ThermoFisher Scientific 146iQ User manual

146iQ
Instruction Manual
Multi-Gas Calibrator
117633-00 • 1Sep2019


Thermo Scientific 146iQ Instruction Manual iii
Contents
Introduction........................................................................................................ 1-1
iQ Series Instrument Platform............................................................. 1-1
Principle of Operation ........................................................................ 1-3
Dilution ........................................................................................... 1-3
Ozone Generation............................................................................ 1-3
Gas Phase Titration.......................................................................... 1-3
Photometer ...................................................................................... 1-4
Permeation Oven ............................................................................. 1-5
Specifications ...................................................................................... 1-9
Dimensions....................................................................................... 1-11
Installation and Setup...................................................................................... 2-1
Unpacking and Inspection .................................................................. 2-1
Cover Removing and Replacing .......................................................... 2-2
Mounting Options.............................................................................. 2-3
Bench Mount................................................................................... 2-3
Rack Mount..................................................................................... 2-4
Setup Procedure .................................................................................. 2-6
Startup ................................................................................................ 2-8
Operation ............................................................................................................ 3-1
Instrument Display ............................................................................. 3-1
Main Menus and Keypads................................................................ 3-4
Numeric Keypad........................................................................... 3-5
Alphanumeric Keypad................................................................... 3-6
Calibration.......................................................................................... 3-8
MFC Calibration ............................................................................. 3-9
Ozonator Calibration ..................................................................... 3-10
Manual Ozonator Calibration........................................................ 3-12
Photometer Calibration.................................................................. 3-14
Calibrate Background.................................................................. 3-15
Calibrate Span Coefficient .......................................................... 3-16
Advanced Photometer Calibration .............................................. 3-17
Manual Calibration..................................................................... 3-18
Photometer Detector Calibration ................................................ 3-21
Pressure Calibration ....................................................................... 3-23
Calibration History ........................................................................ 3-25
Data.................................................................................................. 3-26
Chapter 1
Chapter 2
Chapter 3

Contents
iv 146iQ Instruction Manual Thermo Scientific
View Data Log (Last Hour)............................................................ 3-27
View Data Log (Last 24 Hours) ..................................................... 3-28
View Data Log (User Defined Time) ............................................. 3-29
Advanced Data Setup..................................................................... 3-31
Data Logging Setup .................................................................... 3-32
Select Data Logging Variables ..................................................... 3-33
Streaming Data Setup ................................................................. 3-34
Select Streaming Variables........................................................... 3-35
Settings ............................................................................................. 3-36
Health Check................................................................................. 3-38
Status and Alarms........................................................................ 3-39
Predictive Diagnostics ................................................................. 3-63
Maintenance ............................................................................... 3-64
Preventive Maintenance .............................................................. 3-65
Change Part ................................................................................ 3-67
Maintenance History................................................................... 3-68
File Sharing and Support............................................................. 3-69
iQ360 ......................................................................................... 3-70
Operation ...................................................................................... 3-73
Cylinder Setup ............................................................................... 3-77
Gas Setup....................................................................................... 3-79
Gas Solenoid 16........................................................................ 3-80
Ozonator Setup.............................................................................. 3-81
Ozonator Setup........................................................................... 3-82
GPT Setup.................................................................................. 3-83
Photometer Settings ....................................................................... 3-85
Averaging Time........................................................................... 3-86
Compensation............................................................................. 3-87
Permeation Oven Setup ................................................................. 3-88
Programmed Events ....................................................................... 3-90
View Programs............................................................................ 3-91
Manual Operation ......................................................................... 3-93
Manual Operation Settings ......................................................... 3-94
Communications ........................................................................... 3-96
Wired TCP/DHCP .................................................................... 3-97
Serial RS-232/485....................................................................... 3-99
Analog I/O................................................................................ 3-100
Digital I/O................................................................................ 3-101
Email Server (SMTP)................................................................ 3-102
Instrument Settings...................................................................... 3-103
Display Setup............................................................................ 3-104
Alarm Set Points ....................................................................... 3-105
Clock ........................................................................................ 3-108
Time Zone................................................................................ 3-112
Configuration .............................................................................. 3-115
Security Access Levels................................................................... 3-116

Contents
Thermo Scientific 146iQ Instruction Manual v
Change Security to View Only Access ....................................... 3-118
Change Full Access Security Password....................................... 3-119
USB Drive ................................................................................... 3-121
Firmware Update Via USB Drive.............................................. 3-122
Download Data To USB Drive................................................. 3-123
Change USB Password.............................................................. 3-126
User Contact Information............................................................ 3-128
Update Bootloader....................................................................... 3-129
Calibration.......................................................................................................... 4-1
Calibration of the individual MFC outputs......................................... 4-1
Calibration of the Ozone Generator.................................................... 4-4
Calibration of the Photometer............................................................. 4-7
Verification of Photometer Performance .......................................... 4-8
Photometer Detector Calibration ..................................................... 4-9
Maintenance...................................................................................................... 5-1
Safety Precautions ............................................................................... 5-1
Fan Filter Inspection and Cleaning ..................................................... 5-1
Pump Rebuilding................................................................................ 5-2
Leak Test ............................................................................................ 5-5
Troubleshooting ................................................................................................ 6-1
Safety Precautions ............................................................................... 6-1
Troubleshooting Guide....................................................................... 6-1
Servicing............................................................................................................. 7-1
Safety Precautions ............................................................................... 7-1
Firmware Updates............................................................................... 7-3
Replacement Parts List ........................................................................ 7-3
Fuse Replacement ............................................................................... 7-5
Filter Replacement .............................................................................. 7-6
Fan Replacement................................................................................. 7-7
Measurement Side Removal and Replacing ......................................... 7-9
LCD Module Replacement ............................................................... 7-12
I/O Replacement............................................................................... 7-14
Peripheral Support Board and System Controller Board
Replacement ..................................................................................... 7-16
DMC Pressure and Flow Board ........................................................ 7-17
Pump Replacement (Optional) ......................................................... 7-19
Capillary Cleaning and/or Replacement ............................................ 7-22
Capillary O-Ring Replacement ......................................................... 7-24
Power Supply Replacement............................................................... 7-24
Step POL Board Replacement........................................................... 7-27
Optional Photometer DMC.............................................................. 7-31
Chapter 4
Chapter 5
Chapter 6
Chapter 7
Table of contents
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