Bruker minispec TC3 User manual

minispec
Temperature Unit TC3
User Manual
Version 004
Innovation with Integrity
●
AIC

Copyright © by Bruker Corporation
All rights reserved. No part of this publication may be reproduced, stored in a retrieval
system, or transmitted, in any form, or by any means without the prior consent of the
publisher. Product names used are trademarks or registered trademarks of their re-
spective holders.
This manual was written by
Bruker BioSpin AIC
© December 14, 2016 Bruker Corporation
Document Number: 10000031931
P/N: H148851
For further technical assistance for this product, please do not hesitate to contact your
nearest BRUKER dealer or contact us directly at:
Bruker Corporation
Am Silberstreifen
76287 Rheinstetten
Germany
Phone: + 49 721 5161 0
E-mail: [email protected]
Internet: www.bruker.com

Contents
H148851_4_004 iii
Contents
1 About This Manual .............................................................................................................................5
1.1 Policy Statement .................................................................................................................5
1.2 Symbols and Conventions ..................................................................................................5
2 Introduction.........................................................................................................................................7
2.1 Overview .............................................................................................................................7
2.2 Features..............................................................................................................................8
2.3 Intended Use.......................................................................................................................8
3 Safety...................................................................................................................................................9
3.1 Safety Notices.....................................................................................................................9
3.1.1 Power Cord Set Requirements ...........................................................................................9
3.1.2 Power Cord Safety Maintenance ........................................................................................9
3.1.3 Mains Disconnect................................................................................................................9
3.1.4 Mechanical Hazards .........................................................................................................10
3.1.5 Thermal Hazards ..............................................................................................................11
3.1.6 Operating Environment .....................................................................................................11
3.1.7 Explanation of Warning Labels .........................................................................................12
3.2 Electromagnetic Interference ............................................................................................13
3.3 Explanation of Regulatory Marks ......................................................................................13
4 Technical Data ..................................................................................................................................15
4.1 Environmental Characteristics ..........................................................................................15
4.2 Electrical Characteristics...................................................................................................15
4.3 Gas Connection ................................................................................................................16
4.4 Thermal Characteristics ....................................................................................................16
5 Transport, Packaging and Storage .................................................................................................19
6 Installation.........................................................................................................................................21
7 Operation...........................................................................................................................................23
7.1 Power-On..........................................................................................................................23
7.2 Power-Off..........................................................................................................................23
7.3 Controlling the Temperature .............................................................................................23
7.4 Understanding the LEDs...................................................................................................23
7.4.1 Power Indicator .................................................................................................................23
7.4.2 Zone Status Indicators ......................................................................................................23
8 Maintenance......................................................................................................................................25
8.1 Replacing the Fuse ...........................................................................................................25
8.2 Replacing the Air Filter......................................................................................................26
8.3 Cleaning Instructions ........................................................................................................27
8.4 Cleaning Broken Vials.......................................................................................................28
8.4.1 Cleaning Procedure ..........................................................................................................29
9 Dismantling and Disposal................................................................................................................35
9.1 Dismantling .......................................................................................................................35

Contents
iv H148851_4_004
9.2 Disposal Europe................................................................................................................35
9.3 Disposal USA and Other Countries ..................................................................................36
10 Contact ..............................................................................................................................................37
List of Figures...................................................................................................................................39
List of Tables ....................................................................................................................................41
Index ..................................................................................................................................................43

About This Manual
H148851_4_004 5
1 About This Manual
This manual enables safe and efficient handling of the device.
This manual is an integral part of the device, and must be kept in close proximity to the
device where it is permanently accessible to personnel. In addition, instructions concerning
labor protection laws, operator regulations tools and supplies must be available and adhered
to.
Before starting any work, personnel must read the manual thoroughly and understand
its contents. Compliance with all specified safety and operating instructions, as well as local
work safety regulations, are vital to ensure safe operation.
The figures shown in this manual are designed to be general and informative and may not
represent the specific Bruker model, component or software/firmware version you are
working with. Options and accessories may or may not be illustrated in each figure.
1.1 Policy Statement
It is Bruker’s policy to improve products as new techniques and components become
available. Bruker reserves the right to change specifications at any time.
Every effort has been made to avoid errors in text and Figure presentation in this publication.
In order to produce useful and appropriate documentation, we welcome your comments on
this publication. Field Service Engineers are advised to check regularly with Bruker for
updated information.
Bruker is committed to providing customers with inventive, high-quality, environmentally-
sound products and services.
1.2 Symbols and Conventions
Safety instructions in this manual and labels of devices are marked with symbols. .
The safety instructions are introduced using indicative words which express the extent of the
hazard.
In order to avoid accidents, personal injury or damage to property, always observe safety
instructions and proceed with care.
DANGER
DANGER indicates a hazardous situation which, if not avoided, will result in
death or serious injury.
This is the consequence of not following the warning.
1. This is the safety condition.
uThis is the safety instruction.

About This Manual
6 H148851_4_004
WARNING
WARNING indicates a hazardous situation, which, if not avoided, could result
in death or serious injury.
This is the consequence of not following the warning.
1. This is the safety condition.
uThis is the safety instruction.
CAUTION
CAUTION indicates a hazardous situation, which, if not avoided, may result in
minor or moderate injury or severe material or property damage.
This is the consequence of not following the warning.
1. This is the safety condition.
uThis is the safety instruction.
NOTICE
NOTICE indicates a property damage message.
This is the consequence of not following the notice.
1. This is a safety condition.
uThis is a safety instruction.
SAFETY INSTRUCTIONS
SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event
of an error or emergency.
This is the consequence of not following the safety instructions.
1. This is a safety condition.
uThis is a safety instruction.
This symbol highlights useful tips and recommendations as well as
information designed to ensure efficient and smooth operation.

Introduction
H148851_4_004 7
2 Introduction
2.1 Overview
The TC3 temperature unit, also called a dry bath, allows you to control the temperature of
samples in an ASX-7000-series sample changer. It heats or chills the samples under the
control of a host computer.
Figure2.1: The TC3 Unit.
The temperature unit comes in three versions:
•10 mm SFC version: The unit holds vials in three temperature-controlled zones. Each
zone holds 60 vials, with a maximum temperature of 100° C.
•10 mm polymers version: The unit holds vials in one temperature-controlled zone. The
zone holds 60 vials, with a maximum temperature of 110° C.
•26 mm version: The unit holds vials in two temperature-controlled zones. Each zone
holds 12 vials, with a default maximum temperature of 60° C (the system is capable of
reaching 80° C).
A power cord and appropriate data cables are also provided.

Introduction
8 H148851_4_004
2.2 Features
Temperature Range
Depending on the version, sample temperature can be maintained at 0° C to +110° C.
Sample Changer Compatibility
Use only with an ASX-7600 pick-and-place NMR sample changer.
Chemical Compatibility
Exposed surfaces are made of corrosion‑resistant stainless steel alloys or anodized
aluminum.
2.3 Intended Use
This equipment is designed for use in analytical laboratories performing chemical analysis of
samples.

Safety
H148851_4_004 9
3 Safety
Review this product and related documentation to familiarize with safety markings and
instructions before you operate the instrument.
3.1 Safety Notices
CAUTION
Injury Hazard
If the device is used in a manner not specified by the manufacturer, the protection provided
by the device may be impaired.
Repair or service that is not covered in this manual should only be performed by qualified
personnel.
3.1.1 Power Cord Set Requirements
The power cord set supplied with the device meets the requirements of the country where the
device was purchased. Power is supplied to the device through the included 24V power
supply.
3.1.2 Power Cord Safety Maintenance
The operator should check the condition of the power/signal supply cord. The device should
not be operated if the mains inlet is cracked or broken. Any obvious damage to the case
(from a drop or fall) should be checked by service personnel for loose or damaged parts.
Refer to the individual part lists, or contact Bruker, for approved replacement parts.
3.1.3 Mains Disconnect
The power switch on the rear panel is not the mains disconnect. Power mains disconnect is
accomplished by unplugging the power cord from the power supply or from the wall outlet.
Ensure the power cord is easily accessible and removable, in the event of an emergency
which requires immediate disconnection.

Safety
10 H148851_4_004
WARNING
Fire and Shock Hazard
Incorrect installation or use of the power supply may result in a fire or shock hazard.
uUse only the provided power supply.
uThe power supply must be plugged into an outlet which has a protective ground
connection.
uEnsure that the power cord is disconnected before removing any covers.
3.1.4 Mechanical Hazards
Figure3.1: Bottom View with Filter Drawer Removed
WARNING
Laceration Hazard
If the unit power is left on, the spinning fan blade just above the filter may cause injury.
uEnsure the AC power is off before removing the filter.
WARNING
Lifting Hazard
Lifting without assistance may cause injury.
uTwo people are required to lift the device.
uLifting should be done with a person situated on either side of the device.

Safety
H148851_4_004 11
3.1.5 Thermal Hazards
WARNING
Burn Hazard
Incorrect handling of vials or inserting fingers into any holes in the device may result in burn
injuries.
uDo not handle vials from heated zones until they have been given time to cool.
uDo not attempt to insert fingers into any holes in the device.
3.1.6 Operating Environment
WARNING
Shock Hazard from Rain or Humidity
Device exposure to rain or humidity could result in a risk of fie or electrical shock.
uDo not expose the device to rain or humidity.
uDo not open the cabinet, all maintenance is to be performed by an authorized service
provider.
Protection provided by the device may be impaired if the device is used in a manner not
specified by the manufacturer.
WARNING
Shock Hazard from Liquids
Liquid coming in contact with electrical components may result in a serious injury through
shock.
uDo not allow any liquid to enter the device cabinet other than as intended through the
specified tubing, or come into contact with any electrical components.
uThe device must be thoroughly dry before you reconnect power, or turn the device on.
WARNING
Explosion Hazard
Explosive atmospheres caused by flammable gases, mists or vapors or by combustible
dusts could result in an explosion.
uPrevent the release of dangerous substances, which can create explosive atmospheres.
uPrevent sources of ignition.
uDo not operate the device in an explosive atmosphere.

Safety
12 H148851_4_004
WARNING
Chemical Hazards
Incorrect use of chemicals used in and near the device may result in injury or property
damage.
uLearn about the chemicals which will be used in and near the device, and observe the
necessary precautions.
uAlways use appropriate personal protective equipment, including protective eyewear.
3.1.7 Explanation of Warning Labels
Warning symbol marked on device.
• This symbol means “Attention! Refer to the manual.”
Warning symbol marked on equipment. This symbol means “Hot surface!” Touching external
surfaces of the instrument can cause burn injury.
• Do not touch the instrument until it has cooled down.
Figure3.2: Locaton of Warning Labels

Safety
H148851_4_004 13
3.2 Electromagnetic Interference
FEDERAL COMMUNICATIONS COMMISSION (FCC) NOTICE
This equipment has been tested and found to comply with the limits for a Class A digital
device, pursuant to Part 15 of the FCC Rules. These limits are designed to provide
reasonable protection against harmful interference in a commercial installation.
This equipment generates, uses, and can radiate radio frequency energy and, if not installed
and used in accordance with the instructions, may cause harmful interference to radio
communications. Operation of this equipment in a residential environment is likely to cause
harmful interference, in which case the user will be required to correct the interference at his
expense.
MODIFICATIONS
The FCC requires the user to be notified that any changes or modifications made to this
device that are not expressly approved by the manufacturer may void the user's authority to
operate the equipment.
CABLES
Connections to this device must be made with shielded cables with metallic RFI/EMI
connector hoods to maintain compliance with FCC Rules and Regulations.
CANADIAN NOTICE
This digital apparatus does not exceed the Class A limits for radio noise emissions from
digital apparatus as set out in the interference-causing equipment standard entitled "Digital
Apparatus" ICES-001 of the Department of Communications.
AVIS CANADIEN
Cet appareil numérique respecte les limites de bruits radioélectriques applicables aux
appareils numériques de Classe A prescrites dans la norme sur le matériel brouilleur:
"Appareils Numériques," NMB-001 édictée par le ministre des Communications.
3.3 Explanation of Regulatory Marks
The CE mark is a registered trademark of the European Community. This CE mark
shows that the product complies with all the relevant European Legal Directives.

Safety
14 H148851_4_004

Technical Data
H148851_4_004 15
4 Technical Data
4.1 Environmental Characteristics
These environmental characteristics indicate the conditions for safe operation. Instrument
performance may depend on the ambient conditions.
Operating Temperature +5° C to +40° C (+41° F to +104° F)
Non-Operating
Temperature
+0° C to +55° C (+32° to +131° F)
Operating Altitude Up to 2,000 m (6,562 ft.)
Relative Humidity 0% to 80% non-condensing for temperatures up to 31° C,
decreasing linearly to 50% at 40° C.
Non-Operating Relative
Humidity
0% to 95% non-condensing.
Pollution Degree Pollution degree 2.
Normally no pollution or only dry, non-conductive pollution
occurs. The pollution has no influence. Occasionally,
however, a temporary conductivity caused by condensation
may be expected.
Table4.1: Environmental Characteristics
For indoor use only.
Avoid sudden, extreme temperature changes which could cause condensation on circuit
boards in the device.
4.2 Electrical Characteristics
Power Input:
AC voltage, frequency, and current.
100-240 V ~, 50-60 Hz, 5 A maximum.
Installation category: CAT II (line voltage in appliance and to wall outlet).
RS232 RS-232 serial connection to the sample changer (maximum ±12VDC, 8
mA).
RS485 TIA/EIA-485 (use only for connection to another temperature unit,
maximum ±8VDC, 200 µA).
Table4.2: Electrical Characteristics

Technical Data
16 H148851_4_004
4.3 Gas Connection
One fitting is provided for nitrogen purge gas. The nitrogen source must be regulated to a
pressure of no more than 35 kPa (5 psi, 0.35 bar). A typical gas flow of 0.5 liter/minute shall
apply.
4.4 Thermal Characteristics
Temperature calibration and validation is performed at the factory.
Figure4.1: Thermal Characteristics of a 3-Zone 10 mm SFC Version
Zone Default Temperature Temperature Range
3 0° C 0° C to +66° C
2 65° C Ambient +5° C to +66° C
1 100° C Ambient +5° C to +100° C

Technical Data
H148851_4_004 17
Figure4.2: Thermal Characteristics of a 1-Zone 10 mm Polymers Version
Zone Default Range
1 Ambient +5° C to +110° C

Technical Data
18 H148851_4_004
Figure4.3: Thermal Characteristics of a 2-Zone 26 mm Version
Zone Temperature Range
2 Ambient +5° C to +80° C
1 Ambient + 5° C to +80° C

Transport, Packaging and Storage
H148851_4_004 19
5 Transport, Packaging and
Storage
WARNING
Lifting Hazard
Lifting without assistance may cause injury.
uTwo people are required to lift the device.
uLifting should be done with a person situated on either side of the device.
Inspect external packaging upon receipt for signs of shipping damage. Inspect all items
during unpacking and notify the carrier immediately of any concealed damage. Check for
kinked tubing.
If the system is shipped or removed from storage during cold weather, allow the packaged
equipment to equilibrate to room temperature before opening and exposing to warm, humid
air. It is usually sufficient to provide four to eight hours for this purpose.
CAUTION
Equipment Damage from Condensation
If condensation forms on or inside the unit, allow it to dry thoroughly before connecting it to a
power source and operating it. Failure to do so may cause equipment damage.
Remove the packing checklist from the shipping container, and check off items against it.
Leave accessories in the packing until you are ready to install them.
Note: Keep the factory packaging for use in case the product ever needs to be returned or
shipped to another location.

Transport, Packaging and Storage
20 H148851_4_004