery
LED on the front panel. This will also cause the display to flicker along
with the blinking LED due to the power drain and low battery condition.
At this point the unit should be removed from service and the batteries
recharged.
Figure 2-1: Model 3110XL Rear Panel
2.2 Gas Connections
The customer must provide a means of controlling the pressure and
flowrate of the applied gas. For positive pressure applications, TAI
suggests a simple throttle valve installed in the sample line between the
sample point and the analyzer. The flowrate should be limited to
between 0.2 and 2.5 SCFH. The Sample In port is used for both sample
and calibration gas. For sampling at atmospheric pressure, connect a
pump and flow control valve downstream of the analyzer and draw
(rather than push) the sample through the instrument.
IMPORTANT: IF A PRESSURE REGULATOR IS USED, IT MUST
HAVE A METALLIC DIAPHRAGM. REGULATORS
WITH ORGANIC OR PLASTIC DIAPHRAGMS ARE
0-1 VDC
Signal Output
Battery
Charger
Data-logger
Port (optional)
Sample In
and Vent
Connections

Portable Oxygen Analyzer Installation
Teledyne Analytical Instruments 9
PERMEABLE TO OXYGEN AND, IF USED IN THE
SAMPLING SYSTEM, WILL LEAD TO HIGH OXYGEN
READINGS.
The instrument is shipped with a gas sampling and calibration kit.
This includes a 12” piece of clear tubing with a quick disconnect line for
use as a sample return or vent line plus two quick disconnect fittings to
be installed on the sample and calibration lines. These fittings employ
1/4” tube fittings which can be removed to reveal a 1/8” NPT internal
thread.
It is important in trace analysis applications to use metal for all
wetted components of the sample system. This includes gas lines, filters,
pump housing, diaphragms and any components in contact with the
sample gas. Plastic tubing and parts can be used for percent analysis but
will result in slow and inaccurate measurements at the ppm level.
There are two quick disconnect fittings installed on the rear panel
for mating the instrument with the sample or calibration gas and the vent
line. As shown in Figure 2-1, each fitting has a button which when
depressed allows the rapid detachment of the gas line from the
instrument. It is not necessary to press the button when inserting the
line, just push the male fitting into the mating connector. When a line is
removed, an internal seal prevents gas escape from the female sections
of the fitting.
Note: To avoid pressurizing the sensor, the vent line should be
installed first and removed last.
In setting up the sample lines, any valves used to set the sample
flow or filters must be located on the Sample In line. Do not place any
valves or restrictions on the vent line except as noted above for
atmospheric pressure sampling when using a downstream pump. Doing
so would increase the sensor operating pressure and result in inaccurate
analysis.
For percent measurement applications, flowmeters or rotameters
(with or without control valves) can be placed upstream of the analyzer,
i.e. on the Sample In line.
2.3 Sensor Installation
The Model 3110XL can accept various trace oxygen sensors. For
most applications the A2-C or B-2C is used. Others are available. See
page iii for the specific sensor shipped with your instrument. The
installation procedure is similar for either sensor.

Installation Model 3110XL
Teledyne Analytical Instruments 10
2.3.1 Installing the Trace Sensor
Prior to installing the trace sensor, make sure the analyzer is ready
to purge with zero gas. Connect the vent line to the analyzer then
connect the zero gas line to the sample in port. Set the zero gas flow rate
to between 0.2 and 2.5 SCFH.
Prior to using any bottled gas for calibration or purge, it is good
practice to bleed the regulator and sample line to remove any traces of
trapped air. See Section 2.4.3 Bleeding the Regulator and Purging the
Gas Line.
Once the vent and zero gas lines are attached and the lines are
properly purged, proceed to install the trace sensor as follows:
1. Remove the cell holder cap from the bottom of the
instrument.
2. Remove the outer packaging from the sensor.
3. While the sensor is still in its packaging, grip the shorting
plug through the bag and remove it from the sensor.
4. Remove the packaging and rapidly place the sensor on the
top of the cell holder cap with the concentric gold rings
facing up.
5. Screw the cell holder cap and sensor into the bottom of the
analyzer.
Note: Minimize the time the sensor is exposed to air.
6. Start the purge flow through the analyzer and purge
overnight before calibrating the unit.
2.4 Calibration
Calibration involves using a span gas to calibrate the instrument.
The proper span gas oxygen concentration depends on the range that the
instrument will be used. The correct concentration should be 80-90% of
the range used. For instance, if the analyzer is to be used on a range of 0-
2 ppm oxygen, then a span gas should be prepared with 1.6-1.8 ppm
oxygen in nitrogen. If the analyzer is going to be used on a percent
range, acceptable accuracy may be obtained using air as a span gas.
2.4.1 Calibration Using Air for Percent Analysis
Note: Calibration requires a familiarity with the operational
screens and general operation of the instrument. Read