5. OPERTION
5-1. sta Up
5-1-1. O1eckig of wiring.
Cbnfinn tht all wires are correcy connected over the entire systan (see
paagrph 3-2).
5-1-2. Optig the anlyzer.
Supply the correct p: to the anyzer an plug in.
5-1-3. The magnetic cc.
It is not necsa to ope the case of the 'I0 anyzer for caibtion,
recnfiguation, etc. All halings are pefonned by a magnetic cader. '!s
ccer is place in a click-in hole on the front. For activating a key
(ree-relay), the ccer has to be place in the middle of the gree field.
5-2. Calibation.
The measuring loop for both pH an ORP mesuranents mut be caibted. A
description:is given in the pagrphs belCM.
5-2-1. Calibration of the mesuring loop for pH meaants.
Basically there are thee method:
1. bufer solution calibration
2. pross calibration
3. input of electre chacteristics.
5-2-1-1. Bufer solution calibtion.
Buffer solution calibration (or IIlifer
check") is pefonn using tw bufer solution.
The 1 st solution is for calibtion of the
offset voltage (asyitr lXtential of the pair
of electrodes). Geerlly, a value nea to the
isothenl lXint of intesection is chosen
(nornlly 7 pH).
The 2nd buffer solution is for calibration
of the seni ti vi ty of the electrodes (slope)
and usually, a buffer solution of 4 pH is coosen.
This solution has a high staility.
When bufer solutions accrding to the NB
stad are chosen, then the 'I0 anlyzer
recses these solutions an caibration is
perfonn. The NB stas are listed in
tale 5-1 (ST to ST5).
ID: The procure to ca out bufer ,
solution calibration is describ in: .
pagraph 5-3-4.
When no solution accordg to the NB
stada is used, then the value of the
solution ca be entered in the marry (see
paagrph 6, IIRecnfigliration of the
anlyzer II).
I
g
t:'
~
~
I
~
~
"00
.300
.200
.100
~"
E
t02L
_pH
-100
- 200
12 "
-300
-LOO
Figue 5-1.
Bufer solution calibtion
ST ST2 ST3 ST4 ST5 TE .
1.67 4.00 6.98 9.46 13.42 o "c
1.67 4.00 6.95 9 .JQ. 13.21 5 "C
1..67 4.00 6~92 ~.33 13~9.Q -10-oc
J .67 4.00 6.90 9.28 12.81 -1S"oC
1.68 4.00 6.88 9.23 i 2J~j 20-oC '
1.68 4.01 6.87 9.18 12.45 25 "c
1.68 4.02 6.85 9.14 12.29 30 DC
i.69 4.02 tj.~ s4 9~io 12~lj -3S- °c
~- , -4ö'c
1.69 4.04 6.84 9.07 11 ~~8
1.70 4.05 6.83 9.04 11 . a4 -'4Š-õC
_.- -_.-
J..71 4.06 6.83 ~.Ql 11 .71 50 DC
1.72 4.08 6.83 9.99 11.57 sSOë'
-1.12 1.09 6.84 9.96 n.45 -60-õC
1.73 4.11 6.84 9.94 11 .33 65 DC
1.74 4.13 6.85 8.92 11 .22 70 DC
1.75 4.15 6.86 8.90 11.11 75 DC
1.77 4.16 6.86 8.89 11 .01 80 DC
1.78 4.18 6.87 8.88 10.91 85 DC
1.79 4.21 6.88 8.85 10.82 90 DC
1 .81 4.23 6.89 8.83 10.73 -95" DC
1.83 4.25 6.90 8.81 10:65 100-oc'
Tale 5-1.
NB stas 18