Thermo Scientific Nicolet Summit OA User manual

Nicolet Summit OA
FTIR Spectrometer
USERGUIDE
269-346500 Revision B April 2021
© 2020 Thermo Fisher Scientific Inc. All rights reserved.

For technical support, please contact: www.thermofisher.com
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase
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For Research Use Only. This instrument or accessory is not a medical device and is not
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WARNING
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This instrument or accessory is not designed for use in an explosive
atmosphere.

Contents
Welcome 1
Conventions Used 2
Ordering Parts 3
Contacting Us 3
Get Started with Your Nicolet Summit OA Spectrometer 5
Before Your Summit Spectrometer Arrives 6
Personal Safety with the Summit Spectrometer 9
Unpack and Get Started with the Spectrometer 15
Back up and Recover Your Data 19
Install a USB Wireless Adapter 25
Understand the Spectrometer LightBar 27
View Your Data with the OMNIC Anywhere App 30
Options and Accessories 31
Install and Maintain a Purge Kit 32
Maintenance 43
Maintenance Schedule for the Summit Spectrometer 44
Align the Spectrometer Optics 46
Calibrate the Laser Frequency 47
Clean the Instrument and Crystal 48
Remove and Replace the Crystal Plate 50
Replace the Cover 52
Replace the Desiccant 56
Replace the Source 62

Welcome
The Thermo Scientific Nicolet Summit OA Fourier transform infrared (FTIR) spectrometer lets you
perform chemical analyses of sample materials by collecting data in the mid-IR spectral range. The
system has integrated verification features, a powerful software suite, and many other features that
make data collection easy. You can install optional hardware and perform several service and
maintenance procedures yourself. This document, or other provided documentation, contains the
information you need.
Be sure to read the safety guide that came with the system before operating the instrument.
Note We recommend that you maintain seal and desiccation and/or purge your instrument at all
times. Equipment damage due to failure to maintain seal and desiccation and/or purge is not
covered by the warranty. If you have questions about this requirement, please contact us.
Thermo Scientific Nicolet Summit OA Spectrometer User Guide 1
Chapter 1

Welcome
Conventions Used
Safety precautions and other important information use the following format:
DANGER
Avoid hazard. Indicates a hazardous situation which, if not avoided, will
result in serious injury or death.
WARNING
Avoid hazard. Indicates a hazardous situation which, if not avoided,
could result in serious injury or death.
CAUTION
Avoid hazard. Indicates a hazardous situation which, if not avoided,
could result in minor or moderate injury.
NOTICE
Follow instructions with this label to avoid damaging the system hardware or losing data.
Note Contains helpful supplementary information.
2 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Ordering Parts
To order parts, contact us.
If you need to send the instrument or an accessory to us for repair, call or e-mail us first for any
shipping requirements or other instructions.
Contacting Us
For Technical Support, please contact: www.thermofisher.com
Thermo Scientific Nicolet Summit OA Spectrometer User Guide 3
Welcome

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Get Started with Your Nicolet
Summit OA Spectrometer
To get started with your new Nicolet Summit OA Spectrometer, review the site and safety
requirements before the instrument arrives, unpack and setup the instrument, and connect any
additional accessories.
Before Your Summit Spectrometer Arrives 6
Personal Safety with the Summit Spectrometer 9
Unpack and Get Started with the Spectrometer 15
Back up and Recover Your Data 19
Install a USB Wireless Adapter 25
Understand the Spectrometer LightBar 27
View Your Data with the OMNIC Anywhere App 30
Thermo Scientific Nicolet Summit OA Spectrometer User Guide 5
Chapter 2

Get Started with Your Nicolet Summit OA Spectrometer
Before Your Summit Spectrometer Arrives
Prepare a suitable workspace for your spectrometer before it arrives to ensure the most accurate
data and the best long-term performance.
This article explains what to do when your spectrometer arrives and introduces environmental and
electrical factors that can influence your spectrometer’s performance. For a more comprehensive
explanation of these requirements, see the Site and Safety Information for the spectrometer.
Unpacking the Spectrometer
Before you open the box, there are two important steps to take as soon as the instrument arrives:
lCheck the exterior of the shipping box for damage
If you notice any signs of damage, contact us or your local distributor for instructions.
lAllow the spectrometer to come to room temperature
Inside the shipping box, the spectrometer is sealed in a plastic bag to keep it dry. You must allow
24 hours for the spectrometer to reach room temperature before you open the bag. If you
open the bag before the spectrometer is warmed up, condensation could form that could damage
internal optical components and cause permanent damage.
The warranty will not cover damage due to improper moving techniques or removing the sealed
plastic bag before the instrument has come to room temperature.
Preparing the Workspace
Before your instrument arrives, make sure your workspace will be able to properly support the
spectrometer. In addition to allowing enough room for the spectrometer, consider several
environmental and electrical requirements.
Spectrometer Dimensions
The Summit spectrometer requires a fairly small space, but make sure you also leave room around
the instrument so that heat can dissipate from the vents and so that you can easily access the
instrument’s ports, power , and cables.
lSummit instrument weight: 12.6 Kg (27.8 lbs)
lDimensions (W x H x D): 34 cm x 24 cm x 32 cm; (13.3 in. x 9.6 in. x 12.7 in.)
6 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Environmental Factors
The Summit spectrometer is a robust instrument designed to be used in many environments.
However, for best performance, keep it in a relatively dust-free and low-humidity environment. The
spectrometer operates reliably at temperatures between 15 and 35 °C, but for optimal performance
should be kept between 20 and 22 °C.
Humidity can cause condensation to form inside the instrument, which could damage internal
components. A few precautions can typically protect your instrument from humidity:
lMaintain the instrument’s desiccant, including while the instrument is in storage.
lAvoid rapid changes in temperature.
nKeep the instrument away from sources of cool or hot air, such as near heating and air con-
ditioning vents or large windows.
If your spectrometer will be kept in an especially humid environment, consider installing a purge gas
kit.
Electrical Requirements
Power supplied to the spectrometer must be from dedicated, uninterrupted sources and free from the
following issues:
lVoltage dropouts
lTransient spikes
lFrequency shifts
lOther line disturbances
If you suspect problems with your power, we recommend a power quality audit. Contact us or your
local electrical authority for more information.
Electrical Service Specifications
The following table lists specifications for electrical service. Contact our service representative in
your area if you have questions about the requirements.
Requirements Specification
Input Current 1.5 A Max
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Get Started with Your Nicolet Summit OA Spectrometer
Requirements Specification
Input Voltage 100 to 240 VAC
Line Frequency 50 to 60
Line Disturbances Sags, surges, or other line disturbances must not exceed 10% of input
voltage
Noise Less than 2 V (common mode)
Less than 20 V (normal mode)
8 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Personal Safety with the Summit
Spectrometer
While the Nicolet Summit OA Spectrometer is designed to be a safe instrument, you should take a
few precautions to protect yourself from potential hazards that can arise during normal use and
maintenance.
CAUTION
This guide is an introduction to potential dangers that you should be
aware of, but it is not a comprehensive guide. Before using the instru-
ment, see the Site and Safety Information for the spectrometer for a full
description of these potential hazards.
Potential Hazards during Normal Use
During normal use, most hazards are due to following sources:
lPotentially hazardous samples and solvents
lExposure to zinc selenide (ZnSe)
lParts of the spectrometer that are hot or emit heat
lThe instrument’s laser
You can avoid possibly harming yourself or damaging the instrument by understanding potential
hazards and by taking a few precautions.
Hazardous Samples and Solvents
Take special precautions if you are using or plan to measure potentially hazardous samples or
solvents, such as pressurized gases or corrosive or flammable solvents.
USE PROPER VENTILATION
There are no special ventilation requirements for your spectrometer, but you may need additional
ventilation during certain types of analysis. Ensure that you have proper ventilation if you will be
analyzing highly toxic samples, dissolving your samples in solvents that may interact with the infrared
source, or sampling flammable gases.
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Get Started with Your Nicolet Summit OA Spectrometer
The pyrolysis of solvents containing halogenated hydrocarbons may produce hydrochloric acid (HCl),
hydroflouric acic (HF), or phosgene (COCl2).
WARNING
Avoid toxic inhalation. Hydrochloric acid, hydrofluoric acid, and phos-
gene are highly toxic. If you are using solvents containing halogenated
hydrocarbons, ensure your work area is properly ventilated.
VOLATILE AND FLAMMABLE SOLVENTS
The infrared source inside the spectrometer can ignite flammable and volatile samples and solvents.
Take the following actions when working with samples and solvents that are flammable:
lWork with the sample compartment windows installed.
lEnsure that the workspace is properly ventilated with an active venting system that is free of
spark or other sources of ignition and that prevents flammable vapors from collecting in the atmo-
sphere surrounding the instrument.
lDo not leave flammable solvents or samples near the instrument.
lDo not leave flammable solvents or samples in the sample compartment for longer than neces-
sary.
lPurge the spectrometer with clean, dry air or nitrogen.
CORROSIVE SOLVENTS
Solvents that produce HCl or HF vapors in the sample compartment may severely damage the
system. If you are using halogenated solvents, purge the instrument with clean, dry air or nitrogen.
NOTICE
Your warranty does not cover equipment damage that is due to a failure to purge the instrument.
BIOHAZARD OR RADIOACTIVE MATERIALS AND INFECTIOUS AGENTS
Biological samples, such as tissues, body fluids, infectious agents, and blood, have the potential to
transmit infectious diseases. Follow your organization’s Biosafety Program protocols for working with
potentially infectious materials.
10 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Toxic Materials
The Nicolet Summit OA spectrometer includes a zinc selenide (ZnSe) ATR Crystal, and other Summit
instruments may use the optional ZnSe sample compartment windows.
WARNING
Avoid toxic inhalation and ingestion.
Zinc selenide (ZnSe) is toxic. Refer to the manufacturer's ZnSe Safety Data
Sheet at www.specac.com for handling and exposure controls.
Sources of Heat
Parts of the spectrometer can become quite hot during normal use. Be careful around the
spectrometer’s infrared source and the vents.
The outward facing surface of the infrared source is located on the bottom of the instrument and can
become quite hot. Do not touch the underside of the instrument during operation or shortly after use.
The spectrometer’s vent is located on the left side of the instrument. During normal use, the
spectrometer dissipates hot air from internal components to the area outside the spectrometer
through these vents. Leave enough space around the instrument vents for hot air to dissipate.
Laser and Optical Safety
You will never be exposed to unsafe levels of laser radiation during normal use of the spectrometer. If
the cover is removed during a service procedure, you may need to take special precautions, such as
using protective eyewear. Your service person will notify you if this is necessary.
WARNING
Avoid personal injury.
Never stare into the laser beam or at its reflection. Never tamper with the laser,
even if you are replacing a defective laser, or you could be exposed to laser
light or to high voltage.
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Get Started with Your Nicolet Summit OA Spectrometer
Potential Hazards during Maintenance
You may be exposed to different hazards while performing maintenance on the instrument than you
would encounter during normal use. During maintenance, the primary hazards involve purging the
instrument and working with the instrument’s internal components.
Purging the Instrument
In especially humid environments, we recommend installing a source of clean, dry air or nitrogen to
purge the spectrometer. Purging the instrument can help protect internal optical components from
damage caused by a moist environment or corrosive solvents, and it can ensure more accurate
results.
See "Install and Maintain a Purge Kit" for details on purchasing and installing a purge kit for your
spectrometer.
DANGER
Avoid fire and explosion hazard.
lUse only dried air or nitrogen to purge your spectrometer.
lNever use a flammable, combustible, or toxic gas to purge this instrument.
The purge gas must be free of oil and other reactive materials. Heat from
the source or from laser absorption may ignite flammable gases or reactive
materials in the purge gas.
Working with Internal Components
Typically, there should be no reason for you to remove the instrument cover or attempt to replace
internal components. However, if you need to remove the cover for maintenance, be aware that you
risk being shocked, burned, and exposed to laser light.
CAUTION
Avoid shock hazard.
Even after this instrument has been disconnected from all voltage sources,
capacitors may remain charged for up to 30 seconds and can cause an
electrical shock.
12 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

CAUTION
Avoid burn hazard.
Internal components, especially the infrared source, can become extremely
hot during normal operation. Turn off the instrument and wait at least 10
minutes before replacing any components.
WARNING
Avoid personal injury.
lNever stare into the laser beam or at its reflection. Never tamper with the
laser. You could be exposed to laser light or high voltage.
lIf you adjust the laser or perform procedures that are not described in the
user guides and manuals, you could be exposed to hazardous radiation.
REPLACING THE DESICCANT
When you open the desiccant compartment, you must prevent flammable liquids or gases from
entering the compartment. For instructions on changing the desiccant, see "Replace the Desiccant".
DANGER
Avoid explosion hazard.
Before you open the desiccant compartment, turn off the instrument power,
unplug the power cord and remove samples from the system. Entry of
flammable liquids or gases into the desiccant compartment could cause an
explosion. If such entry occurs, contact us immediately and do not apply power
to the instrument until the condition has been corrected.
REPLACING THE IR SOURCE
The IR source becomes extremely hot during use. If you need to replace the IR source, avoid burn
and explosion hazards.
CAUTION
Avoid burn hazard.
The source becomes extremely hot during normal use. Always allow the
source to cool for at least 10 minutes after the spectrometer is turned off before
you work with the source.
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Get Started with Your Nicolet Summit OA Spectrometer

Get Started with Your Nicolet Summit OA Spectrometer
DANGER
Avoid explosion hazard.
Before you remove the source from the spectrometer, turn off the instrument
power, unplug the power cord, disconnect any purge lines, and remove
samples from the system. Entry of flammable liquids or gases into the source
compartment could cause an explosion. If such entry occurs, contact us
immediately and do not apply power to the instrument until the condition has
been corrected.
Summary
The Nicolet Summit OA spectrometer is a safe and rugged instrument, but you can be exposed to
hazards during use and maintenance. During normal operation, use caution when handling
potentially hazardous samples and solvents and avoid parts of the spectrometer that are hot or emit
heat. During maintenance, take precautions to avoid harm or damage that could occur when purging
the instrument, handling internal components, or changing the desiccant.
14 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Unpack and Get Started with the
Spectrometer
Unpacking and setting up your Thermo Scientific Nicolet Summit OA Spectrometer requires you to
place the instrument in your workspace, to connect and power on the spectrometer, and to run a short
performance test.
Before You Begin
NOTICE
Wait 24 hours before taking the spectrometer out of its plastic shipping bag to prevent
condensation from forming that can damage internal optics. The warranty will not cover damage
due to opening the sealed plastic bag before the instrument has come to room temperature.
Reminder: Review the spectrometer's Site and Safety Information to ensure that the workspace is
safe and suitable for the instrument.
Unpacking and Setup
The steps for unpacking and setting up your spectrometer vary somewhat depending on the options
you purchased.
1. Unpack the shipping box
Remove the spectrometer from the shipping box and bag and remove additional packing
materials.
The spectrometer comes with a removable dust cover over the ATR crystal. Use the dust cover
when storing or moving the instrument, and remove it for regular use.
2. Connect the power supply to the spectrometer and to a properly grounded AC power source.
3. Connect the monitor, keyboard, and mouse.
a. Connect your monitor to the spectrometer's Mini DisplayPort connection.
b. Connect the keyboard and mouse to one of the spectrometer's USB ports.
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Get Started with Your Nicolet Summit OA Spectrometer
Note Some USB and Mini DisplayPort devices are known to interfere with the signal from
wireless USB devices, such as wireless keyboards and mice. If you notice performance
issues with your wireless keyboard and mouse, such as lag or delayed or missed input,
use the provided USB extension cable to position the wireless USB receiver farther from
the USB ports.
4. Press the instrument's power button to turn on the spectrometer. The spectrometer's LightBar
displays a cycling green light while the instrument warms up and shows a solid green bar when
the instrument is ready for use.
When you turn the instrument on or off, you may hear the sound of the internal polystyrene
reference moving. This is normal.
The first time you turn on the spectrometer, you are prompted to enter a new password. We
recommend that you do not enter a password at this time. Proceed without entering a password, then
when you have completed setup, manage accounts and passwords on the device according to your
organization's policies.
Note If the screen is black when you turn the system on, check the monitor power, DisplayPort
connection, and the monitor input. See the documentation that came with your monitor for details
on changing the input settings.
5. Open OMNIC Paradigm software.
The software may take several minutes to start and to connect to the instrument. The software
displays the connection status in the upper right corner of the screen. When the status shows you
are connected to the Nicolet Summit OA, proceed to the next step.
16 Nicolet Summit OA Spectrometer User Guide Thermo Scientific

Note If you open any menus in the software before the instrument is connected, Align and
Calibrate will be disabled. To enable them, when the instrument is connected, click Dashboard
in the toolbar.
6. Verify the spectrometer’s performance.
a. Align the spectrometer optics.
i. From the Desktop interface, go to Acquire Data > Diagnostics > Align Spectrometer.
ii. Select Start to begin alignment. The screen says "Align complete" when alignment has
finished successfully.
b. Calibrate the laser.
i. Go to the Acquire Data > Diagnostics > Laser Calibration.
ii. Select Start to begin calibration.
iii. Laser calibration may take several minutes to complete. When calibration is finished, the
display shows "Measurement complete" and indicates any change in laser frequency.
The instrument takes up to 12 hours to come to thermal equilibrium. For best results, re-run
alignment and calibration after the first 12 hours of operation.
c. Run the Nicolet Summit OA - PV Test workflow.
The performance verification workflow uses a reference material to run a series of standard
tests to verify your instrument operation and to ensure the accuracy of your data.
i. From the Dashboard of the Desktop interface, scroll to the Workflows pane.
ii. In the Workflow pane, right-click the Nicolet Summit OA - PV Workflow and select Run.
Thermo Scientific Nicolet Summit OA Spectrometer User Guide 17
Get Started with Your Nicolet Summit OA Spectrometer