Agilent Technologies G2623A User manual

Installation Guide
Thermal Conductivity Detector on a 6850 GC
Accessory G2623A

Agilent Technologies, Inc.
2850 Centerville Road
Wilmington, DE 19808-1610
USA
© Agilent Technologies 2000
All Rights Reserved. Reproduction,
adaptation, or translation without
permission is prohibited, except as allowed
under the copyright laws.
Part number G2623-90107
First Edition, JAN 2001
Replaces Part No. G2623-90100 Operating
and Service Manual.
HP® is a registered trademark of
Hewlett-Packard Co.
Printed in USA
Safety Information
The Agilent Technologies Thermal
Conductivity Detector meets the following
IEC (International Electrotechnical
Commission) classifications: Safety Class 1,
Transient Overvoltage Category II, and
Pollution Degree 2.
This unit has been designed and tested in
accordance with recognized safety
standards and designed for use indoors. If
the instrument is used in a manner not
specified by the manufacturer, the
protection provided by the instrument may
be impaired. Whenever the safety protection
of the Agilent G2623 has been
compromised, disconnect the unit from all
power sources and secure the unit against
unintended operation.
Refer servicing to qualified service
personnel. Substituting parts or performing
any unauthorized modification to the
instrument may result in a safety hazard.
Disconnect the AC power cord before
removing covers. The customer should not
attempt to replace the battery or fuses in
this instrument.
Safety Symbols
Warnings in the manual or on the
instrument must be observed during all
phases of operation, service, and repair of
this instrument. Failure to comply with these
precautions violates safety standards of
design and the intended use of the
instrument. Agilent Technologies assumes
no liability for the customer’s failure to
comply with these requirements.
WARNING
A warning calls attention to a condition or
possible situation that could cause injury to
the user.
CAUTION
A caution calls attention to a condition or
possible situation that could damage or
destroy the product or the user’s work.
Sound Emission Certification for Federal
Republic of Germany
Sound pressure Lp < 68 dB(A)
During normal operation
At the operator position
According to ISO 7779 (Type Test)
Schallemission
Schalldruckpegel LP < 68 dB(A)
Am Arbeitsplatz
Normaler Betrieb
Nach DIN 45635 T. 19 (Typprüfung)

Copyright© 2000
Agilent Technologies
Printed in USA Dec 2000
Agilent Part No. G2623-90107
1
Installing a Thermal Conductivity Detector on a
6850 Gas Chromatograph
This kit contains:
The TCD assembly is a factory-assembled, tested, and calibrated unit.
Disassembly of the unit is not required for installation.
Kit G2623-64000 Qty.
Thermal conductivity detector system 1
Performance evaluation sample kit 1
Bottom insulation 1
Seal insulation 1
Plastic grommet 1
Screw, M4 x 12 mm, pan head 5
Wrist strap, disposable, large 1
Installation sheet (this document) 1

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
2
Tools Required
Safety Information
Before continuing, read the safety information on your Agilent 6850 Gas
Chromatograph User Information CD-ROM.
Torx™T-20 driver
Flat blade screwdriver
Open end wrenches
Switching valve extension
Heater/sensor cable
Bottom insulation
Seal insulation
Tubing plugs
Plastic
grommet
Screws
Signal
board
PRT and
filament wires
Flow manifold cable
TCD assembly
cable and grommet

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
3
Prepare for Installation
WARNING Before proceeding, turn off the oven and any heated zones and let them cool
down. Turn off all detector gases at their supplies, then turn off the main
power switch and unplug the power cord.
1. Open the lid. If a column is installed, disconnect it at the detector end.
Remove the nut warmer, insulation, and capillary adapter, if present.
Close the lid.
2. Turn all gases off at their sources. Disconnect the carrier and detector
gas tubing from the back panel of the instrument.
ToBase - T
ToBase - T
Local Talk
Local Talk
BNC
BNC
Disconnect gas supply tubing
from these fittings

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
4
Remove the Lid Top Cover
Remove the lid top cover.
Disconnect the Heater/Sensor Cable
1. Trace the detector heater/sensor cable to the wiring harness near the
injection port cooling fan.
2. Disconnect the cable.
Raise the Lid to the Service Position
1. Open the lid. Locate the counterbalance cam in the left rear corner
under the lid. Loosen the screw on the right side of the cam. This allows
the stop plate to drop down.
Remove vent lines,
Remove T-20 Torx™
screws (8 places)
Remove detector
cover, if desired
Lid top cover, without
valve box accessory
if present

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
5
2. Raise the lid until it is stopped by the safety cable.
3. Raise the stop plate and tighten the screw to lock the lid in the upright
service position.
WARNING The lid is heavy. Always lock the lid when it is in the service position.
Counterbalance cam
Cam follower
Stop plate
Screw

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
6
Remove the Detector Electronics Cover
1. Loosen the two bottom screws on the detector electronics cover.
2. Remove the top screw on the cover.
3. Lift and remove the detector electronics cover.
Remove screw
Detector electronics cover
Loosen screws

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
7
4. Loosen the signal board clamp.
5. Unplug the signal board from the A/D converter board.
6. Disconnect the wiring from the signal board.
FID – Disconnect the ribbon cable. Unplug the ignitor cable. Pass both
cables through the hole to the top side of the lid.
The ribbon cable connector will not pass through the rubber grommet in
the hole. Use a small screwdriver to push the grommet to the top of the
lid; the cables will now fit through the hole.
Signal board clamp
Ribbon cable
A/D converter board
Signal board
(FID shown)

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
8
TCD –Unplug the two-wire switching valve cable at the connector. To
release the PRT and filament wires, press on the orange tabs. Pass the
disconnected cables/wires through the hole to the top side of the lid.
7. Lower the stop plate on the lid cam. Pull the lid forward until the cam
follower rests on the curved surface of the cam. Leave the stop plate in
the "down" position.
8. Close the lid.
Ribbon cable connector
Ignitor cable connector
Switching valve
Filament wires
PRT wires
cable connector

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
9
Remove the Existing Detector and Flow Manifold
1. On the top of the lid, loosen the connector cover plate and remove the
plates.
2. Disconnect the gas fittings. The figure above shows the FID manifold;
the TCD manifold is similar but has only one gas connection.
3. Trace the ribbon cable from the flow manifold and disconnect it from
the harness.
4. Remove the three manifold mounting screws.
5. Remove the screws holding the detector assembly in place.
Cover plate screws
Manifold mounting
Gas fittings
Gas manifold
(FID shown)
screws

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
10
FID –Remove four mounting screws.
TCD –Remove two mounting screws.
6. Lift the detector and flow manifold out of the lid as a unit.
WARNING The fibrous insulation material used in the Agilent 6850 can cause irritation
to the skin, eyes, and mucous membranes. Always wear gloves when
working with the insulation. If the insulation is flaky/crumbly, wear
protective eyewear and a respirator.
7. Remove any insulation that may be in the hole under the detector.
Install the Thermal Conductivity Detector and Flow Manifold
1. Place the bottom insulation in the detector hole. Align the flat sides
parallel to the sides of the lid.
2. Slide the seal insulation onto the bottom of the detector. Align it to
cover the detector bottom.
FID mounting screws
(one concealed)
Mounting screws

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
11
3. Align the thermal conductivity detector as shown and lower it into
place. Position the flow manifold. Check that no wiring or tubing is
trapped under either assembly.
4. Secure the detector assembly to the lid with two screws.
5. Secure the manifold to the lid with three screws.
6. Plug the manifold ribbon cable into its connector under the connector
cover plate.
7. Install the two connector cover plates.
8. Connect the gas supply line labeled Mto the center fitting on the flow
manifold.
Switching valve
cable connection
PRT and filament
Screws
Heater/sensor
cable connection
leads
Manifold cable connector
is under this plate
Connect gas line Mhere

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
12
WARNING The gas line labelled His plumbed to the hydrogen supply. Be sure to plug
this line to prevent accidental release of hydrogen gas into the instrument.
9. The A and Hgas lines are not used with the TC detector. If they are not
already plugged, plug them with the brass plugs and push them down
into the space under the manifold fittings. Avoid kinking the tubing.
Connect the Heater/Sensor Cable
Connect the detector heater/sensor cable to the wiring harness near the
injection port cooling fan.
Install the Switching Valve Extension Cable and Grommet
1. Locate the oblong hole for the switching valve extension cable. If there
is a grommet in the hole, remove it.
2. Pass the end of the extension cable through the oblong hole into the
signal board space. Use a small flat blade screwdriver to install the
grommet in the oblong hole.
Connect the other Leads and the Signal Board
1. Raise the lid to the upright service position and lock it in place by
raising the stop plate and tightening the screw.
2. Locate the round hole for the PRT and filament leads. If there is a
grommet in the hole, remove it and install the one from the kit. Pass the
two PRT leads and the two filament leads through the grommet into the
signal board space.
3. Plug the signal board into the A/D converter board and secure it with
the signal board clamp.
4. Connect the PRT and filament leads to the signal board by pressing the
orange tabs and inserting the appropriate wires. Polarity does not
matter, but the wires must go to the correct pair of connectors.
•PRT leads have light-colored insulation
•Filament leads have thick, black insulation

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
13
Caution Double check the PRT and filament connections before proceeding. An
incorrect connection can damage the detector when power is restored.
5. Plug the switching valve extension cable into the signal board.
6. Install the detector electronics cover and tighten all three screws.
7. Lower the stop plate on the lid cam. Pull the lid forward until the cam
follower rests on the curved surface of the cam. Raise the stop plate
behind the cam follower and tighten the screw.
8. Close the lid.
9. Install the lid top cover.
Finishing Up
1. If not already present, make an external T-connection between the
carrier gas supply and the Reference/Makeup gas fitting on the back of
the instrument.
2. Install the capillary adapter, if used.
3. Restore the column connection.
4. Restore carrier gas to the instrument.
5. Restore power.
6. Apply your normal operating pressures. Leak-check the manifold, back
panel, and column fittings.
Switching valve
Filament wires
PRT wires
cable connector

Installing a Thermal Conductivity Detector on a 6850 Gas Chromatograph
14

Printed on recycled paper.
This product is recyclable.
Agilent Technologies, Inc.
Printed in USA JAN 2001
G2623-90107