5
Note: There is no need to repeat this procedure every time
unless one decides to change the buffer settings.
pH Calibration
1. With pH on the display, press the “Mode” key for 2
seconds to enter the “pH Calibration Mode”.
2. Immerse the electrode into either pH 7.00 or 6.86 buffer
solution, depending on the Buffer Set selected. A ‘WAIT”
icon will flash. The pH/EC1030A will determine when the
calibration reading is stable.
3. When the “WAIT” icon disappears, one/first point
calibration is now complete. Press “Mode” key to exit (i.e.
only complete a one point calibration) or wait 5 seconds
for the meter to enter two/second point calibration.
4. Repeat Steps 2 and 3 for two points/second point
calibration by immersing in pH 4.01/4.00 or 10.01/9.18
buffers.
Note: For highest accuracy, perform a 2-point calibration.
5. Move to #6 for three/third point calibration or press
“Mode” to exit two point calibration.
6. Repeat Steps 2 and 3 for three/third point calibration.
7. When the “WAIT” icon disappears, the unit will
automatically return to Measure Mode.
D. Conductivity Calibration
Preparing Standard Solutions
Suitable conductivity standards are available commercially
or the user can prepare them using research grade reagents.
When calibrating, it is best to use a standard in the middle
range of the solutions to be measured.
Here are some standard solutions the user can prepare to
calibrate the conductivity sensor:
1. Standard solution of 1413 μS at 25 °C: Accurately weigh
out 0.746 grams of research grade dried Potassium
Chloride (KCl). Dissolve in 1000 mL of distilled water.
2. Standard solution of 12.90 mS at 25 °C: Accurately weigh
out 7.4365 grams of research grade dried Potassium
Chloride (KCl). Dissolve in 1000 mL of distilled water.
[Note: You can store the remaining solution in a plastic
container for one week but the air space between the cap and
the solution must be kept to an absolute minimum. Storing
the excess solution below 4 °C can increase the storage life.
If you have any doubt of the accuracy of the stored solution, a
fresh batch should be prepared.]