Agilent Technologies 5973N Operating instructions

Agilent Technologies
5973N and 5973 inert
Mass Selective
Detectors
Site Preparation Guide

2Site Preparation Guide
Notices
© Agilent Technologies, Inc. 2003
No part of this manual may be reproduced in
any form or by any means (including elec-
tronic storage and retrieval or translation
into a foreign language) without prior agree-
ment and written consent from Agilent
Technologies, Inc. as governed by United
States and international copyright laws.
Manual Part Number
G2589-90070
Edition
First edition, August 2003
Replaces part number G2589-90010
Printed in USA
Agilent Technologies, Inc.
2850 Centerville Road
Wilmington, DE 19808-1610 USA
Warranty
The material contained in this docu-
ment is provided “as is,” and is sub-
ject to being changed, without notice,
in future editions. Further, to the max-
imum extent permitted by applicable
law, Agilent disclaims all warranties,
either express or implied, with regard
to this manual and any information
contained herein, including but not
limited to the implied warranties of
merchantability and fitness for a par-
ticular purpose. Agilent shall not be
liable for errors or for incidental or
consequential damages in connec-
tion with the furnishing, use, or per-
formance of this document or of any
information contained herein. Should
Agilent and the user have a separate
written agreement with warranty
terms covering the material in this
document that conflict with these
terms, the warranty terms in the sep-
arate agreement shall control.
Safety Notices
CAUTION
A CAUTION notice denotes a haz-
ard. It calls attention to an operat-
ing procedure, practice, or the like
that, if not correctly performed or
adhered to, could result in damage
to the product or loss of important
data. Do not proceed beyond a
CAUTION notice until the indicated
conditions are fully understood and
met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could result
in personal injury or death. Do not
proceed beyond a WARNING
notice until the indicated condi-
tions are fully understood and
met.
Acknowledgements
Microsoft® and Windows® are U.S. regis-
tered trademarks of Microsoft Corporation

Site Preparation Guide 3
Contents
1 General Information
Instrument Identification 6
5973N MSD version 6
5973 inert MSD version 6
Important Safety Warnings 7
Many internal parts of the MSD carry dangerous voltages 7
Electrostatic discharge is a threat to MSD electronics 8
Many parts are dangerously hot 8
Hydrogen 9
Chemical safety 10
Safety and Regulatory Certifications 11
Information 11
Symbols 12
Electromagnetic compatibility 13
Sound emission certification for Federal Republic of
Germany 13
Cleaning 14
Recycling the Product 14
2 Site Preparation
Overview 16
Customer responsibility 16
Agilent responsibility 17
Other documentation 19
Space and Weight Requirements 20

4Site Preparation Guide
Communications Requirements 22
Telephone 22
Building network 22
Electrical Requirements 23
Voltage ranges of major components 23
Power configurations 24
Power requirements 25
Power plugs and cords 26
Other electrical considerations 27
Air Conditioning Requirements 29
Temperature and humidity 29
Airborne dust 30
Exhaust venting 30
Fume (exhaust) hood 31
Carrier and Reagent Gas Requirements 32
Regulators, tubing, and fittings 33
Laboratory Supply Requirements 34
Cleaning solvents 34
Data system supplies 34
Spare parts and consumables 35
Receiving the System 38
Delivery and unloading 38
Inspecting for damage 38
Storage 39
Unpacking 39
Installation and Verification 40
Installation 40
Verification 40
Sensitivity specifications 41
APowerCords

5
5973N and 5973 inert Mass Selective Detectors
Site Preparation Guide
Agilent Technologies
1
General Information
Instrument Identification 6
Important Safety Warnings 7
Safety and Regulatory Certifications 11
Cleaning 14
Recycling the Product 14
This section provides information on how to identify
specifically what type of MSD you are working with as well as
how to properly clean and dispose of the instrument. Also
included in this section are the “Important Safety Warnings”
which list critical safety precautions for all users.

6Site Preparation Guide
General Information
Instrument Identification
Each 5973N and 5973 inert Mass Selective Detector (MSD) is
identified by a unique 10-character serial number. This serial
number is located on a label on the lower left side near the front
of the instrument. On CI upgrades, a serial number is located on
the flow module.
When corresponding with Agilent Technologies about your
instrument, be sure to include the model number and both full
10-character serial numbers.
Write the serial number of your 5973 MSD here for reference:
5973N MSD version
The 5973N MSD is equipped with a diffusion pump. The serial
number label displays a product number that tells what kind of
MSD you have:
5973 inert MSD version
The 5973 inert MSD is equipped with either a standard
turbomolecular pump or a performance turbomolecular pump.
Chemical Ionization is available for the turbo MSDs only. The
serial number label displays a product number that tells what
kind of MSD you have:
This site preparation guide will refer to both 5973N and
5973 inert MSDs as 5973 Series MSDs unless noted otherwise.
Product number MSD type
G2577A Diffusion Pump, EI
Product number MSD type
G2578A Standard Turbo Pump, EI
G2579A Performance Turbo Pump, EI
G2589A Performance Turbo Pump, EI, NCI, PCI

General Information
Site Preparation Guide 7
Important Safety Warnings
Before moving on, there are several important safety notices
that you should always keep in mind when using the 5973 Series
Mass Selective Detector.
Many internal parts of the MSD carry dangerous voltages
If the MSD is connected to a power source, even if the power
switch is off, potentially dangerous voltages exist on:
•The wiring between the MSD power cord and the AC power
supply, the AC power supply itself, and the wiring from the
AC power supply to the power switch.
With the power switch on, potentially dangerous voltages also
exist on:
•All electronics boards in the instrument.
•The internal wires and cables connected to these boards.
•The wires for any heater.
Connecting the MSD to power sources that are not equipped
with protective earth contacts creates a shock hazard for the
operator and can damage the instrument.
Interrupting the protective conductor inside or outside the MSD
or disconnecting the protective earth terminal creates a shock
hazard for the operator and can damage the instrument.
WARNING All these parts are shielded by covers. With the covers in place, it
should be difficult to accidentally make contact with dangerous
voltages. Unless specifically instructed to, never remove a cover
unless the detector, inlet, or oven are turned off.
WARNING If the power cord insulation is frayed or worn, the cord must be
replaced. Contact your Agilent service representative.

8Site Preparation Guide
General Information
Make sure the power cords supplied with the MSD are
appropriate for your country and site before using them.
Maintain easy access to the power cords so they can be
disconnected during maintenance.
The use of incorrect or makeshift fuses or the short-circuiting of
fuse holders creates a shock hazard for the operator and can
damage the instrument. Replace fuses only with fuses of
identical current rating and type.
Excessive fluctuations in the line voltage can create a shock
hazard and can damage the instrument. Make sure the supply
voltage does not fluctuate more than +5% or -10% from the rated
voltage. This equipment must be installed in a Category II
environment as defined in IEC 664.
Electrostatic discharge is a threat to MSD electronics
The printed circuit (PC) boards in the MSD can be damaged by
electrostatic discharge. Do not touch any of the boards unless it
is absolutely necessary. If you must handle them, wear a
grounded wrist strap and take other antistatic precautions.
Wear a grounded wrist strap any time you must remove the MSD
covers.
Many parts are dangerously hot
Many parts of the MSD operate at temperatures high enough to
cause serious burns.
You should always cool heated areas of the MSD to room
temperature before working on them. They will cool faster if you
first set the temperature of the heated zone to room
temperature. Turn the zone off after it has reached the setpoint.
If you must perform maintenance on hot parts, use a wrench
and wear gloves. Whenever possible, cool the part of the
instrument that you will be maintaining before you begin
working on it.

General Information
Site Preparation Guide 9
Hydrogen
Hydrogen gas may be used as carrier gas, and/or as fuel for an
FID. When mixed with air, hydrogen can form explosive
mixtures.
WARNING Be careful when working behind the gas chromatograph (GC).
During cool-down cycles, the GC emits hot exhaust which can cause
burns.
WARNING The insulation around the GC inlets, detectors, valve box, and the
insulation cups is made of refractory ceramic fibers. To avoid
inhaling fiber particles, we recommend the following safety
procedures: ventilate your work area; wear long sleeves, gloves,
safety glasses, and a disposable dust/mist respirator; dispose of
insulation in a sealed plastic bag; wash your hands with mild soap
and cold water after handling the insulation.
WARNING When using hydrogen (H2) as the carrier gas or fuel gas, be aware
that hydrogen gas can flow into the oven and create an explosion
hazard. Therefore, be sure that the supply is off until all connections
are made, and ensure that the GC inlet and detector column fittings
are either connected to a column or capped at all times when
hydrogen gas is supplied to the instrument.
Hydrogen is flammable. Leaks, when confined in an enclosed space,
may create a fire or explosion hazard. In any application using
hydrogen, leak test all connections, lines, and valves before
operating the instrument. Always turn off the hydrogen supply at its
source before working on the instrument.
WARNING The MSD cannot detect leaks in gas streams. For this reason, it is
vital that column fittings should always be either connected to a
column, or have a cap or plug installed.

10 Site Preparation Guide
General Information
When using hydrogen gas, check the system for leaks as
described by your local Environmental Health and Safety (EHS)
requirements to prevent possible fire and explosion hazards.
Always check for leaks after changing a tank or servicing the
gas lines. Always make sure the vent line is vented into a fume
hood.
Chemical safety
WARNING The foreline pump exhaust and split vent exhaust will contain traces
of the chemicals you are analyzing. These could potentially be toxic.
Vent the foreline pump exhaust and split vent exhaust outside your
laboratory or into a fume hood. Be sure to comply with all local
environmental regulations.

General Information
Site Preparation Guide 11
Safety and Regulatory Certifications
The 5973 Series Mass Selective Detector conforms to the
following safety standards:
•Canadian Standards Association (CSA): C22.2 No. 1010.1
•CSA/Nationally Recognized Test Laboratory (NRTL):
UL 61010A–1
•International Electrotechnical Commission (IEC): 61010–1
•EuroNorm (EN): 61010–1
The 5973 Series Mass Selective Detector conforms to the
following regulations on Electromagnetic Compatibility (EMC)
and Radio Frequency Interference (RFI):
•CISPR 11/EN 55011: Group 1, Class A
•IEC/EN 61326
•AUS/NZ
This ISM device complies with Canadian ICES-001. Cet appareil
ISM est conforme a la norme NMB—001 du Canada.
The 5973 Series Mass Selective Detector is designed and
manufactured under a quality system registered to ISO 9001.
Information
The Agilent Technologies 5973 Series Mass Selective Detector
meets the following IEC (International Electro-technical
Commission) classifications: Safety Class I, Transient
Overvoltage Category II, Pollution Degree 2.
This unit has been designed and tested in accordance with
recognized safety standards and is designed for use indoors. If
the instrument is used in a manner not specified by the
manufacturer, the protection provided by the instrument may
be impaired. Whenever the safety protection of the MSD has
been compromised, disconnect the unit from all power sources
and secure the unit against unintended operation.

12 Site Preparation Guide
General Information
Refer servicing to qualified service personnel. Substituting
parts or performing any unauthorized modification to the
instrument may result in a safety hazard.
Symbols
Warnings in the manual or on the instrument must be observed
during all phases of operation, service, and repair of this
instrument. Failure to comply with these precautions violates
safety standards of design and the intended use of the
instrument. Agilent Technologies assumes no liability for the
customer’s failure to comply with these requirements.
See accompanying instructions for more
information.
Indicates a hot surface.
Indicates hazardous voltages.
Indicates earth (ground) terminal.
Indicates explosion hazard.
Indicates radioactivity hazard.
Indicates electrostatic discharge hazard.

General Information
Site Preparation Guide 13
Electromagnetic compatibility
This device complies with the requirements of CISPR 11.
Operation is subject to the following two conditions:
•This device may not cause harmful interference.
•This device must accept any interference received, including
interference that may cause undesired operation.
If this equipment does cause harmful interference to radio or
television reception, which can be determined by turning the
equipment off and on, the user is encouraged to try one or more
of the following measures:
1Relocate the radio or antenna.
2Move the device away from the radio or television.
3Plug the device into a different electrical outlet, so that the
device and the radio or television are on separate electrical
circuits.
4Make sure that all peripheral devices are also certified.
5Make sure that appropriate cables are used to connect the
device to peripheral equipment.
6Consult your equipment dealer, Agilent Technologies, or an
experienced technician for assistance.
7Changes or modifications not expressly approved by Agilent
Technologies could void the user’s authority to operate the
equipment.
Sound emission certification for Federal Republic of Germany
Sound pressure
Sound pressure Lp < 70 dB according to EN 27779:1991.
Schalldruckpegel
Schalldruckpegel LP < 70 dB am nach EN 27779:1991.

14 Site Preparation Guide
General Information
Cleaning
To clean the unit, disconnect the power and wipe down with a
damp, lint-free cloth.
Recycling the Product
For recycling, contact your local Agilent sales office.

15
5973N and 5973 inert Mass Selective Detectors
Site Preparation Guide
Agilent Technologies
2
Site Preparation
Overview 16
Space and Weight Requirements 20
Communications Requirements 22
Electrical Requirements 23
Air Conditioning Requirements 29
Carrier and Reagent Gas Requirements 32
Laboratory Supply Requirements 34
Receiving the System 38
Installation and Verification 40
This section describes how to properly prepare your site for a
new MSD. Follow these instructions carefully as delays due to
improper site preparation may result in loss of instrument use
during the warranty period.

16 Site Preparation Guide
Site Preparation
Overview
Before the 5973 Series Mass Selective Detector system can be
installed, the site must be properly prepared. Site preparation
includes, but is not limited to, ensuring that adequate facilities
are available. Among the site requirements are:
•Adequate space is available for the MSD system.
•A suitable supporting bench is available.
•Adequate electrical power is available at the correct voltages
and frequencies.
•Environmental control systems are adequate to maintain a
correct, stable operating environment.
•Preparations for safe exhaust venting are adequate.
•Supplies necessary for instrument operation are available,
including solvents, carrier and reagent gasses, and printer
paper.
Delays due to inadequate site preparation could cause loss of
instrument use during the warranty period. In extreme cases,
Agilent Technologies may ask to be reimbursed for the
additional time required to complete the installation. Agilent
Technologies provides service during the warranty period and
under maintenance agreements only if the specified site
requirements are met.
Customer responsibility
Unless previous arrangements have been made with Agilent
Technologies, site preparation is the customer’s responsibility.
Customer responsibilities include, but are not limited to:
•Planning, scheduling, and preparing the site according to the
specifications in this manual
NOTE Installation and verification will only be performed using helium carrier
gas.

Site Preparation
Site Preparation Guide 17
•Verifying that the electrical environment is safe and adequate
for the MSD system installation and operation
•Complying with all local laws (codes, ordinances, and
regulations) for mechanical, building, and electrical
distribution systems, hazardous waste disposal, and
chemical storage.
Compliance must exist prior to installation.
•Providing lifting equipment adequate to unload the system
from the delivery vehicle and transport it to the site where it
will be installed
•Providing someone to help lift the MSD onto the laboratory
bench
•Providing adequate secure storage space for the system until
it can be installed by an Agilent Technologies representative
Agilent responsibility
An Agilent Technologies service representative will install the
MSD and verify its performance. The service representative’s
responsibilities are limited to:
•Unpacking the MSD system and verifying that all components
are present and undamaged
•Connecting the carrier gas line to the instrument from the
tank, regulators, and lines previously installed by the
customer
•Installing, connecting, and turning on MSD system
components
•Verifying that the system meets Agilent Technologies
performance standards
•Providing basic user familiarization for system hardware and
software
•Signing the customer up through the Response Centers for
instrument and software support

18 Site Preparation Guide
Site Preparation
Agilent Technologies is not responsible for:
•Any task not listed in the 5973 Series MSD Hardware
Installation Manual (G2589-90073) or the installation guides
for the GC, data system, and other accessories
•Installing helium carrier gas or reagent gas tanks and
regulators
•Connecting or verifying the performance of hardware and
software not provided by Agilent Technologies
•Connecting the MSD/ChemStation system to the building
network
•Testing the MSD against customer standards or samples
•Providing detailed instruction in the operation of the
computer operating system and MSD software
•Setting up laboratory procedures
•Operating the MSD system following installation
NOTE Items that do not include installation by Agilent Technologies must be
installed by the customer.
NOTE Contact Agilent Technologies for information concerning training classes.
NOTE Contact Agilent Technologies for information concerning Application
Assist or Chemical Analysis Consulting services.

Site Preparation
Site Preparation Guide 19
Other documentation
Additional information is contained in the following
documentation:
•5973N or 5973 inert Mass Selective Detector Hardware
Manual, which is located on the 5973N and 5973 inert Mass
Selective Detector User Information CD-ROM
•5973 Network Mass Selective Detector Site Preparation
manual or 5973 inert Mass Selective Detector Site
Preparation Guide
•6890 Series GC manuals
•GC accessories (autosampler, etc.) manuals
•G1701DA MSD Productivity ChemStations software manuals
and online help
•The appropriate sensitivity specifications for your
instrument:
5973N: Agilent publication 5968-7358E
5973 inert: Agilent publication 5988-9991EN
•Hydrogen Carrier Gas Safety Guide (5955-5398)
For updated information, see the Agilent Technologies website
at http://www.agilent.com/chem.

20 Site Preparation Guide
Site Preparation
Space and Weight Requirements
Table 1 lists dimension and weight information for the MSD and
related components. Your site must have enough bench space
for the MSD, GC, data system, and accessories. In addition,
there must be sufficient space around the system for ventilation
and maintenance access. At least 30 cm (12 inches) to the left of
the MSD and at least 20 cm (8 1/4 inches) behind the MSD must
be kept clear.
Benches must be sturdy enough to support the weight of the
entire system.
The foreline pump can be located on the laboratory bench or on
the floor. It must be close to the MSD because it is connected by
a 200-cm (79-inch) hose. The hose is stiff and cannot be bent
sharply.
CAUTION Do not put the foreline pump on your laboratory bench if
vibration-sensitive equipment is located on the bench.
PC
Monitor
Printer
6890 Series GC
ALS tray
5973 Series MSD